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51.428571 0 0 51.428571 0 1102 Tm 10.091667 0 Td 50.555556 Tz (\(2013.01\); ) Tj 3.305556 0 Td 68.865741 Tz (COIB ) Tj 1.886111 0 Td 55.092593 Tz (3/02 ) Tj 1.575 0 Td 50.231481 Tz (\(2013.01\); ) Tj 3.305556 0 Td 69.675926 Tz (C25B ) Tj 2.002778 0 Td 51.851852 Tz (I/003 ) Tj 51.428571 0 0 51.428571 0 1060 Tm 11.977778 0 Td 50.555556 Tz (\(2013.01\); ) Tj 3.325 0 Td 68.865741 Tz (C25B ) Tj 1.983333 0 Td 50.231481 Tz (I/04 ) Tj 1.458333 0 Td 50.555556 Tz (\(2013.01\); ) Tj 3.305556 0 Td 69.675926 Tz (C25B ) Tj 51.428571 0 0 51.428571 0 1018 Tm 10.130556 0 Td 56.481481 Tz (II/0447 ) Tj 2.547222 0 Td 50.231481 Tz (\(2013.01\); ) Tj 3.286111 0 Td 62.384259 Tz (B01J ) Tj 1.75 0 Td 56.712963 Tz (2531/845 ) Tj 2.975 0 Td 50.231481 Tz (\(2013.01\); ) Tj 51.428571 0 0 51.428571 0 977 Tm 16.858333 0 Td 64.00463 Tz (Y02E ) Tj 1.788889 0 Td 55.092593 Tz (60/366 ) Tj 2.236111 0 Td 52.572016 Tz (\(2013.01\) ) Tj 51.428571 0 0 51.428571 0 2764 Tm 25.219444 0 Td 50.231481 Tz (\(58\) ) Tj 1.963889 0 Td 50.555556 Tz (Field ) Tj 1.808333 0 Td 53.472222 Tz (of ) Tj 0.836111 0 Td 49.074074 Tz (Classification ) Tj 4.355556 0 Td 59.953704 Tz (Search ) Tj 48.571429 0 0 48.571429 0 2726 Tm 28.741176 0 Td 78.921569 Tz (CPC ) Tj 1.811765 0 Td 40.03268 Tz (... ) Tj 1.070588 0 Td 64.338235 Tz (B01J ) Tj 1.791176 0 Td 57.046569 Tz (31/1815; ) Tj 2.964706 0 Td 65.196078 Tz (B01J ) Tj 1.811765 0 Td 56.617647 Tz (31/2295; ) Tj 2.964706 0 Td 73.77451 Tz (C25B ) Tj 2.1 0 Td 52.614379 Tz (1/003; ) Tj 40 0 0 40 0 2690 Tm 50.7 0 Td 89.583333 Tz (C25B ) Tj 2.575 0 Td 64.583333 Tz (1/04 ) Tj 51.428571 0 0 51.428571 0 2646.068702 Tm 27.163889 0 Td 58.333333 Tz (See ) Tj 1.244444 0 Td 49.200337 Tz (application ) Tj 3.519444 0 Td 38.078704 Tz (file ) Tj 1.166667 0 Td 47.530864 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (complete ) Tj 2.916667 0 Td 51.311728 Tz (search ) Tj 2.080556 0 Td 44.560185 Tz (history. ) Tj 42.857143 0 0 42.857143 0 2568.465409 Tm 30.263333 0 Td 59.305556 Tz (\(56\) ) Tj 7.326667 0 Td 66.111111 Tz (References ) Tj 4.293333 0 Td 67.666667 Tz (Cited ) Tj 38.571429 0 0 38.571429 0 2498 Tm 39.277778 0 Td 70.216049 Tz (U.S. ) Tj 2.1 0 Td 96.502058 Tz (PATENT ) Tj 3.837037 0 Td 110.42524 Tz (DOCUMENTS ) Tj 35.714286 0 0 35.714286 0 2426 Tm 36.848 0 Td 74.277778 Tz (2008/0308407 ) Tj 5.88 0 Td 91.777778 Tz (A1* ) Tj 2.492 0 Td 69.333333 Tz (12/2008 ) Tj 3.696 0 Td 67.2 Tz (Rostovtsev ) Tj 4.62 0 Td 38.051282 Tz (............. ) Tj 3.36 0 Td 91 Tz (CO1B ) Tj 2.408 0 Td 70 Tz (3.042 ) Tj 35.714286 0 0 35.714286 0 2389 Tm 57.204 0 Td 70 Tz (204,157.47 ) Tj 35.714286 0 0 35.714286 0 2355 Tm 36.876 0 Td 73.888889 Tz (2011/0042227 ) Tj 5.852 0 Td 88.666667 Tz (A1 ) Tj 2.912 0 Td 66.888889 Tz (2/2011 ) Tj 3.248 0 Td 73.111111 Tz (Corbea ) Tj 3.276 0 Td 38.033333 Tz (.................... ) Tj 5.012 0 Td 79.333333 Tz (B01J ) Tj 2.156 0 Td 56 Tz (31, ) Tj 1.316 0 Td 63 Tz (16 ) Tj 35.714286 0 0 35.714286 0 2317 Tm 58.38 0 Td 63 Tz (205/.340 ) Tj 35.714286 0 0 35.714286 0 2283 Tm 36.876 0 Td 73.888889 Tz (2013/O181174 ) Tj 5.852 0 Td 91.777778 Tz (A1* ) Tj 2.884 0 Td 44.333333 Tz (7, ) Tj 0.672 0 Td 75.833333 Tz (2013 ) Tj 2.604 0 Td 73.111111 Tz (Pan ) Tj 1.876 0 Td 38.222222 Tz (..................... ) Tj 5.32 0 Td 85.166667 Tz (CO7F ) Tj 2.408 0 Td 68.666667 Tz (15.OO33 ) Tj 35.714286 0 0 35.714286 0 2246 Tm 57.68 0 Td 62.066667 Tz (252/.519.2 ) Tj 38.571429 0 0 38.571429 0 2154 Tm 40.003704 0 Td 108.024691 Tz (OTHER ) Tj 3.62963 0 Td 94.701646 Tz (PUBLICATIONS ) Tj 45.714286 0 0 45.714286 0 2080.028777 Tm 28.328125 0 Td 62.708333 Tz (Zhang ) Tj 2.1 0 Td 47.193287 Tz (\("Electrocatalytic ) Tj 5.29375 0 Td 57.421875 Tz (hydrogen ) Tj 2.975 0 Td 50.231481 Tz (evolution ) Tj 2.93125 0 Td 58.333333 Tz (from ) Tj 1.61875 0 Td 47.916667 Tz (neutral ) Tj 2.23125 0 Td 53.958333 Tz (water ) Tj 1.771875 0 Td 63.802083 Tz (by ) Tj 45.714286 0 0 45.714286 0 2038.691542 Tm 28.35 0 Td 54.282407 Tz (molecular ) Tj 3.325 0 Td 49.826389 Tz (cobalt ) Tj 2.209375 0 Td 49.698465 Tz (tripyridine-diamine ) Tj 6.08125 0 Td 54.6875 Tz (complexes. ) Tj 4.025 0 Td 63.4375 Tz (Chem. ) Tj 2.31875 0 Td 93.576389 Tz (Com ) Tj 45.714286 0 0 45.714286 0 1994.884157 Tm 28.35 0 Td 54.6875 Tz (mun., ) Tj 1.903125 0 Td 53.958333 Tz (2013, ) Tj 1.8375 0 Td 52.256944 Tz (49, ) Tj 1.1375 0 Td 49.21875 Tz (p. ) Tj 0.83125 0 Td 57.604167 Tz (9455\) ) Tj 2.40625 0 Td 53.06713 Tz (published ) Tj 3.10625 0 Td 41.015625 Tz (Jul. ) Tj 1.26875 0 Td 43.75 Tz (8, ) Tj 0.809375 0 Td 54.079861 Tz (2013.* ) Tj 51.428571 0 0 51.428571 0 1942 Tm 32.2 0 Td 52.73569 Tz (\(Continued\) ) Tj 51.428571 0 0 51.428571 0 1864.803636 Tm 25.2 0 Td 57.407407 Tz (Primary ) Tj 2.722222 0 Td 58.333333 Tz (Examiner ) Tj 2.955556 0 Td 113.425926 Tz ( ) Tj 0.855556 0 Td 52.662037 Tz (Nicholas ) Tj 2.780556 0 Td 84.259259 Tz (A ) Tj 0.7 0 Td 58.981481 Tz (Smith ) Tj 51.428571 0 0 51.428571 0 1820.385417 Tm 25.219444 0 Td 49.421296 Tz (\(74\) ) Tj 1.536111 0 Td 48.611111 Tz (Attorney, ) Tj 2.877778 0 Td 50.771605 Tz (Agent, ) Tj 2.158333 0 Td 55.092593 Tz (or ) Tj 0.933333 0 Td 57.523148 Tz (Firm ) Tj 1.575 0 Td 113.425926 Tz ( ) Tj 0.836111 0 Td 57.037037 Tz (Mintz ) Tj 2.002778 0 Td 55.092593 Tz (Levin ) Tj 1.905556 0 Td 65.625 Tz (Cohn ) Tj 1.866667 0 Td 45.37037 Tz (Ferris ) Tj 51.428571 0 0 51.428571 0 1778.476712 Tm 25.2 0 Td 58.333333 Tz (Glovsky ) Tj 2.702778 0 Td 59.41358 Tz (and ) Tj 1.341667 0 Td 54.012346 Tz (Popeo, ) Tj 2.216667 0 Td 44.074074 Tz (P.C.; ) Tj 1.613889 0 Td 50.555556 Tz (Peter ) Tj 1.75 0 Td 38.888889 Tz (F. ) Tj 0.738889 0 Td 49.016204 Tz (Corless; ) Tj 2.605556 0 Td 52.662037 Tz (Carolina ) Tj 2.819444 0 Td 45.37037 Tz (E. ) Tj 38.571429 0 0 38.571429 0 1743 Tm 33.625926 0 Td 77.777778 Tz (Sve ) Tj 45 0 0 45 0 1662.165414 Tm 28.822222 0 Td 56.481481 Tz (\(57\) ) Tj 7.666667 0 Td 94.907407 Tz (ABSTRACT ) Tj 51.428571 0 0 51.428571 0 1597.673203 Tm 25.2 0 Td 63.734568 Tz (The ) Tj 1.438889 0 Td 50.411523 Tz (invention ) Tj 3.072222 0 Td 43.981481 Tz 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) Tj 2.936111 0 Td 52.662037 Tz (with ) Tj 1.711111 0 Td 54.444444 Tz (remarkable ) Tj 51.428571 0 0 51.428571 0 1288.615861 Tm 6.241667 0 Td 52.256944 Tz (turnover ) Tj 2.722222 0 Td 61.574074 Tz (number ) Tj 2.411111 0 Td 65.462963 Tz (\(TON\) ) Tj 2.138889 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 62.87037 Tz (>2700 ) Tj 2.061111 0 Td 52.932099 Tz (per ) Tj 1.147222 0 Td 60.493827 Tz (mol ) Tj 1.302778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 71.296296 Tz (Co ) Tj 1.069444 0 Td 46.180556 Tz (catalyst ) Tj 2.430556 0 Td 50.231481 Tz (in ) Tj 60 0 0 60 0 1245 Tm 5.366667 0 Td 44.444444 Tz (a ) Tj 0.533333 0 Td 37.962963 Tz (1:1 ) Tj 0.966667 0 Td 37.222222 Tz (ratio ) Tj 1.35 0 Td 50 Tz (of ) Tj 0.733333 0 Td 73.45679 Tz (CHCN/HO.' ) Tj 51.428571 0 0 51.428571 0 1208.737374 Tm 7 0 Td 56.712963 Tz (Although ) Tj 2.916667 0 Td 49.259259 Tz (there ) Tj 1.652778 0 Td 52.932099 Tz (has ) Tj 1.127778 0 Td 57.523148 Tz (been ) Tj 1.575 0 Td 46.254209 Tz (significant ) Tj 3.227778 0 Td 51.041667 Tz (progress ) Tj 2.663889 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 52.211934 Tz (designing ) Tj 51.428571 0 0 51.428571 0 1163.34375 Tm 6.261111 0 Td 54.372428 Tz (molecular ) Tj 3.188889 0 Td 46.450617 Tz (catalysts ) Tj 2.819444 0 Td 47.530864 Tz (for ) Tj 1.147222 0 Td 87.5 Tz (H ) Tj 1.069444 0 Td 48.287037 Tz (evolution, ) Tj 3.227778 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 50.771605 Tz (search ) Tj 2.138889 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 49.691358 Tz (robust ) Tj 51.428571 0 0 51.428571 0 1125.158028 Tm 6.261111 0 Td 58.333333 Tz (and ) Tj 1.263889 0 Td 51.851852 Tz (highly ) Tj 2.080556 0 Td 49.151235 Tz (active ) Tj 2.002778 0 Td 45.730453 Tz (catalysts ) Tj 2.683333 0 Td 46.990741 Tz (that ) Tj 1.341667 0 Td 55.092593 Tz (can ) Tj 1.263889 0 Td 50.462963 Tz (operate ) Tj 2.352778 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 51.311728 Tz (purely ) Tj 2.080556 0 Td 67.24537 Tz (aque ) Tj 51.428571 0 0 51.428571 0 1081.589421 Tm 6.261111 0 Td 56.17284 Tz (ous ) Tj 1.380556 0 Td 46.090535 Tz (Solution, ) Tj 2.838889 0 Td 59.953704 Tz (by ) Tj 1.069444 0 Td 46.990741 Tz (either ) Tj 1.983333 0 Td 51.203704 Tz (electrochemical ) Tj 4.958333 0 Td 53.472222 Tz (or ) Tj 0.952778 0 Td 54.843305 Tz (photochemical ) Tj 58.571429 0 0 58.571429 0 1043.138249 Tm 5.497561 0 Td 45.78714 Tz (approaches, ) Tj 3.226829 0 Td 31.869919 Tz (still ) Tj 1.178049 0 Td 47.96748 Tz (remains ) Tj 2.202439 0 Td 51.219512 Tz (a ) Tj 0.495122 0 Td 43.252033 Tz (great ) Tj 1.502439 0 Td 49.408721 Tz (challenge.' ) Tj 3.602439 0 Td 42.682927 Tz (' ) Tj 38.571429 0 0 38.571429 0 966 Tm 12.859259 0 Td 117.283951 Tz (SUMMARY ) Tj 5.211111 0 Td 101.54321 Tz (OF ) Tj 1.555556 0 Td 105.144033 Tz (THE ) Tj 2.22963 0 Td 98.902606 Tz (INVENTION ) Tj 51.428571 0 0 51.428571 0 878.084337 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.438889 0 Td 50.05144 Tz (invention ) Tj 3.013889 0 Td 51.851852 Tz (provides ) Tj 2.819444 0 Td 52.5 Tz (novel ) Tj 1.925 0 Td 51.851852 Tz (metal ) Tj 1.847222 0 Td 57.613169 Tz (complexes ) Tj 3.441667 0 Td 44.560185 Tz (that ) Tj 1.361111 0 Td 49.691358 Tz (are ) Tj 51.428571 0 0 51.428571 0 836.042408 Tm 6.241667 0 Td 49.691358 Tz (useful ) Tj 2.197222 0 Td 48.611111 Tz (as ) Tj 1.011111 0 Td 45.730453 Tz (catalysts ) Tj 2.897222 0 Td 43.75 Tz (in ) Tj 0.933333 0 Td 55.092593 Tz (redox ) Tj 2.041667 0 Td 46.342593 Tz (reactions. ) Tj 3.208333 0 Td 48.611111 Tz (In ) Tj 0.972222 0 Td 44.486532 Tz (particular, ) Tj 3.344444 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 796.499356 Tm 6.261111 0 Td 50.771605 Tz (invention ) Tj 3.111111 0 Td 52.662037 Tz (provides ) Tj 2.955556 0 Td 52.5 Tz (metal ) Tj 1.963889 0 Td 54.768519 Tz (complexes, ) Tj 3.694444 0 Td 58.333333 Tz (which ) Tj 2.158333 0 Td 55.902778 Tz (comprise ) Tj 3.052778 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 754.095238 Tm 6.261111 0 Td 44.722222 Tz (least ) Tj 1.516667 0 Td 58.333333 Tz (one ) Tj 1.244444 0 Td 45.37037 Tz (transition ) Tj 2.955556 0 Td 52.5 Tz (metal ) Tj 1.75 0 Td 59.41358 Tz (complexed ) Tj 3.383333 0 Td 53.472222 Tz (with ) Tj 1.458333 0 Td 53.674769 Tz (N,N-bis\(2-pyridi ) Tj 51.428571 0 0 51.428571 0 717 Tm 6.261111 0 Td 52.013889 Tz (nylmethyl\)-2,2'-bipyridine-6-methanamine ) Tj 13.980556 0 Td 57.685185 Tz (\(DPA-Bpy\), ) Tj 51.428571 0 0 51.428571 0 675 Tm 6.261111 0 Td 51.157407 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin ) Tj 51.428571 0 0 51.428571 0 630.374241 Tm 6.261111 0 Td 55.700231 Tz (2-yl\)methanamine ) Tj 5.6 0 Td 56.712963 Tz (\(DIQ-Bpy\), ) Tj 3.655556 0 Td 55.092593 Tz (or ) Tj 0.836111 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 48.611111 Tz (derivative ) Tj 3.169444 0 Td 45.775463 Tz (thereof. ) Tj 2.469444 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 586.889734 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.886111 0 Td 56.893004 Tz (complexes ) Tj 3.325 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.411523 Tz (invention ) Tj 2.955556 0 Td 50.771605 Tz (are ) Tj 1.166667 0 Td 48.611111 Tz (useful ) Tj 1.983333 0 Td 50.231481 Tz (as ) Tj 0.875 0 Td 45.730453 Tz (catalysts ) Tj 2.741667 0 Td 48.611111 Tz (in ) Tj 51.428571 0 0 51.428571 0 544.976303 Tm 6.241667 0 Td 57.928241 Tz (hydrogen ) Tj 2.936111 0 Td 50.378788 Tz (production. ) Tj 3.538889 0 Td 46.990741 Tz (In ) Tj 0.758333 0 Td 46.759259 Tz (certain ) Tj 2.138889 0 Td 57.253086 Tz (embodiments, ) Tj 4.297222 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 51.131687 Tz (invention ) Tj 51.428571 0 0 51.428571 0 505.948749 Tm 6.261111 0 Td 51.851852 Tz (provides ) Tj 2.702778 0 Td 52.5 Tz (novel ) Tj 1.730556 0 Td 69.675926 Tz (Co ) Tj 1.011111 0 Td 57.613169 Tz (complexes ) Tj 3.266667 0 Td 50.231481 Tz (as ) Tj 0.758333 0 Td 43.569959 Tz (efficient ) Tj 2.488889 0 Td 46.788194 Tz (electrocatalysts ) Tj 4.686111 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 461.829016 Tm 6.261111 0 Td 54.73251 Tz (producing ) Tj 3.266667 0 Td 56.712963 Tz (H2 ) Tj 1.05 0 Td 57.523148 Tz (from ) Tj 1.652778 0 Td 58.333333 Tz (an ) Tj 0.972222 0 Td 56.018519 Tz (aqueous ) Tj 2.663889 0 Td 46.090535 Tz (Solution. ) Tj 2.838889 0 Td 43.75 Tz (In ) Tj 0.836111 0 Td 50.555556 Tz (other ) Tj 1.769444 0 Td 66.975309 Tz (embodi ) Tj 51.428571 0 0 51.428571 0 420.907243 Tm 6.261111 0 Td 52.932099 Tz (ments, ) Tj 2.177778 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 50.771605 Tz (invention ) Tj 3.013889 0 Td 51.851852 Tz (provides ) Tj 2.780556 0 Td 52.5 Tz (novel ) Tj 1.827778 0 Td 71.296296 Tz (Co ) Tj 1.147222 0 Td 56.893004 Tz (complexes ) Tj 3.325 0 Td 51.851852 Tz (as ) Tj 0.894444 0 Td 47.800926 Tz (effi ) Tj 51.428571 0 0 51.428571 0 381.247657 Tm 6.261111 0 Td 47.314815 Tz (cient ) Tj 1.788889 0 Td 49.768519 Tz (photocatalysts ) Tj 4.608333 0 Td 47.530864 Tz (for ) Tj 1.205556 0 Td 55.092593 Tz (producing ) Tj 3.402778 0 Td 58.333333 Tz (H2 ) Tj 1.205556 0 Td 56.712963 Tz (from ) Tj 1.788889 0 Td 55.092593 Tz (an ) Tj 1.088889 0 Td 56.481481 Tz (aqueous ) Tj 40 0 0 40 0 343 Tm 8.075 0 Td 63.020833 Tz (Solution ) Tj 51.428571 0 0 51.428571 0 295.455026 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.797222 0 Td 57.253086 Tz (one ) Tj 1.205556 0 Td 47.685185 Tz (aspect, ) Tj 2.197222 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 50.411523 Tz (invention ) Tj 2.936111 0 Td 44.444444 Tz (relates ) Tj 2.080556 0 Td 45.37037 Tz (to ) Tj 0.758333 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 52.5 Tz (metal ) Tj 1.788889 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 251 Tm 6.261111 0 Td 54.62963 Tz (formula ) Tj 2.566667 0 Td 38.888889 Tz (\(I\) ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 40 0 0 40 0 2921 Tm 32.375 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 2872 Tm 27.444118 0 Td 113.235294 Tz (M ) Tj 0.947059 0 Td 41.176471 Tz (is ) Tj 0.741176 0 Td 61.764706 Tz (a ) Tj 0.658824 0 Td 47.696078 Tz (transition ) Tj 3.170588 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 2833.52657 Tm 25.919444 0 Td 84.259259 Tz (G ) Tj 0.836111 0 Td 37.268519 Tz (is ) Tj 0.758333 0 Td 51.521164 Tz (N,N-bis\(2-pyridinylmethyl\)-2,2'-bipyridine-6-meth ) Tj 51.428571 0 0 51.428571 0 2788.833333 Tm 25.2 0 Td 58.333333 Tz (anamine ) Tj 2.780556 0 Td 58.333333 Tz (\(DPA-Bpy\), ) Tj 3.830556 0 Td 51.666667 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6- ) Tj 51.428571 0 0 51.428571 0 2746.533414 Tm 25.219444 0 Td 51.169591 Tz (\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 12.152778 0 Td 56.712963 Tz (\(DIQ-Bpy\), ) Tj 3.908333 0 Td 50.231481 Tz (or ) Tj 1.069444 0 Td 55.092593 Tz (a ) Tj 48.571429 0 0 48.571429 0 2697 Tm 26.682353 0 Td 51.470588 Tz (derivative ) Tj 3.355882 0 Td 52.45098 Tz (thereof ) Tj 51.428571 0 0 51.428571 0 2655.299742 Tm 25.9 0 Td 51.851852 Tz (Y, ) Tj 0.855556 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 54.282407 Tz (each ) Tj 1.555556 0 Td 50.673401 Tz (occurrence, ) Tj 3.558333 0 Td 52.599715 Tz (independently ) Tj 4.336111 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 55.092593 Tz (halogen ) Tj 2.527778 0 Td 55.740741 Tz (group ) Tj 51.428571 0 0 51.428571 0 2611.672131 Tm 25.2 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 53.796296 Tz (water ) Tj 1.847222 0 Td 51.851852 Tz (moiety; ) Tj 51.428571 0 0 51.428571 0 2566.45706 Tm 25.9 0 Td 59.953704 Tz (X, ) Tj 0.972222 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 50.968013 Tz (occurrence, ) Tj 3.616667 0 Td 52.599715 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (an ) Tj 0.933333 0 Td 50.231481 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 2522.425806 Tm 25.919444 0 Td 90.740741 Tz (m ) Tj 0.836111 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 61.033951 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 2479.476821 Tm 25.919444 0 Td 58.333333 Tz (n ) Tj 0.641667 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 52.932099 Tz (anions ) Tj 2.158333 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.902778 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 2435 Tm 27.464706 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 42.892157 Tz (is ) Tj 0.782353 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 53.186275 Tz (or ) Tj 0.864706 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50.490196 Tz (neutral ) Tj 2.429412 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 2390.917001 Tm 25.919444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 46.296296 Tz (neutral ) Tj 2.236111 0 Td 54.012346 Tz (molecules ) Tj 3.15 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 59.259259 Tz (complex ) Tj 51.428571 0 0 51.428571 0 2349.025907 Tm 25.219444 0 Td 39.429012 Tz (\(e.g., ) Tj 1.711111 0 Td 42.12963 Tz (0, ) Tj 0.855556 0 Td 35.648148 Tz (1, ) Tj 0.7 0 Td 53.472222 Tz (or ) Tj 0.875 0 Td 42.12963 Tz (2\); ) Tj 51.428571 0 0 51.428571 0 2308.087855 Tm 25.919444 0 Td 53.877315 Tz (provided ) Tj 2.916667 0 Td 45.37037 Tz (that ) Tj 1.419444 0 Td 64.00463 Tz (when ) Tj 1.866667 0 Td 84.259259 Tz (G ) Tj 0.855556 0 Td 38.888889 Tz (is ) Tj 0.797222 0 Td 50.957854 Tz (N,N-bis\(2-pyridinylmethyl\)-2, ) Tj 51.428571 0 0 51.428571 0 2264.41039 Tm 25.2 0 Td 52.451989 Tz (2'-bipyridine-6-methanamine ) Tj 8.75 0 Td 58.333333 Tz (\(DPA-Bpy\), ) Tj 3.733333 0 Td 106.944444 Tz (M ) Tj 0.894444 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 50.771605 Tz (not ) Tj 1.186111 0 Td 52.932099 Tz (Ru. ) Tj 51.428571 0 0 51.428571 0 2219.040609 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.855556 0 Td 46.759259 Tz (certain ) Tj 2.236111 0 Td 56.712963 Tz (embodiments, ) Tj 4.355556 0 Td 84.259259 Tz (G ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.719444 0 Td 51.592593 Tz (N,N-bis\(isoquinolin-1-yl\) ) Tj 51.428571 0 0 51.428571 0 2178.152941 Tm 25.2 0 Td 51.311728 Tz (methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 15.711111 0 Td 72.916667 Tz (\(DIQ ) Tj 51.428571 0 0 51.428571 0 2131.272727 Tm 25.219444 0 Td 53.148148 Tz (Bpy\). ) Tj 1.963889 0 Td 46.990741 Tz (In ) Tj 0.913889 0 Td 50.555556 Tz (other ) Tj 1.808333 0 Td 56.983025 Tz (embodiments, ) Tj 4.433333 0 Td 87.5 Tz (G ) Tj 0.875 0 Td 38.888889 Tz (is ) Tj 0.816667 0 Td 55.25463 Tz (N,N-bis\(2-pyridinylm ) Tj 51.428571 0 0 51.428571 0 2092 Tm 25.2 0 Td 50.861626 Tz (ethyl\)-2,2'-bipyridine-6-methanamine ) Tj 11.219444 0 Td 58.009259 Tz (\(DPA-Bpy\). ) Tj 48.571429 0 0 48.571429 0 2042 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 0.988235 0 Td 50.490196 Tz (certain ) Tj 2.511765 0 Td 60.04902 Tz (embodiments, ) Tj 4.735294 0 Td 109.803922 Tz (M ) Tj 1.070588 0 Td 42.892157 Tz (is ) Tj 0.885294 0 Td 61.764706 Tz (Co, ) Tj 1.564706 0 Td 57.189542 Tz (Ru, ) Tj 1.420588 0 Td 56.617647 Tz (or ) Tj 1.05 0 Td 51.470588 Tz (Fe. ) Tj 1.358824 0 Td 49.754902 Tz (In ) Tj 1.008824 0 Td 61.764706 Tz (one ) Tj 48.571429 0 0 48.571429 0 1998 Tm 26.682353 0 Td 61.14082 Tz (embodiment, ) Tj 4.323529 0 Td 109.803922 Tz (M ) Tj 0.947059 0 Td 39.460784 Tz (is ) Tj 0.720588 0 Td 60.620915 Tz (Co. ) Tj 51.428571 0 0 51.428571 0 1954.262613 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.738889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 49.421296 Tz (separate ) Tj 2.488889 0 Td 58.038721 Tz (embodiment, ) Tj 4.005556 0 Td 84.259259 Tz (Y ) Tj 0.661111 0 Td 42.12963 Tz (in ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 54.166667 Tz (formula ) Tj 2.430556 0 Td 39.969136 Tz (\(I\) ) Tj 0.894444 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 47.170782 Tz (chloride. ) Tj 48.571429 0 0 48.571429 0 1911 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 0.844118 0 Td 60.620915 Tz (one ) Tj 1.255882 0 Td 61.452763 Tz (embodiment, ) Tj 4.220588 0 Td 61.764706 Tz (a ) Tj 0.555882 0 Td 41.176471 Tz (is ) Tj 0.720588 0 Td 44.607843 Tz (0. ) Tj 0.782353 0 Td 49.754902 Tz (In ) Tj 0.761765 0 Td 56.372549 Tz (another ) Tj 2.532353 0 Td 61.14082 Tz (embodiment, ) Tj 4.220588 0 Td 54.901961 Tz (a ) Tj 0.555882 0 Td 39.460784 Tz (is ) Tj 0.741176 0 Td 41.176471 Tz (1. ) Tj 51.428571 0 0 51.428571 0 1867.366887 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 46.296296 Tz (certain ) Tj 2.216667 0 Td 57.253086 Tz (embodiments, ) Tj 4.394444 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 49.691358 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.8 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1823.400271 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 61.574074 Tz (of ) Tj 0.933333 0 Td 54.166667 Tz (formula ) Tj 2.586111 0 Td 36.458333 Tz (\(I\), ) Tj 1.205556 0 Td 45.37037 Tz (in ) Tj 0.855556 0 Td 58.333333 Tz (which ) Tj 2.041667 0 Td 90.740741 Tz (X ) Tj 0.855556 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 61.574074 Tz (same ) Tj 1.769444 0 Td 48.611111 Tz (for ) Tj 1.127778 0 Td 56.712963 Tz (each ) Tj 40 0 0 40 0 1786 Tm 32.4 0 Td 68.333333 Tz (occurrence ) Tj 4.425 0 Td 75 Tz (and ) Tj 1.675 0 Td 47.916667 Tz (is ) Tj 0.875 0 Td 84.722222 Tz (Cl. ) Tj 52.857143 0 0 52.857143 0 1737.822917 Tm 25.237838 0 Td 47.297297 Tz (In ) Tj 0.775676 0 Td 49.189189 Tz (other ) Tj 1.608108 0 Td 55.705706 Tz (embodiments, ) Tj 4.237838 0 Td 59.90991 Tz (L ) Tj 0.548649 0 Td 45.720721 Tz (in ) Tj 0.737838 0 Td 48.348348 Tz (the ) Tj 1.078378 0 Td 52.702703 Tz (formula ) Tj 2.421622 0 Td 38.888889 Tz (\(I\) ) Tj 0.87027 0 Td 39.414414 Tz (is ) Tj 0.681081 0 Td 68.975225 Tz (\(C\)alkyl ) Tj 51.428571 0 0 51.428571 0 1697.285714 Tm 25.2 0 Td 82.638889 Tz (CN ) Tj 1.244444 0 Td 41.049383 Tz (\(e.g., ) Tj 1.730556 0 Td 75.07716 Tz (CHCN\). ) Tj 51.428571 0 0 51.428571 0 1655.540682 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.913889 0 Td 45.775463 Tz (specific ) Tj 2.508333 0 Td 57.253086 Tz (embodiments, ) Tj 4.433333 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 50.411523 Tz (invention ) Tj 3.033333 0 Td 52.256944 Tz (provides ) Tj 2.838889 0 Td 49.691358 Tz (cobalt ) Tj 51.428571 0 0 51.428571 0 1616.97416 Tm 25.2 0 Td 54.768519 Tz (complexes, ) Tj 3.655556 0 Td 54.282407 Tz (such ) Tj 1.652778 0 Td 48.611111 Tz (as ) Tj 0.933333 0 Td 63.069801 Tz (Co\(DPA-Bpy\)C1 ) Tj 5.522222 0 Td 56.17284 Tz (\(complex ) Tj 3.461111 0 Td 46.450617 Tz (1\) ) Tj 1.166667 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 1577 Tm 25.394444 0 Td 64.944444 Tz (Co\(DPA-Bpy\)\(Cl\)Cl.\(CHCN\). ) Tj 51.428571 0 0 51.428571 0 1530.639281 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.836111 0 Td 49.907407 Tz (other ) Tj 1.672222 0 Td 57.253086 Tz (embodiments, ) Tj 4.355556 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 50.411523 Tz (invention ) Tj 2.936111 0 Td 52.256944 Tz (provides ) Tj 2.741667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 59.259259 Tz (complex ) Tj 51.428571 0 0 51.428571 0 1493.669725 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 1.205556 0 Td 51.118099 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyri ) Tj 51.428571 0 0 51.428571 0 1451.269182 Tm 25.2 0 Td 54.282407 Tz (din-2-yl\)methanamine ) Tj 6.902778 0 Td 56.388889 Tz (\(DIQ-Bpy\). ) Tj 3.830556 0 Td 46.990741 Tz (In ) Tj 0.952778 0 Td 55.092593 Tz (a ) Tj 0.738889 0 Td 46.180556 Tz (specific ) Tj 2.586111 0 Td 68.055556 Tz (embodi ) Tj 51.428571 0 0 51.428571 0 1407.787724 Tm 25.2 0 Td 53.796296 Tz (ment, ) Tj 1.963889 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 50.05144 Tz (invention ) Tj 3.033333 0 Td 52.256944 Tz (provides ) Tj 2.858333 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 59.722222 Tz (complex ) Tj 3.072222 0 Td 61.868687 Tz (Ru\(DIQ-Bpy\) ) Tj 51.428571 0 0 51.428571 0 1363.945322 Tm 25.219444 0 Td 52.777778 Tz (\(Cl\)Cl. ) Tj 2.294444 0 Td 88.796296 Tz (\(HO\), ) Tj 3.130556 0 Td 65.462963 Tz (Ru\(DIQ-Bpy\)\(HO\) ) Tj 6.163889 0 Td 66.111111 Tz (\(PF\), ) Tj 2.197222 0 Td 51.851852 Tz (or ) Tj 1.030556 0 Td 72.916667 Tz (Ru\(DIQ ) Tj 51.428571 0 0 51.428571 0 1323.58804 Tm 25.2 0 Td 54.6875 Tz (Bpy\)\(Cl\) ) Tj 2.897222 0 Td 59.773663 Tz (\(PF\).H.O. ) Tj 51.428571 0 0 51.428571 0 1279.366887 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 46.296296 Tz (certain ) Tj 2.216667 0 Td 57.253086 Tz (embodiments, ) Tj 4.394444 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 49.691358 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.8 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1240.099099 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 54.62963 Tz (formula ) Tj 2.547222 0 Td 39.699074 Tz (\(II\) ) Tj 40 0 0 40 0 509 Tm 32.375 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 461 Tm 27.444118 0 Td 113.235294 Tz (M ) Tj 0.967647 0 Td 39.460784 Tz (is ) Tj 0.761765 0 Td 59.477124 Tz (Co, ) Tj 1.379412 0 Td 58.333333 Tz (Ru, ) Tj 1.276471 0 Td 54.901961 Tz (Ni, ) Tj 1.276471 0 Td 53.186275 Tz (or ) Tj 0.885294 0 Td 52.614379 Tz (Fe: ) Tj 52.857143 0 0 52.857143 0 421.031579 Tm 25.237838 0 Td 52.027027 Tz (R, ) Tj 0.889189 0 Td 47.297297 Tz (for ) Tj 1.059459 0 Td 54.391892 Tz (each ) Tj 1.589189 0 Td 49.5905 Tz (occurrence, ) Tj 3.518919 0 Td 51.420651 Tz (independently ) Tj 4.275676 0 Td 37.837838 Tz (is ) Tj 0.756757 0 Td 52.027027 Tz (H. ) Tj 0.927027 0 Td 59.90991 Tz (\(C\)alkyl, ) Tj 51.428571 0 0 51.428571 0 381.782557 Tm 25.2 0 Td 52.932099 Tz (cyano, ) Tj 2.061111 0 Td 44.722222 Tz (aryl, ) Tj 1.497222 0 Td 50.925926 Tz (benzyl, ) Tj 2.313889 0 Td 55.092593 Tz (amino, ) Tj 2.177778 0 Td 39.699074 Tz (nitrile, ) Tj 2.080556 0 Td 49.691358 Tz (carboxylate, ) Tj 3.733333 0 Td 51.851852 Tz (hydroxyl, ) Tj 3.013889 0 Td 51.851852 Tz (or ) Tj 42.857143 0 0 42.857143 0 337 Tm 30.24 0 Td 51.851852 Tz (ester, ) Tj 51.428571 0 0 51.428571 0 295.486009 Tm 25.9 0 Td 59.953704 Tz (X, ) Tj 0.972222 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 50.968013 Tz (occurrence, ) Tj 3.616667 0 Td 52.599715 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (an ) Tj 0.933333 0 Td 55.092593 Tz (anion ) Tj 51.428571 0 0 51.428571 0 253.239521 Tm 25.919444 0 Td 58.333333 Tz (Z ) Tj 0.583333 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 49.074074 Tz (cations ) Tj 2.294444 0 Td 54.012346 Tz (per ) Tj 1.225 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex, ) Tj 2.897222 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 212.472727 Tm 25.9 0 Td 61.574074 Tz (b ) Tj 0.661111 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 52.932099 Tz (anions ) Tj 2.158333 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.902778 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 169.919321 Tm 25.919444 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 38.240741 Tz (salt, ) Tj 1.438889 0 Td 48.611111 Tz (solvate ) Tj 2.275 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 52.314815 Tz (hydrate ) Tj 2.469444 0 Td 45.775463 Tz (thereof. ) Tj 1.428571 0 0 1.428571 0 1156 Tm 1028.3 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 264 0 obj << /Length 1 >> stream q endstream endobj 265 0 obj << /Length 42300 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.359459 0 Td 72.522523 Tz (3 ) Tj 51.428571 0 0 51.428571 0 2913 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.952778 0 Td 58.333333 Tz (one ) Tj 1.419444 0 Td 58.038721 Tz (embodiment, ) Tj 4.2 0 Td 106.944444 Tz (M ) Tj 1.05 0 Td 42.12963 Tz (in ) Tj 0.933333 0 Td 48.611111 Tz (the ) Tj 1.263889 0 Td 54.62963 Tz (formula ) Tj 2.683333 0 Td 40.509259 Tz (\(II\) ) Tj 1.322222 0 Td 42.12963 Tz (is ) Tj 0.855556 0 Td 56.17284 Tz (Co. ) Tj 1.438889 0 Td 51.851852 Tz (In ) Tj 51.428571 0 0 51.428571 0 2870 Tm 6.261111 0 Td 52.777778 Tz (another ) Tj 2.430556 0 Td 57.744108 Tz (embodiment, ) Tj 4.083333 0 Td 103.703704 Tz (M ) Tj 0.855556 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 54.62963 Tz (formula ) Tj 2.547222 0 Td 40.509259 Tz (\(II\) ) Tj 1.205556 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 47.530864 Tz (Ni. ) Tj 51.428571 0 0 51.428571 0 2826 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 59.41358 Tz (one ) Tj 1.302778 0 Td 57.449495 Tz (embodiment, ) Tj 4.063889 0 Td 55.092593 Tz (Z ) Tj 0.563889 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 54.62963 Tz (formula ) Tj 2.566667 0 Td 40.509259 Tz (\(II\) ) Tj 1.186111 0 Td 40.509259 Tz (is ) Tj 0.797222 0 Td 38.888889 Tz (1. ) Tj 48.571429 0 0 48.571429 0 2784 Tm 7.432353 0 Td 49.754902 Tz (In ) Tj 0.741176 0 Td 56.372549 Tz (another ) Tj 2.470588 0 Td 61.764706 Tz (embodiment, ) Tj 4.220588 0 Td 96.078431 Tz (X ) Tj 0.741176 0 Td 41.176471 Tz (is ) Tj 0.638235 0 Td 53.75817 Tz (the ) Tj 1.132353 0 Td 65.196078 Tz (same ) Tj 1.75 0 Td 51.470588 Tz (for ) Tj 1.029412 0 Td 59.191176 Tz (each ) Tj 1.585294 0 Td 56.617647 Tz (occurrence ) Tj 52.857143 0 0 52.857143 0 2739.315364 Tm 6.091892 0 Td 56.756757 Tz (and ) Tj 1.305405 0 Td 36.261261 Tz (is ) Tj 0.718919 0 Td 85.135135 Tz (PF. ) Tj 1.816216 0 Td 48.873874 Tz (In ) Tj 0.832432 0 Td 53.603604 Tz (a ) Tj 0.605405 0 Td 48.085586 Tz (separate ) Tj 2.535135 0 Td 56.183456 Tz (embodiment, ) Tj 4.010811 0 Td 81.981982 Tz (X ) Tj 0.756757 0 Td 40.990991 Tz (is ) Tj 0.756757 0 Td 47.297297 Tz (the ) Tj 1.135135 0 Td 59.90991 Tz (same ) Tj 1.702703 0 Td 47.297297 Tz (for ) Tj 51.428571 0 0 51.428571 0 2695 Tm 6.261111 0 Td 55.092593 Tz (each ) Tj 1.594444 0 Td 53.148148 Tz (occurrence ) Tj 3.422222 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 38.888889 Tz (is ) Tj 0.738889 0 Td 89.660494 Tz (BF. ) Tj 51.428571 0 0 51.428571 0 2652.284818 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.719444 0 Td 47.222222 Tz (certain ) Tj 2.158333 0 Td 56.712963 Tz (embodiments, ) Tj 4.277778 0 Td 48.611111 Tz (the ) Tj 1.011111 0 Td 50.771605 Tz (invention ) Tj 2.916667 0 Td 51.851852 Tz (provides ) Tj 2.858333 0 Td 76.697531 Tz (Co\(DPA ) Tj 52.857143 0 0 52.857143 0 2610.91425 Tm 6.091892 0 Td 66.61036 Tz (Bpy\)\(OH\) ) Tj 3.443243 0 Td 57.387387 Tz (\(PF\), ) Tj 2.081081 0 Td 55.005005 Tz (\("complex ) Tj 3.235135 0 Td 58.858859 Tz (2\). ) Tj 1.324324 0 Td 60.960961 Tz (The ) Tj 1.4 0 Td 49.049049 Tz (invention ) Tj 2.913514 0 Td 47.297297 Tz (also ) Tj 1.418919 0 Td 65.165165 Tz (pro ) Tj 51.428571 0 0 51.428571 0 2570.479889 Tm 6.241667 0 Td 51.851852 Tz (vides ) Tj 1.808333 0 Td 69.027778 Tz (NiCDPA-ABpy\)\(OH\)\(BF\) ) Tj 8.536111 0 Td 56.893004 Tz (\(complex ) Tj 3.286111 0 Td 46.180556 Tz (3\). ) Tj 51.428571 0 0 51.428571 0 2523.664122 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.719444 0 Td 53.240741 Tz (another ) Tj 2.352778 0 Td 47.685185 Tz (aspect, ) Tj 2.197222 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 50.411523 Tz (invention ) Tj 2.916667 0 Td 51.851852 Tz (provides ) Tj 2.663889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 51.851852 Tz (metal ) Tj 1.769444 0 Td 59.722222 Tz (complex ) Tj 51.428571 0 0 51.428571 0 2477 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 54.166667 Tz (formula ) Tj 2.547222 0 Td 37.268519 Tz (\(III\): ) Tj 51.428571 0 0 51.428571 0 2332.915254 Tm 6.261111 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 38.240741 Tz (salt, ) Tj 1.438889 0 Td 48.611111 Tz (solvate ) Tj 2.275 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 52.314815 Tz (hydrate ) Tj 2.45 0 Td 46.180556 Tz (thereof; ) Tj 40 0 0 40 0 2298 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 2250 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.926471 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 47.696078 Tz (transition ) Tj 3.191176 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 2213.527141 Tm 7 0 Td 84.259259 Tz (G ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.738889 0 Td 51.587302 Tz (N,N-bis\(2-pyridinylmethyl\)-2,2'-bipyridine-6-meth ) Tj 51.428571 0 0 51.428571 0 2171.826542 Tm 6.261111 0 Td 58.333333 Tz (anamine ) Tj 2.819444 0 Td 57.523148 Tz (\(DPA-Bpy'\), ) Tj 4.530556 0 Td 49.56427 Tz (6'-\(\(bis\(pyridin-2-ylmethyl\)amino\) ) Tj 51.428571 0 0 51.428571 0 2129.881398 Tm 6.261111 0 Td 51.927218 Tz (methyl\)-N,N-dimethyl-2,2'-bipyridin-6-amine ) Tj 15.283333 0 Td 72.592593 Tz (\(DPA ) Tj 51.428571 0 0 51.428571 0 2090 Tm 6.261111 0 Td 59.259259 Tz (ABpy'\), ) Tj 3.422222 0 Td 50.865539 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2- ) Tj 51.428571 0 0 51.428571 0 2046.044444 Tm 6.241667 0 Td 52.572016 Tz (yl\)pyridin-2-yl\)methanamine ) Tj 8.963889 0 Td 56.388889 Tz (\(DIQ-Bpy\), ) Tj 3.811111 0 Td 53.472222 Tz (or ) Tj 1.05 0 Td 51.851852 Tz (a ) Tj 0.777778 0 Td 48.287037 Tz (derivative ) Tj 48.571429 0 0 48.571429 0 2001 Tm 6.608824 0 Td 53.431373 Tz (thereof ) Tj 51.428571 0 0 51.428571 0 1960.330818 Tm 6.980556 0 Td 50.231481 Tz (Y, ) Tj 0.777778 0 Td 49.691358 Tz (for ) Tj 0.991667 0 Td 55.902778 Tz (each ) Tj 1.516667 0 Td 50.968013 Tz (occurrence, ) Tj 3.558333 0 Td 52.350427 Tz (independently ) Tj 4.277778 0 Td 38.888889 Tz (is ) Tj 0.622222 0 Td 48.148148 Tz (absent, ) Tj 2.216667 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 56.018519 Tz (halogen ) Tj 51.428571 0 0 51.428571 0 1919.780781 Tm 6.261111 0 Td 56.388889 Tz (group ) Tj 1.963889 0 Td 51.851852 Tz (or ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.602778 0 Td 54.444444 Tz (water ) Tj 1.866667 0 Td 51.851852 Tz (moiety; ) Tj 51.428571 0 0 51.428571 0 1876.468705 Tm 6.980556 0 Td 59.953704 Tz (X, ) Tj 0.952778 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 51.262626 Tz (occurrence, ) Tj 3.616667 0 Td 52.849003 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 49.691358 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 1834.418006 Tm 7 0 Td 90.740741 Tz (m ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 51.851852 Tz (the ) Tj 1.205556 0 Td 61.574074 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 1793.463576 Tm 7 0 Td 58.333333 Tz (n ) Tj 0.622222 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 52.391975 Tz (anions ) Tj 2.138889 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 1751 Tm 7.432353 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 41.176471 Tz (is ) Tj 0.761765 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 54.901961 Tz (or ) Tj 0.885294 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50 Tz (neutral ) Tj 2.408824 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 1709.922563 Tm 7 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 46.759259 Tz (neutral ) Tj 2.255556 0 Td 54.012346 Tz (molecules ) Tj 3.15 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 52.5 Tz (metal ) Tj 1.827778 0 Td 59.722222 Tz (complex ) Tj 51.428571 0 0 51.428571 0 1669.035897 Tm 6.280556 0 Td 39.969136 Tz (\(e.g., ) Tj 1.711111 0 Td 42.12963 Tz (0, ) Tj 0.855556 0 Td 37.268519 Tz (1, ) Tj 0.7 0 Td 53.472222 Tz (or ) Tj 0.875 0 Td 42.12963 Tz (2\); ) Tj 52.857143 0 0 52.857143 0 1629.06435 Tm 6.791892 0 Td 52.815315 Tz (provided ) Tj 2.818919 0 Td 45.720721 Tz (that ) Tj 1.362162 0 Td 64.63964 Tz (when ) Tj 1.891892 0 Td 75.675676 Tz (G ) Tj 0.794595 0 Td 37.837838 Tz (is ) Tj 0.794595 0 Td 49.471886 Tz (N,N-bis\(2-pyridinylmethyl\)-2, ) Tj 51.428571 0 0 51.428571 0 1588.481898 Tm 6.261111 0 Td 52.451989 Tz (2'-bipyridine-6-methanamine ) Tj 8.769444 0 Td 57.253086 Tz (\(DPA-Bpy'\), ) Tj 4.394444 0 Td 103.703704 Tz (M ) Tj 0.855556 0 Td 38.888889 Tz (is ) Tj 0.777778 0 Td 49.691358 Tz (not ) Tj 1.166667 0 Td 54.012346 Tz (Ru. ) Tj 51.428571 0 0 51.428571 0 1543.807542 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.836111 0 Td 58.333333 Tz (one ) Tj 1.302778 0 Td 47.530864 Tz (instance, ) Tj 2.819444 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.994444 0 Td 64.00463 Tz (NiCDPA-ABpy\) ) Tj 52.857143 0 0 52.857143 0 1499.286783 Tm 6.110811 0 Td 74.624625 Tz (\(OH\)\(BF\). ) Tj 4.389189 0 Td 44.144144 Tz (In ) Tj 0.813514 0 Td 51.801802 Tz (another ) Tj 2.421622 0 Td 46.246246 Tz (instance, ) Tj 2.8 0 Td 48.348348 Tz (the ) Tj 1.172973 0 Td 48.698699 Tz (invention ) Tj 2.932432 0 Td 50.844595 Tz (provides ) Tj 51.428571 0 0 51.428571 0 1465 Tm 6.475 0 Td 68.703704 Tz (Ni\(DPA-Bpy\)\(OH\)\(BF\). ) Tj 51.428571 0 0 51.428571 0 1416.385235 Tm 6.280556 0 Td 48.611111 Tz (In ) Tj 0.952778 0 Td 36.296296 Tz (still ) Tj 1.458333 0 Td 52.777778 Tz (another ) Tj 2.547222 0 Td 47.530864 Tz (instance, ) Tj 2.936111 0 Td 48.611111 Tz (the ) Tj 1.263889 0 Td 50.411523 Tz (invention ) Tj 3.091667 0 Td 52.256944 Tz (provides ) Tj 2.877778 0 Td 58.333333 Tz (a ) Tj 0.738889 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1381.43833 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 68.818083 Tz (Co\(DPA-ABpy\)\(PF\). ) Tj 51.428571 0 0 51.428571 0 1335.080214 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.380556 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 49.421296 Tz (also ) Tj 1.438889 0 Td 51.851852 Tz (provides ) Tj 2.8 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 57.613169 Tz (complexes ) Tj 3.383333 0 Td 45.37037 Tz (in ) Tj 0.855556 0 Td 48.611111 Tz (the ) Tj 51.428571 0 0 51.428571 0 1292.567723 Tm 6.261111 0 Td 58.333333 Tz (form ) Tj 1.672222 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 40.509259 Tz (salts, ) Tj 1.730556 0 Td 46.450617 Tz (Solvates, ) Tj 2.741667 0 Td 48.971193 Tz (hydrates, ) Tj 2.897222 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 49.537037 Tz (stereoisomers. ) Tj 51.428571 0 0 51.428571 0 1251.277078 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.7 0 Td 53.240741 Tz (another ) Tj 2.333333 0 Td 48.148148 Tz (aspect, ) Tj 2.158333 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 50.771605 Tz (invention ) Tj 2.897222 0 Td 44.907407 Tz (relates ) Tj 2.022222 0 Td 48.611111 Tz (to ) Tj 0.738889 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 43.930041 Tz (catalyst, ) Tj 2.527778 0 Td 59.62963 Tz (which ) Tj 51.428571 0 0 51.428571 0 1211.665025 Tm 6.261111 0 Td 54.372428 Tz (comprises ) Tj 3.188889 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 47.962963 Tz (invention. ) Tj 51.428571 0 0 51.428571 0 1170.402235 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.536111 0 Td 50.411523 Tz (invention ) Tj 3.130556 0 Td 49.421296 Tz (also ) Tj 1.594444 0 Td 52.256944 Tz (provides ) Tj 2.916667 0 Td 58.333333 Tz (a ) Tj 0.719444 0 Td 52.314815 Tz (process ) Tj 2.625 0 Td 48.611111 Tz (for ) Tj 1.263889 0 Td 54.73251 Tz (producing ) Tj 51.428571 0 0 51.428571 0 1128.84878 Tm 6.241667 0 Td 57.928241 Tz (hydrogen ) Tj 2.936111 0 Td 57.523148 Tz (from ) Tj 1.555556 0 Td 56.712963 Tz (an ) Tj 0.836111 0 Td 56.481481 Tz (aqueous ) Tj 2.566667 0 Td 48.206019 Tz (solution ) Tj 2.469444 0 Td 59.953704 Tz (by ) Tj 0.894444 0 Td 52.5 Tz (using ) Tj 1.730556 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 46.180556 Tz (catalyst ) Tj 2.372222 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1087.66485 Tm 6.261111 0 Td 48.287037 Tz (invention. ) Tj 3.305556 0 Td 64.814815 Tz (The ) Tj 1.555556 0 Td 52.314815 Tz (process ) Tj 2.625 0 Td 54.372428 Tz (comprises ) Tj 3.344444 0 Td 51.851852 Tz (a ) Tj 0.758333 0 Td 48.611111 Tz (step ) Tj 1.594444 0 Td 56.712963 Tz (of ) Tj 0.972222 0 Td 56.17284 Tz (adding ) Tj 2.430556 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1043.498688 Tm 6.261111 0 Td 46.990741 Tz (catalyst ) Tj 2.488889 0 Td 46.990741 Tz (to ) Tj 0.855556 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 56.481481 Tz (aqueous ) Tj 2.683333 0 Td 46.090535 Tz (solution. ) Tj 2.838889 0 Td 45.37037 Tz (In ) Tj 0.836111 0 Td 58.333333 Tz (one ) Tj 1.341667 0 Td 47.530864 Tz (instance, ) Tj 2.858333 0 Td 55.092593 Tz (an ) Tj 0.972222 0 Td 58.333333 Tz (elec ) Tj 51.428571 0 0 51.428571 0 1004.352941 Tm 6.241667 0 Td 44.965278 Tz (trolysis ) Tj 2.333333 0 Td 48.611111 Tz (step ) Tj 1.380556 0 Td 37.268519 Tz (is ) Tj 0.622222 0 Td 56.532922 Tz (performed ) Tj 3.208333 0 Td 45.37037 Tz (after ) Tj 1.536111 0 Td 48.611111 Tz (the ) Tj 1.011111 0 Td 49.826389 Tz (addition ) Tj 2.586111 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 46.990741 Tz (catalyst ) Tj 2.411111 0 Td 46.990741 Tz (to ) Tj 51.428571 0 0 51.428571 0 960.620506 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 56.944444 Tz (aqueous ) Tj 2.761111 0 Td 46.090535 Tz (solution. ) Tj 2.897222 0 Td 46.990741 Tz (In ) Tj 0.894444 0 Td 58.333333 Tz (a ) Tj 0.719444 0 Td 46.296296 Tz (certain ) Tj 2.333333 0 Td 44.074074 Tz (situation, ) Tj 2.994444 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 56.944444 Tz (aqueous ) Tj 51.428571 0 0 51.428571 0 918.667954 Tm 6.280556 0 Td 47.800926 Tz (solution ) Tj 2.547222 0 Td 46.018519 Tz (after ) Tj 1.594444 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 49.826389 Tz (addition ) Tj 2.644444 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 46.990741 Tz (catalyst ) Tj 2.469444 0 Td 52.932099 Tz (has ) Tj 1.186111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 74.537037 Tz (pH ) Tj 1.147222 0 Td 51.851852 Tz (value ) Tj 1.75 0 Td 46.990741 Tz (at ) Tj 40 0 0 40 0 883 Tm 8.05 0 Td 70 Tz (about ) Tj 2.4 0 Td 54.166667 Tz (7. ) Tj 51.428571 0 0 51.428571 0 834.15601 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.758333 0 Td 53.240741 Tz (another ) Tj 2.430556 0 Td 47.170782 Tz (instance, ) Tj 2.741667 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 52.314815 Tz (process ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 52.932099 Tz (the ) Tj 1.147222 0 Td 50.05144 Tz (invention ) Tj 2.936111 0 Td 50.231481 Tz (includes ) Tj 51.428571 0 0 51.428571 0 796.44335 Tm 6.261111 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 50.231481 Tz (photolysis ) Tj 3.188889 0 Td 48.611111 Tz (step ) Tj 1.361111 0 Td 58.333333 Tz (on ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 56.018519 Tz (aqueous ) Tj 2.566667 0 Td 48.206019 Tz (solution ) Tj 2.469444 0 Td 46.666667 Tz (after ) Tj 1.536111 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 46.585648 Tz (catalyst ) Tj 2.391667 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 752.629442 Tm 6.261111 0 Td 52.391975 Tz (added. ) Tj 2.216667 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 57.253086 Tz (one ) Tj 1.302778 0 Td 55.092593 Tz (example, ) Tj 2.877778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 56.944444 Tz (aqueous ) Tj 2.683333 0 Td 48.206019 Tz (solution ) Tj 2.547222 0 Td 49.421296 Tz (also ) Tj 1.477778 0 Td 49.826389 Tz (contains ) Tj 51.428571 0 0 51.428571 0 710.991747 Tm 6.261111 0 Td 50.231481 Tz (ascorbic ) Tj 2.780556 0 Td 46.018519 Tz (acid. ) Tj 1.827778 0 Td 46.990741 Tz (In ) Tj 0.913889 0 Td 53.240741 Tz (another ) Tj 2.586111 0 Td 54.6875 Tz (example, ) Tj 3.033333 0 Td 48.611111 Tz (the ) Tj 1.244444 0 Td 74.537037 Tz (pH ) Tj 1.302778 0 Td 51.203704 Tz (value ) Tj 1.905556 0 Td 59.953704 Tz (of ) Tj 0.991667 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 669.257534 Tm 6.261111 0 Td 56.481481 Tz (aqueous ) Tj 2.683333 0 Td 48.206019 Tz (Solution ) Tj 2.605556 0 Td 38.888889 Tz (is ) Tj 0.738889 0 Td 51.311728 Tz (within ) Tj 2.138889 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 54.444444 Tz (range ) Tj 1.886111 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 53.796296 Tz (about ) Tj 1.886111 0 Td 58.333333 Tz (3 ) Tj 0.602778 0 Td 48.611111 Tz (to ) Tj 0.875 0 Td 42.12963 Tz (6. ) Tj 0.836111 0 Td 46.990741 Tz (In ) Tj 0.855556 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 630.311688 Tm 6.280556 0 Td 45.775463 Tz (specific ) Tj 2.488889 0 Td 54.6875 Tz (example, ) Tj 2.897222 0 Td 51.851852 Tz (the ) Tj 1.205556 0 Td 72.916667 Tz (pH ) Tj 1.186111 0 Td 51.203704 Tz (value ) Tj 1.827778 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 56.481481 Tz (aqueous ) Tj 2.663889 0 Td 48.611111 Tz (solution ) Tj 2.625 0 Td 40.509259 Tz (is ) Tj 40 0 0 40 0 592 Tm 8.05 0 Td 70 Tz (about ) Tj 2.375 0 Td 56.25 Tz (4. ) Tj 51.428571 0 0 51.428571 0 544.323567 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 47.314815 Tz (particular ) Tj 2.994444 0 Td 57.744108 Tz (embodiment, ) Tj 3.986111 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 50.411523 Tz (invention ) Tj 2.936111 0 Td 44.907407 Tz (relates ) Tj 2.061111 0 Td 48.611111 Tz (to ) Tj 0.777778 0 Td 53.148148 Tz (using ) Tj 51.428571 0 0 51.428571 0 508.014354 Tm 6.475 0 Td 66.759259 Tz (Co\(DPA-Bpy\)\(OH\) ) Tj 6.280556 0 Td 66.759259 Tz (\(PF\), ) Tj 2.702778 0 Td 68.703704 Tz (Ni\(DPA-Bpy\)\(OH\)\(BF\), ) Tj 51.428571 0 0 51.428571 0 466.690504 Tm 6.475 0 Td 69.753086 Tz (Ni\(DPA-ABpy\)\(OH\)\(BF\), ) Tj 9.1 0 Td 53.472222 Tz (or ) Tj 0.972222 0 Td 66.255144 Tz ([Co\(DPA-ABpy\)\(PF\), ) Tj 51.428571 0 0 51.428571 0 423.807107 Tm 6.261111 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 46.585648 Tz (catalyst ) Tj 2.469444 0 Td 48.611111 Tz (for ) Tj 1.088889 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 56.712963 Tz (hydrogen ) Tj 2.975 0 Td 50.378788 Tz (production. ) Tj 3.616667 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 47.314815 Tz (particular ) Tj 51.428571 0 0 51.428571 0 378.918239 Tm 6.261111 0 Td 57.744108 Tz (embodiment, ) Tj 4.102778 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 50.411523 Tz (invention ) Tj 3.033333 0 Td 44.444444 Tz (relates ) Tj 2.177778 0 Td 45.37037 Tz (to ) Tj 0.836111 0 Td 51.851852 Tz (using ) Tj 2.061111 0 Td 61.868687 Tz (Ru\(DIQ-Bpy\) ) Tj 52.857143 0 0 52.857143 0 336.33795 Tm 6.110811 0 Td 51.351351 Tz (\(CI\)Cl. ) Tj 2.232432 0 Td 66.216216 Tz (\(HO\), ) Tj 2.232432 0 Td 28.378378 Tz (s, ) Tj 1.172973 0 Td 60.48321 Tz (Ru\(DIQ-Bpy\) ) Tj 4.559459 0 Td 74.099099 Tz (\(HO\) ) Tj 2.024324 0 Td 64.954955 Tz (\(PF\), ) Tj 2.516216 0 Td 53.603604 Tz (or ) Tj 1.437838 0 Td 67.792793 Tz (Ru ) Tj 51.428571 0 0 51.428571 0 297.749082 Tm 6.280556 0 Td 56.339031 Tz (\(DIQ-Bpy\)\(Cl\) ) Tj 4.666667 0 Td 67.24537 Tz (\(PF\).HO, ) Tj 3.461111 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 46.585648 Tz (catalyst ) Tj 2.469444 0 Td 46.450617 Tz (for ) Tj 1.05 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 58.333333 Tz (hydrogen ) Tj 51.428571 0 0 51.428571 0 259 Tm 6.261111 0 Td 50.084175 Tz (production. ) Tj 51.428571 0 0 51.428571 0 213.629073 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.302778 0 Td 50.05144 Tz (invention ) Tj 2.897222 0 Td 47.685185 Tz (further ) Tj 2.1 0 Td 52.256944 Tz (provides ) Tj 2.683333 0 Td 52.391975 Tz (design ) Tj 2.041667 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 48.971193 Tz (synthesis ) Tj 2.8 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 170.677966 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.886111 0 Td 56.893004 Tz (complexes ) Tj 3.325 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 48.287037 Tz (invention. ) Tj 40 0 0 40 0 2394 Tm 29.325 0 Td 38.333333 Tz (\(III\) ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.677778 0 Td 77.777778 Tz (4 ) Tj 48.571429 0 0 48.571429 0 2915 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 0.844118 0 Td 49.509804 Tz (certain ) Tj 2.264706 0 Td 60.334967 Tz (embodiments, ) Tj 4.508824 0 Td 53.75817 Tz (the ) Tj 1.152941 0 Td 53.75817 Tz (invention ) Tj 3.108824 0 Td 47.54902 Tz (relates ) Tj 2.182353 0 Td 49.754902 Tz (to ) Tj 0.782353 0 Td 61.764706 Tz (a ) Tj 0.576471 0 Td 64.052288 Tz (method ) Tj 51.428571 0 0 51.428571 0 2872.726817 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 51.851852 Tz (preparing ) Tj 3.013889 0 Td 58.333333 Tz (a ) Tj 0.602778 0 Td 52.5 Tz (metal ) Tj 1.827778 0 Td 59.259259 Tz (complex ) Tj 2.761111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 48.935185 Tz (invention, ) Tj 3.15 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 59.953704 Tz (method ) Tj 51.428571 0 0 51.428571 0 2834 Tm 25.2 0 Td 51.851852 Tz (comprising: ) Tj 51.428571 0 0 51.428571 0 2786.359946 Tm 25.977778 0 Td 45.37037 Tz (1\) ) Tj 0.758333 0 Td 56.17284 Tz (adding ) Tj 2.216667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 41.319444 Tz (salt ) Tj 1.225 0 Td 50.231481 Tz (or ) Tj 0.816667 0 Td 36.728395 Tz (its ) Tj 0.875 0 Td 52.777778 Tz (hydrate ) Tj 2.411111 0 Td 51.388889 Tz (thereof ) Tj 2.275 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 49.016204 Tz (solution ) Tj 51.428571 0 0 51.428571 0 2751 Tm 25.2 0 Td 51.203704 Tz (containing ) Tj 3.752778 0 Td 50.771605 Tz (N,N-Bis\(2-pyridinylmethyl\)-2,2'-Bipyridine-6- ) Tj 51.428571 0 0 51.428571 0 2707.037209 Tm 25.2 0 Td 56.983025 Tz (methanamine, ) Tj 4.841667 0 Td 50.07716 Tz (6'-\(\(bis\(pyridin-2-ylmethyl\)amino\)methyl\)- ) Tj 51.428571 0 0 51.428571 0 2667.314286 Tm 25.180556 0 Td 51.944444 Tz (N,N-dimethyl-2,2'-bipyridin-6-amine ) Tj 11.141667 0 Td 59.579772 Tz (\(DPA-ABpy'\), ) Tj 4.880556 0 Td 60.763889 Tz (N,N- ) Tj 51.428571 0 0 51.428571 0 2626 Tm 25.180556 0 Td 49.281609 Tz (bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 2578.186597 Tm 25.2 0 Td 59.511785 Tz (methanamine ) Tj 4.316667 0 Td 56.17284 Tz (\(DIQ-Bpy'\), ) Tj 4.433333 0 Td 53.472222 Tz (or ) Tj 0.972222 0 Td 51.851852 Tz (a ) Tj 0.738889 0 Td 48.287037 Tz (derivative ) Tj 3.305556 0 Td 50.462963 Tz (thereof ) Tj 2.45 0 Td 43.75 Tz (in ) Tj 0.933333 0 Td 55.092593 Tz (a ) Tj 48.571429 0 0 48.571429 0 2537 Tm 26.682353 0 Td 51.470588 Tz (reaction ) Tj 2.738235 0 Td 53.431373 Tz (solvent ) Tj 2.45 0 Td 51.470588 Tz (to ) Tj 0.885294 0 Td 53.186275 Tz (obtain ) Tj 2.161765 0 Td 61.764706 Tz (a ) Tj 0.658824 0 Td 52.757353 Tz (mixture; ) Tj 2.820588 0 Td 64.052288 Tz (and ) Tj 51.428571 0 0 51.428571 0 2498.431847 Tm 25.919444 0 Td 51.851852 Tz (2\) ) Tj 0.816667 0 Td 53.06713 Tz (allowing ) Tj 2.761111 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 43.75 Tz (to ) Tj 0.719444 0 Td 60.648148 Tz (complex ) Tj 2.761111 0 Td 52.662037 Tz (with ) Tj 1.477778 0 Td 54.890046 Tz (N,N-Bis\(2-pyridi ) Tj 51.428571 0 0 51.428571 0 2460 Tm 25.2 0 Td 51.930894 Tz (nylmethyl\)-2,2'-Bipyridine-6-methanamine, ) Tj 13.786111 0 Td 47.115385 Tz (6'-\(\(bis\(pyri ) Tj 51.428571 0 0 51.428571 0 2418 Tm 25.2 0 Td 52.585604 Tz (din-2-ylmethyl\)amino\)methyl\)-N,N-dimethyl-2,2'-bipyri ) Tj 51.428571 0 0 51.428571 0 2374.96483 Tm 25.2 0 Td 53.914141 Tz (din-6-amine ) Tj 3.869444 0 Td 59.579772 Tz (\(DPA-ABpy'\), ) Tj 4.938889 0 Td 55.092593 Tz (or ) Tj 0.933333 0 Td 51.462963 Tz (N,N-bis\(isoquinolin-1-yl\) ) Tj 51.428571 0 0 51.428571 0 2334.012687 Tm 25.2 0 Td 51.311728 Tz (methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 15.380556 0 Td 69.351852 Tz (\(DIQ ) Tj 51.428571 0 0 51.428571 0 2288.305211 Tm 25.219444 0 Td 53.472222 Tz (Bpy'\), ) Tj 2.119444 0 Td 51.851852 Tz (or ) Tj 0.797222 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 48.611111 Tz (derivative ) Tj 3.130556 0 Td 45.775463 Tz (thereof, ) Tj 2.391667 0 Td 40.833333 Tz (e.g., ) Tj 1.419444 0 Td 59.953704 Tz (by ) Tj 0.952778 0 Td 48.251029 Tz (refluxing ) Tj 2.8 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 53.240741 Tz (mixture ) Tj 51.428571 0 0 51.428571 0 2247.569231 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 46.990741 Tz (step ) Tj 1.438889 0 Td 38.888889 Tz (1\). ) Tj 51.428571 0 0 51.428571 0 2206.067797 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.855556 0 Td 52.777778 Tz (another ) Tj 2.430556 0 Td 47.685185 Tz (aspect, ) Tj 2.275 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 50.411523 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.761111 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 64.00463 Tz (compound ) Tj 51.428571 0 0 51.428571 0 2169 Tm 25.2 0 Td 50.259909 Tz (N,N-bis\(\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin ) Tj 51.428571 0 0 51.428571 0 2122.805042 Tm 25.2 0 Td 53.948802 Tz (2-yl\)methanamine, ) Tj 5.755556 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 48.287037 Tz (derivative ) Tj 3.15 0 Td 45.775463 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 2081.64557 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.738889 0 Td 53.240741 Tz (another ) Tj 2.352778 0 Td 47.685185 Tz (aspect, ) Tj 2.197222 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 50.411523 Tz (invention ) Tj 2.897222 0 Td 52.256944 Tz (provides ) Tj 2.663889 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 52.5 Tz (metal ) Tj 1.788889 0 Td 59.259259 Tz (complex ) Tj 51.428571 0 0 51.428571 0 2044 Tm 25.2 0 Td 55.092593 Tz (comprising ) Tj 3.441667 0 Td 50.795089 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2- ) Tj 51.428571 0 0 51.428571 0 1998.252427 Tm 25.180556 0 Td 52.572016 Tz (yl\)pyridin-2-yl\)methanamine ) Tj 8.769444 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 48.611111 Tz (derivative ) Tj 3.15 0 Td 46.585648 Tz (thereof, ) Tj 2.527778 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 1954.260809 Tm 25.180556 0 Td 46.342593 Tz (transition ) Tj 3.033333 0 Td 49.151235 Tz (metal; ) Tj 2.061111 0 Td 50.231481 Tz (or ) Tj 0.816667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 39.537037 Tz (salt, ) Tj 1.458333 0 Td 46.180556 Tz (Solvate, ) Tj 2.469444 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 52.314815 Tz (hydrate ) Tj 2.430556 0 Td 46.180556 Tz (thereof. ) Tj 48.571429 0 0 48.571429 0 1913 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 0.761765 0 Td 50 Tz (certain ) Tj 2.264706 0 Td 60.334967 Tz (embodiments, ) Tj 4.529412 0 Td 51.470588 Tz (the ) Tj 1.111765 0 Td 47.696078 Tz (transition ) Tj 3.088235 0 Td 54.901961 Tz (metal ) Tj 1.811765 0 Td 42.892157 Tz (is ) Tj 0.658824 0 Td 61.764706 Tz (Co, ) Tj 1.317647 0 Td 57.189542 Tz (Ru, ) Tj 1.173529 0 Td 53.75817 Tz (Ni, ) Tj 51.428571 0 0 51.428571 0 1871.331613 Tm 25.2 0 Td 53.472222 Tz (or ) Tj 0.913889 0 Td 48.611111 Tz (Fe. ) Tj 1.225 0 Td 46.990741 Tz (In ) Tj 0.855556 0 Td 47.222222 Tz (certain ) Tj 2.294444 0 Td 56.983025 Tz (embodiments, ) Tj 4.433333 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 59.722222 Tz (complex ) Tj 2.819444 0 Td 47.685185 Tz (further ) Tj 2.255556 0 Td 84.259259 Tz (com ) Tj 51.428571 0 0 51.428571 0 1828.901408 Tm 25.2 0 Td 47.530864 Tz (prises ) Tj 1.847222 0 Td 56.712963 Tz (an ) Tj 0.855556 0 Td 49.151235 Tz (anion. ) Tj 1.983333 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 46.759259 Tz (certain ) Tj 2.119444 0 Td 56.983025 Tz (embodiments, ) Tj 4.277778 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 53.796296 Tz (anion ) Tj 1.769444 0 Td 40.509259 Tz (is ) Tj 0.7 0 Td 63.194444 Tz (PF ) Tj 1.536111 0 Td 51.851852 Tz (or ) Tj 52.857143 0 0 52.857143 0 1787.357895 Tm 24.518919 0 Td 89.339339 Tz (BF. ) Tj 1.986486 0 Td 45.720721 Tz (In ) Tj 0.87027 0 Td 46.396396 Tz (certain ) Tj 2.27027 0 Td 55.18018 Tz (embodiments, ) Tj 4.332432 0 Td 47.297297 Tz (the ) Tj 1.172973 0 Td 58.108108 Tz (complex ) Tj 2.781081 0 Td 39.414414 Tz (is ) Tj 1.040541 0 Td 70.42042 Tz (Ru\(DIQ ) Tj 51.428571 0 0 51.428571 0 1749.843049 Tm 25.2 0 Td 54.6875 Tz (Bpy\)\(Cl\) ) Tj 2.897222 0 Td 57.037037 Tz (\(PF\). ) Tj 51.428571 0 0 51.428571 0 1704.192201 Tm 25.919444 0 Td 56.388889 Tz (Other ) Tj 2.080556 0 Td 49.537037 Tz (aspects ) Tj 2.488889 0 Td 58.333333 Tz (and ) Tj 1.477778 0 Td 59.217172 Tz (embodiments ) Tj 4.336111 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 47.530864 Tz (the ) Tj 1.302778 0 Td 50.771605 Tz (invention ) Tj 3.130556 0 Td 50.771605 Tz (are ) Tj 40 0 0 40 0 1670 Tm 32.4 0 Td 66.666667 Tz (described ) Tj 3.9 0 Td 60.119048 Tz (herein. ) Tj 38.571429 0 0 38.571429 0 1590 Tm 36.503704 0 Td 90.740741 Tz (BRIEF ) Tj 3.111111 0 Td 94.276094 Tz (DESCRIPTION ) Tj 6.585185 0 Td 101.54321 Tz (OF ) Tj 1.503704 0 Td 106.584362 Tz (THE ) Tj 2.281481 0 Td 95.061728 Tz (FIGURES ) Tj 51.428571 0 0 51.428571 0 1502.654987 Tm 25.938889 0 Td 55.092593 Tz (FIG. ) Tj 1.711111 0 Td 51.851852 Tz (1 ) Tj 0.719444 0 Td 49.421296 Tz (presents ) Tj 2.761111 0 Td 54.012346 Tz (molecular ) Tj 3.266667 0 Td 47.170782 Tz (structure ) Tj 2.858333 0 Td 61.574074 Tz (of ) Tj 1.186111 0 Td 63.930976 Tz (Co\(DPA-Bpy\) ) Tj 51.428571 0 0 51.428571 0 1458.376655 Tm 25.219444 0 Td 68.554131 Tz (\(Cl\)Cl.\(CHCN\) ) Tj 5.502778 0 Td 53.472222 Tz (with ) Tj 1.477778 0 Td 52.777778 Tz (thermal ) Tj 2.391667 0 Td 46.342593 Tz (ellipsoids ) Tj 2.975 0 Td 60.925926 Tz (drawn ) Tj 1.983333 0 Td 45.37037 Tz (at ) Tj 0.738889 0 Td 47.530864 Tz (the ) Tj 1.069444 0 Td 72.376543 Tz (50% ) Tj 51.428571 0 0 51.428571 0 1420.366255 Tm 25.2 0 Td 48.021886 Tz (probability ) Tj 3.441667 0 Td 43.209877 Tz (level. ) Tj 51.428571 0 0 51.428571 0 1376.532609 Tm 25.938889 0 Td 55.092593 Tz (FIG. ) Tj 1.613889 0 Td 55.092593 Tz (2 ) Tj 0.602778 0 Td 38.888889 Tz (is ) Tj 0.719444 0 Td 52.824074 Tz (UV-visible ) Tj 3.441667 0 Td 48.148148 Tz (spectra ) Tj 2.255556 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 59.722222 Tz (complex ) Tj 2.838889 0 Td 32.407407 Tz (1 ) Tj 0.544444 0 Td 53.703704 Tz (\(dashed ) Tj 2.527778 0 Td 43.425926 Tz (line\) ) Tj 51.428571 0 0 51.428571 0 1334.275711 Tm 25.2 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 60.185185 Tz (complex ) Tj 2.761111 0 Td 58.333333 Tz (2 ) Tj 0.622222 0 Td 45.37037 Tz (\(solid ) Tj 1.905556 0 Td 44.074074 Tz (line\) ) Tj 1.575 0 Td 43.75 Tz (in ) Tj 0.797222 0 Td 61.574074 Tz (H.O. ) Tj 51.428571 0 0 51.428571 0 1294.597884 Tm 25.938889 0 Td 57.037037 Tz (FIGS. ) Tj 1.983333 0 Td 49.259259 Tz (3a-b. ) Tj 1.730556 0 Td 40.833333 Tz (\(3.a\) ) Tj 1.438889 0 Td 57.253086 Tz (UV-vis ) Tj 2.333333 0 Td 48.148148 Tz (spectra ) Tj 2.255556 0 Td 57.79321 Tz (change ) Tj 2.294444 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 58.333333 Tz (2 ) Tj 0.583333 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 1252.304348 Tm 25.2 0 Td 53.240741 Tz (varying ) Tj 2.430556 0 Td 60.493827 Tz (pH; ) Tj 1.361111 0 Td 40.185185 Tz (\(3.b\) ) Tj 1.380556 0 Td 58.009259 Tz (Absorbance ) Tj 3.713889 0 Td 57.253086 Tz (change ) Tj 2.313889 0 Td 50.231481 Tz (vs ) Tj 0.855556 0 Td 74.537037 Tz (pH ) Tj 1.108333 0 Td 45.37037 Tz (at ) Tj 0.777778 0 Td 61.574074 Tz (470 ) Tj 1.322222 0 Td 74.537037 Tz (nm ) Tj 1.127778 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 1209.329897 Tm 25.2 0 Td 59.41358 Tz (478 ) Tj 1.341667 0 Td 72.916667 Tz (nm ) Tj 1.108333 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 42.12963 Tz (2. ) Tj 0.719444 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 42.12963 Tz (best-fit ) Tj 2.216667 0 Td 45.37037 Tz (lines ) Tj 1.594444 0 Td 57.523148 Tz (from ) Tj 1.594444 0 Td 54.282407 Tz (both ) Tj 1.536111 0 Td 61.574074 Tz (470 ) Tj 1.302778 0 Td 77.777778 Tz (nm ) Tj 51.428571 0 0 51.428571 0 1167.422709 Tm 25.219444 0 Td 45.37037 Tz (\(solid ) Tj 1.866667 0 Td 44.722222 Tz (line\) ) Tj 1.555556 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 60.493827 Tz (478 ) Tj 1.361111 0 Td 72.916667 Tz (nm ) Tj 1.147222 0 Td 53.703704 Tz (\(dashed ) Tj 2.508333 0 Td 44.074074 Tz (line\) ) Tj 1.555556 0 Td 47.962963 Tz (yield ) Tj 1.672222 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 60.493827 Tz (pKa ) Tj 1.419444 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 43.75 Tz (5.0. ) Tj 51.428571 0 0 51.428571 0 1126.745214 Tm 25.938889 0 Td 55.092593 Tz (FIG. ) Tj 1.633333 0 Td 61.574074 Tz (4 ) Tj 0.641667 0 Td 38.888889 Tz (is ) Tj 0.816667 0 Td 72.376543 Tz (EPR ) Tj 1.594444 0 Td 48.148148 Tz (spectra ) Tj 2.352778 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 49.151235 Tz (water: ) Tj 2.1 0 Td 44.290123 Tz (\(a\) ) Tj 1.069444 0 Td 59.722222 Tz (complex ) Tj 2.877778 0 Td 35.648148 Tz (1 ) Tj 0.563889 0 Td 58.333333 Tz (and ) Tj 1.361111 0 Td 46.450617 Tz (\(b\) ) Tj 51.428571 0 0 51.428571 0 1087.235294 Tm 25.2 0 Td 59.259259 Tz (complex ) Tj 2.955556 0 Td 42.12963 Tz (2. ) Tj 0.952778 0 Td 58.796296 Tz (Samples ) Tj 2.897222 0 Td 59.953704 Tz (were ) Tj 1.847222 0 Td 53.472222 Tz (recorded ) Tj 3.013889 0 Td 43.75 Tz (in ) Tj 0.991667 0 Td 55.092593 Tz (2 ) Tj 0.816667 0 Td 97.222222 Tz (mM ) Tj 1.594444 0 Td 56.944444 Tz (aqueous ) Tj 51.428571 0 0 51.428571 0 1043.88946 Tm 25.219444 0 Td 47.800926 Tz (solution ) Tj 2.508333 0 Td 51.527778 Tz (containing ) Tj 3.363889 0 Td 68.055556 Tz (10% ) Tj 1.458333 0 Td 49.421296 Tz (glycerol ) Tj 2.566667 0 Td 45.37037 Tz (at ) Tj 0.797222 0 Td 51.851852 Tz (15 ) Tj 0.894444 0 Td 84.259259 Tz (K ) Tj 0.680556 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 55.092593 Tz (15 ) Tj 0.875 0 Td 69.675926 Tz (dB ) Tj 1.069444 0 Td 63.518519 Tz (micro ) Tj 51.428571 0 0 51.428571 0 1003.104478 Tm 25.180556 0 Td 64.814815 Tz (wave ) Tj 1.788889 0 Td 55.632716 Tz (power; ) Tj 2.294444 0 Td 59.41358 Tz (microwave ) Tj 3.441667 0 Td 50.87963 Tz (frequency, ) Tj 3.286111 0 Td 55.740741 Tz (9.050 ) Tj 1.886111 0 Td 64.00463 Tz (GHz. ) Tj 51.428571 0 0 51.428571 0 962.835742 Tm 25.938889 0 Td 57.037037 Tz (FIGS. ) Tj 1.983333 0 Td 54.282407 Tz (5a-c ) Tj 1.516667 0 Td 49.691358 Tz (are ) Tj 1.127778 0 Td 48.070988 Tz (cyclic ) Tj 1.983333 0 Td 60.078348 Tz (voltammograms ) Tj 4.958333 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 44.290123 Tz (\(a\) ) Tj 0.991667 0 Td 60.185185 Tz (complex ) Tj 2.819444 0 Td 38.888889 Tz (1, ) Tj 51.428571 0 0 51.428571 0 922.273684 Tm 25.219444 0 Td 46.450617 Tz (\(b\) ) Tj 1.069444 0 Td 60.185185 Tz (complex ) Tj 2.838889 0 Td 38.888889 Tz (1 ) Tj 0.583333 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 45.37037 Tz (\(c\) ) Tj 1.088889 0 Td 67.12963 Tz (DPA-Bpy ) Tj 3.111111 0 Td 50.771605 Tz (ligand ) Tj 2.080556 0 Td 42.12963 Tz (in ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 53.472222 Tz (presence ) Tj 2.819444 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 875 Tm 25.2 0 Td 50.771605 Tz (ferrocene ) Tj 2.975 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 94.791667 Tz (CHCN ) Tj 2.547222 0 Td 45.730453 Tz (solution, ) Tj 2.722222 0 Td 45.37037 Tz (0.1 ) Tj 1.166667 0 Td 76.697531 Tz (MTBAP. ) Tj 3.013889 0 Td 59.143519 Tz (Scan ) Tj 1.652778 0 Td 42.12963 Tz (rate, ) Tj 1.555556 0 Td 57.253086 Tz (100 ) Tj 51.428571 0 0 51.428571 0 835.219355 Tm 25.2 0 Td 58.333333 Tz (mV/s; ) Tj 2.177778 0 Td 56.944444 Tz (working ) Tj 2.761111 0 Td 47.962963 Tz (electrode, ) Tj 3.266667 0 Td 49.691358 Tz (glassy ) Tj 2.197222 0 Td 51.388889 Tz (carbon; ) Tj 2.566667 0 Td 50.05144 Tz (reference ) Tj 3.091667 0 Td 58.333333 Tz (elec ) Tj 51.428571 0 0 51.428571 0 793.480355 Tm 25.180556 0 Td 46.990741 Tz (trode, ) Tj 1.963889 0 Td 59.143519 Tz (Ag/AgCl; ) Tj 3.15 0 Td 52.777778 Tz (counter ) Tj 2.469444 0 Td 47.638889 Tz (electrode, ) Tj 3.208333 0 Td 48.611111 Tz (Pt ) Tj 0.855556 0 Td 48.611111 Tz (wire. ) Tj 1.827778 0 Td 53.292181 Tz (Ferrocene ) Tj 3.188889 0 Td 45.37037 Tz (\(*\) ) Tj 51.428571 0 0 51.428571 0 750 Tm 25.180556 0 Td 63.734568 Tz (was ) Tj 1.4 0 Td 52.256944 Tz (included ) Tj 2.741667 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 45.775463 Tz (internal ) Tj 2.488889 0 Td 49.691358 Tz (reference ) Tj 2.916667 0 Td 49.907407 Tz (\(0.64 ) Tj 1.75 0 Td 81.018519 Tz (V ) Tj 0.758333 0 Td 51.851852 Tz (vs ) Tj 0.894444 0 Td 58.333333 Tz (SHE\). ) Tj 58.571429 0 0 58.571429 0 713.180263 Tm 22.758537 0 Td 49.796748 Tz (FIG. ) Tj 1.365854 0 Td 54.065041 Tz (6 ) Tj 0.495122 0 Td 34.146341 Tz (is ) Tj 0.580488 0 Td 51.219512 Tz (a ) Tj 0.478049 0 Td 46.95122 Tz (pourbaix ) Tj 2.458537 0 Td 48.780488 Tz (diagram ) Tj 2.253659 0 Td 42.682927 Tz (for ) Tj 0.921951 0 Td 42.682927 Tz (the ) Tj 0.921951 0 Td 94.850949 Tz (Co' ) Tj 1.895122 0 Td 48.943089 Tz (redox ) Tj 1.621951 0 Td 47.899729 Tz (couple ) Tj 51.428571 0 0 51.428571 0 669.688086 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 59.722222 Tz (complex ) Tj 2.8 0 Td 55.092593 Tz (2 ) Tj 0.622222 0 Td 43.75 Tz (in ) Tj 0.816667 0 Td 56.481481 Tz (aqueous ) Tj 2.722222 0 Td 52.256944 Tz (Britton-Robinson ) Tj 5.288889 0 Td 49.151235 Tz (buffer ) Tj 2.022222 0 Td 58.333333 Tz (\(E ) Tj 1.711111 0 Td 50.231481 Tz (vs ) Tj 51.428571 0 0 51.428571 0 626 Tm 25.219444 0 Td 58.333333 Tz (SHE\). ) Tj 51.428571 0 0 51.428571 0 587.842795 Tm 25.938889 0 Td 55.092593 Tz (FIG. ) Tj 1.788889 0 Td 58.333333 Tz (7 ) Tj 0.758333 0 Td 49.691358 Tz (are ) Tj 1.302778 0 Td 48.070988 Tz (cyclic ) Tj 2.197222 0 Td 60.078348 Tz (voltammograms ) Tj 5.113889 0 Td 59.953704 Tz (of ) Tj 1.088889 0 Td 48.611111 Tz (1.0 ) Tj 1.263889 0 Td 110.185185 Tz (M ) Tj 1.088889 0 Td 58.873457 Tz (sodium ) Tj 51.428571 0 0 51.428571 0 545.415265 Tm 25.2 0 Td 54.73251 Tz (phosphate ) Tj 3.227778 0 Td 48.070988 Tz (buffer ) Tj 2.022222 0 Td 48.206019 Tz (solution ) Tj 2.566667 0 Td 46.990741 Tz (at ) Tj 0.797222 0 Td 76.157407 Tz (pH ) Tj 1.205556 0 Td 50.771605 Tz (7.0 ) Tj 1.166667 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 53.06713 Tz (presence ) Tj 2.838889 0 Td 45.910494 Tz (\(solid ) Tj 51.428571 0 0 51.428571 0 502.361257 Tm 25.2 0 Td 44.074074 Tz (line\) ) Tj 1.594444 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 55.092593 Tz (absence ) Tj 2.586111 0 Td 49.074074 Tz (\(dotted ) Tj 2.313889 0 Td 43.425926 Tz (line\) ) Tj 1.575 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 63.194444 Tz (50 ) Tj 1.05 0 Td 77.777778 Tz (uM ) Tj 1.186111 0 Td 60.185185 Tz (complex ) Tj 2.8 0 Td 40.509259 Tz (2. ) Tj 0.797222 0 Td 59.143519 Tz (Scan ) Tj 51.428571 0 0 51.428571 0 462.279188 Tm 25.2 0 Td 42.12963 Tz (rate, ) Tj 1.633333 0 Td 57.253086 Tz (100 ) Tj 1.302778 0 Td 57.037037 Tz (mV/s; ) Tj 2.041667 0 Td 57.87037 Tz (working ) Tj 2.702778 0 Td 46.990741 Tz (electrode, ) Tj 3.15 0 Td 56.944444 Tz (mercury ) Tj 2.683333 0 Td 48.611111 Tz (pool; ) Tj 1.769444 0 Td 52.777778 Tz (counter ) Tj 51.428571 0 0 51.428571 0 420.617647 Tm 25.2 0 Td 47.314815 Tz (electrode, ) Tj 3.111111 0 Td 50.231481 Tz (Pt ) Tj 0.875 0 Td 55.092593 Tz (mesh; ) Tj 1.925 0 Td 50.411523 Tz (reference ) Tj 2.936111 0 Td 47.638889 Tz (electrode, ) Tj 3.091667 0 Td 56.944444 Tz (aqueous ) Tj 2.625 0 Td 58.333333 Tz (Ag/AgCl. ) Tj 51.428571 0 0 51.428571 0 379.747368 Tm 25.938889 0 Td 57.037037 Tz (FIGS. ) Tj 1.983333 0 Td 56.712963 Tz (8a-b ) Tj 1.594444 0 Td 50.771605 Tz (are ) Tj 1.166667 0 Td 48.070988 Tz (charts ) Tj 1.983333 0 Td 59.259259 Tz (showing ) Tj 2.702778 0 Td 54.552469 Tz (charge ) Tj 2.197222 0 Td 51.446759 Tz (build-up ) Tj 2.722222 0 Td 55.902778 Tz (over ) Tj 1.575 0 Td 44.290123 Tz (\(a\) ) Tj 51.428571 0 0 51.428571 0 338.129608 Tm 25.180556 0 Td 55.092593 Tz (time ) Tj 1.477778 0 Td 55.632716 Tz (\(200s\) ) Tj 2.119444 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 46.450617 Tz (\(b\) ) Tj 0.952778 0 Td 49.358974 Tz (overpotential ) Tj 4.005556 0 Td 48.611111 Tz (for ) Tj 1.011111 0 Td 49.691358 Tz (the ) Tj 1.011111 0 Td 49.259259 Tz (controlled ) Tj 3.111111 0 Td 47.170782 Tz (potential ) Tj 51.428571 0 0 51.428571 0 297.485149 Tm 25.2 0 Td 45.910494 Tz (electrolysis ) Tj 3.461111 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 63.194444 Tz (50 ) Tj 0.952778 0 Td 79.398148 Tz (uM ) Tj 1.108333 0 Td 60.185185 Tz (complex ) Tj 2.722222 0 Td 55.092593 Tz (2 ) Tj 0.544444 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 48.611111 Tz (1.0 ) Tj 1.011111 0 Td 106.944444 Tz (M ) Tj 0.836111 0 Td 58.333333 Tz (sodium ) Tj 2.275 0 Td 55.092593 Tz (phosphate ) Tj 51.428571 0 0 51.428571 0 252.709091 Tm 25.180556 0 Td 49.151235 Tz (buffer ) Tj 1.963889 0 Td 45.37037 Tz (at ) Tj 0.777778 0 Td 76.157407 Tz (pH ) Tj 1.166667 0 Td 43.75 Tz (7.0. ) Tj 51.428571 0 0 51.428571 0 212.513089 Tm 25.938889 0 Td 57.037037 Tz (FIGS. ) Tj 1.983333 0 Td 51.203704 Tz (9a-b. ) Tj 1.827778 0 Td 50 Tz (present ) Tj 2.430556 0 Td 43.981481 Tz (results ) Tj 2.119444 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 49.259259 Tz (controlled ) Tj 3.208333 0 Td 47.530864 Tz (potential ) Tj 2.819444 0 Td 59.953704 Tz (elec ) Tj 51.428571 0 0 51.428571 0 170.541667 Tm 25.180556 0 Td 44.965278 Tz (trolysis ) Tj 2.391667 0 Td 43.75 Tz (at ) Tj 0.738889 0 Td 54.282407 Tz (-1.4 ) Tj 1.536111 0 Td 84.259259 Tz (V ) Tj 0.738889 0 Td 48.611111 Tz (\(vs ) Tj 1.108333 0 Td 58.981481 Tz (SHE\). ) Tj 2.002778 0 Td 46.450617 Tz (\(a\) ) Tj 1.069444 0 Td 46.990741 Tz (In ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 53.877315 Tz (presence ) Tj 2.819444 0 Td 44.830247 Tz (\(solid ) Tj 1.886111 0 Td 43.425926 Tz (line\) ) Tj ET Q endstream endobj 266 0 obj << /Length 1 >> stream q endstream endobj 267 0 obj << /Length 46690 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 51.428571 0 0 51.428571 0 2968 Tm 14.777778 0 Td 74.537037 Tz (5 ) Tj 51.428571 0 0 51.428571 0 2915.573217 Tm 6.261111 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 55.555556 Tz (absence ) Tj 2.527778 0 Td 49.074074 Tz (\(dotted ) Tj 2.275 0 Td 44.074074 Tz (line\) ) Tj 1.516667 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 61.574074 Tz (50 ) Tj 0.972222 0 Td 81.018519 Tz (uM ) Tj 1.166667 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 43.75 Tz (2; ) Tj 0.777778 0 Td 45.37037 Tz (\(b\) ) Tj 1.011111 0 Td 46.090535 Tz (Stability ) Tj 51.428571 0 0 51.428571 0 2872.90815 Tm 6.241667 0 Td 43.75 Tz (test ) Tj 1.225 0 Td 61.574074 Tz (of ) Tj 0.855556 0 Td 59.953704 Tz (50 ) Tj 1.127778 0 Td 66.435185 Tz (LM ) Tj 1.011111 0 Td 59.259259 Tz (complex ) Tj 2.702778 0 Td 58.333333 Tz (2 ) Tj 0.602778 0 Td 43.75 Tz (in ) Tj 0.797222 0 Td 48.611111 Tz (1.0 ) Tj 1.088889 0 Td 103.703704 Tz (M ) Tj 0.836111 0 Td 58.873457 Tz (sodium ) Tj 2.333333 0 Td 55.092593 Tz (phosphate ) Tj 3.169444 0 Td 49.151235 Tz (buffer ) Tj 51.428571 0 0 51.428571 0 2829.564165 Tm 6.280556 0 Td 48.206019 Tz (Solution ) Tj 2.488889 0 Td 42.12963 Tz (at ) Tj 0.680556 0 Td 72.916667 Tz (pH ) Tj 1.05 0 Td 43.75 Tz (7.0. ) Tj 1.225 0 Td 57.87037 Tz (working ) Tj 2.586111 0 Td 47.314815 Tz (electrode, ) Tj 3.052778 0 Td 56.018519 Tz (mercury ) Tj 2.508333 0 Td 49.907407 Tz (pool; ) Tj 1.691667 0 Td 52.314815 Tz (counter ) Tj 51.428571 0 0 51.428571 0 2786.620859 Tm 6.261111 0 Td 47.314815 Tz (electrode, ) Tj 3.111111 0 Td 50.231481 Tz (Pt ) Tj 0.875 0 Td 55.092593 Tz (mesh; ) Tj 1.944444 0 Td 50.05144 Tz (reference ) Tj 2.916667 0 Td 47.638889 Tz (electrode, ) Tj 3.091667 0 Td 56.944444 Tz (aqueous ) Tj 2.625 0 Td 58.333333 Tz (Ag/AgCl. ) Tj 52.857143 0 0 52.857143 0 2745.51195 Tm 6.810811 0 Td 56.756757 Tz (FIGS. ) Tj 1.948649 0 Td 53.603604 Tz (10a-b ) Tj 1.816216 0 Td 48.348348 Tz (are ) Tj 1.078378 0 Td 73.048048 Tz (GC-TCD ) Tj 2.837838 0 Td 56.271656 Tz (chromatograms ) Tj 4.597297 0 Td 56.756757 Tz (of ) Tj 0.832432 0 Td 59.90991 Tz (H, ) Tj 0.945946 0 Td 52.702703 Tz (produc- ) Tj 2.8 0 Td 37.837838 Tz (5 ) Tj 51.428571 0 0 51.428571 0 2701.53973 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.536111 0 Td 55.902778 Tz (over ) Tj 1.730556 0 Td 48.611111 Tz (time: ) Tj 1.905556 0 Td 45.37037 Tz (\(a\) ) Tj 1.244444 0 Td 46.990741 Tz (In ) Tj 1.069444 0 Td 47.530864 Tz (1.0 ) Tj 1.244444 0 Td 103.703704 Tz (M ) Tj 1.030556 0 Td 49.074074 Tz (acetate ) Tj 2.45 0 Td 48.611111 Tz (buffer ) Tj 2.119444 0 Td 45.37037 Tz (at ) Tj 0.952778 0 Td 72.916667 Tz (pH ) Tj 1.283333 0 Td 51.851852 Tz (4.0 ) Tj 58.571429 0 0 58.571429 0 2664.217553 Tm 5.497561 0 Td 44.674797 Tz (containing ) Tj 2.85122 0 Td 52.439024 Tz (complex ) Tj 2.339024 0 Td 51.219512 Tz (2 ) Tj 0.478049 0 Td 41.260163 Tz (\(5.0 ) Tj 1.178049 0 Td 49.796748 Tz (uM\), ) Tj 1.553659 0 Td 65.091463 Tz (Ru\(bpy\)* ) Tj 3.295122 0 Td 40.54878 Tz (\(0.5 ) Tj 1.178049 0 Td 57.621951 Tz (mM\), ) Tj 1.536585 0 Td 53.116531 Tz (and ) Tj 51.428571 0 0 51.428571 0 2618.87395 Tm 6.261111 0 Td 50.231481 Tz (ascorbic ) Tj 2.780556 0 Td 51.851852 Tz (acid ) Tj 1.613889 0 Td 43.75 Tz (\(0.1 ) Tj 1.536111 0 Td 57.253086 Tz (M\). ) Tj 1.458333 0 Td 78.858025 Tz (LED ) Tj 1.769444 0 Td 42.12963 Tz (light, ) Tj 1.905556 0 Td 61.574074 Tz (450 ) Tj 1.497222 0 Td 58.333333 Tz (nm. ) Tj 1.477778 0 Td 46.450617 Tz (\(b\) ) Tj 1.205556 0 Td 52.777778 Tz (Control ) Tj 51.428571 0 0 51.428571 0 2578.84225 Tm 6.261111 0 Td 53.619529 Tz (experiments ) Tj 3.966667 0 Td 43.75 Tz (in ) Tj 0.913889 0 Td 50.771605 Tz (the ) Tj 1.283333 0 Td 55.555556 Tz (absence ) Tj 2.702778 0 Td 58.333333 Tz (of ) Tj 0.991667 0 Td 50.636574 Tz (ascorbic ) Tj 2.819444 0 Td 46.666667 Tz (acid, ) Tj 1.808333 0 Td 41.589506 Tz (light, ) Tj 2.158333 0 Td 69.675926 Tz (Ru ) Tj 51.714286 0 0 51.714286 0 2542.002681 Tm 6.245856 0 Td 59.219613 Tz (\(bpy\)'', ) Tj 3.055249 0 Td 53.176796 Tz (or ) Tj 0.850829 0 Td 63.996317 Tz (Complex ) Tj 2.900552 0 Td 43.508287 Tz (2. ) Tj 11.022099 0 Td 43.508287 Tz (10 ) Tj 51.428571 0 0 51.428571 0 2496.581457 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 53.472222 Tz (11 ) Tj 0.894444 0 Td 37.268519 Tz (is ) Tj 0.641667 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 49.907407 Tz (chart ) Tj 1.691667 0 Td 58.333333 Tz (showing ) Tj 2.644444 0 Td 49.074074 Tz (photocatalytic ) Tj 4.336111 0 Td 50.231481 Tz (H. ) Tj 0.972222 0 Td 51.131687 Tz (evolution ) Tj 2.955556 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 2452.456865 Tm 6.261111 0 Td 50.925926 Tz (various ) Tj 2.275 0 Td 76.157407 Tz (pH ) Tj 1.108333 0 Td 46.759259 Tz (values. ) Tj 2.119444 0 Td 51.557239 Tz (Conditions: ) Tj 3.636111 0 Td 56.712963 Tz (10 ) Tj 0.855556 0 Td 81.018519 Tz (mL ) Tj 1.166667 0 Td 48.611111 Tz (1.0 ) Tj 0.991667 0 Td 106.944444 Tz (M ) Tj 0.777778 0 Td 49.691358 Tz (buffer ) Tj 1.905556 0 Td 48.611111 Tz (solutions ) Tj 58.571429 0 0 58.571429 0 2411.639676 Tm 5.480488 0 Td 47.662602 Tz (with ) Tj 1.570732 0 Td 44.817073 Tz (ascorbic ) Tj 2.407317 0 Td 49.441057 Tz (acid-0.1 ) Tj 2.680488 0 Td 58.333333 Tz (M, ) Tj 1.195122 0 Td 48.018293 Tz (Ru\(bpy\), ) Tj 2.817073 0 Td 47.804878 Tz ("-0.5 ) Tj 1.690244 0 Td 66.395664 Tz (mM, ) Tj 1.639024 0 Td 74.932249 Tz (com ) Tj 51.428571 0 0 51.428571 0 2371.36853 Tm 6.241667 0 Td 53.472222 Tz (plex ) Tj 1.497222 0 Td 64.814815 Tz (2=5.0 ) Tj 2.216667 0 Td 62.654321 Tz (uM, ) Tj 1.438889 0 Td 76.697531 Tz (LED ) Tj 1.633333 0 Td 41.589506 Tz (light: ) Tj 1.769444 0 Td 59.41358 Tz (450 ) Tj 1.322222 0 Td 60.493827 Tz (nm. ) Tj 51.428571 0 0 51.428571 0 2330.42132 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 58.333333 Tz (12 ) Tj 0.894444 0 Td 42.12963 Tz (is ) Tj 0.661111 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 49.907407 Tz (chart ) Tj 1.691667 0 Td 58.333333 Tz (showing ) Tj 2.644444 0 Td 48.842593 Tz (photocatalytic ) Tj 4.336111 0 Td 50.231481 Tz (H. ) Tj 0.952778 0 Td 51.131687 Tz (evolution ) Tj 2.955556 0 Td 45.37037 Tz (at ) Tj 0.991667 0 Td 43.75 Tz (15 ) Tj 51.428571 0 0 51.428571 0 2286.274074 Tm 6.261111 0 Td 50.925926 Tz (various ) Tj 2.333333 0 Td 50.854701 Tz (concentration ) Tj 4.2 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 43.75 Tz (2. ) Tj 0.758333 0 Td 51.262626 Tz (Conditions: ) Tj 3.675 0 Td 58.333333 Tz (10 ) Tj 0.913889 0 Td 82.638889 Tz (mL ) Tj 1.244444 0 Td 46.450617 Tz (1.0 ) Tj 51.428571 0 0 51.428571 0 2244.531825 Tm 6.261111 0 Td 106.944444 Tz (M ) Tj 1.011111 0 Td 48.148148 Tz (acetate ) Tj 2.372222 0 Td 48.611111 Tz (buffer ) Tj 2.080556 0 Td 45.37037 Tz (at ) Tj 0.855556 0 Td 76.157407 Tz (pH ) Tj 1.263889 0 Td 45.37037 Tz (4.0, ) Tj 1.672222 0 Td 50.636574 Tz (ascorbic ) Tj 2.8 0 Td 56.30787 Tz (acid-0.1 ) Tj 3.130556 0 Td 68.055556 Tz (M. ) Tj 1.458333 0 Td 69.675926 Tz (Ru ) Tj 58.571429 0 0 58.571429 0 2205.035503 Tm 5.514634 0 Td 44.105691 Tz (\(bpy\), ) Tj 2.1 0 Td 46.666667 Tz ("-0.5 ) Tj 1.639024 0 Td 65.447154 Tz (mM, ) Tj 1.434146 0 Td 68.292683 Tz (LED ) Tj 1.434146 0 Td 36.99187 Tz (light: ) Tj 1.553659 0 Td 54.065041 Tz (450 ) Tj 1.178049 0 Td 53.116531 Tz (nm. ) Tj 52.857143 0 0 52.857143 0 2165.333333 Tm 6.810811 0 Td 53.603604 Tz (FIG. ) Tj 1.551351 0 Td 55.18018 Tz (13 ) Tj 0.908108 0 Td 40.990991 Tz (is ) Tj 0.681081 0 Td 53.603604 Tz (a ) Tj 0.567568 0 Td 47.297297 Tz (chart ) Tj 1.645946 0 Td 57.207207 Tz (showing ) Tj 2.610811 0 Td 47.522523 Tz (photocatalytic ) Tj 4.275676 0 Td 47.297297 Tz (H. ) Tj 0.964865 0 Td 51.711712 Tz (production ) Tj 51.428571 0 0 51.428571 0 2119.453012 Tm 6.261111 0 Td 55.092593 Tz (over ) Tj 1.477778 0 Td 47.314815 Tz (time. ) Tj 1.613889 0 Td 50.968013 Tz (Conditions: ) Tj 3.636111 0 Td 56.712963 Tz (10 ) Tj 0.836111 0 Td 82.638889 Tz (mL ) Tj 1.205556 0 Td 47.530864 Tz (1.0 ) Tj 0.991667 0 Td 106.944444 Tz (M ) Tj 0.777778 0 Td 48.611111 Tz (acetate ) Tj 2.197222 0 Td 48.611111 Tz (buffer ) Tj 1.905556 0 Td 43.75 Tz (at ) Tj 0.661111 0 Td 76.157407 Tz (pH ) Tj 1.069444 0 Td 45.37037 Tz (4.0, ) Tj 1.555556 0 Td 45.37037 Tz (20 ) Tj 58.571429 0 0 58.571429 0 2081.517647 Tm 5.668293 0 Td 45.172764 Tz (ascorbic ) Tj 2.492683 0 Td 50.863821 Tz (acid-0.5 ) Tj 2.8 0 Td 59.756098 Tz (M, ) Tj 1.263415 0 Td 59.756098 Tz (Ru\(bpy\)*-2.0 ) Tj 4.660976 0 Td 65.447154 Tz (mM, ) Tj 1.707317 0 Td 53.658537 Tz (complex ) Tj 51.428571 0 0 51.428571 0 2037.468599 Tm 6.261111 0 Td 64.166667 Tz (2=5.0 ) Tj 2.236111 0 Td 62.654321 Tz (uM, ) Tj 1.4 0 Td 76.697531 Tz (LED ) Tj 1.652778 0 Td 41.049383 Tz (light: ) Tj 1.75 0 Td 59.41358 Tz (450 ) Tj 1.341667 0 Td 59.41358 Tz (nm. ) Tj 51.428571 0 0 51.428571 0 1999.301713 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.594444 0 Td 58.333333 Tz (14 ) Tj 0.913889 0 Td 40.509259 Tz (is ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 48.611111 Tz (chart ) Tj 1.672222 0 Td 58.796296 Tz (showing ) Tj 2.702778 0 Td 48.842593 Tz (photocatalytic ) Tj 4.394444 0 Td 58.333333 Tz (H2 ) Tj 0.972222 0 Td 53.472222 Tz (production ) Tj 51.428571 0 0 51.428571 0 1953.469413 Tm 6.261111 0 Td 55.092593 Tz (over ) Tj 1.477778 0 Td 47.314815 Tz (time. ) Tj 1.613889 0 Td 50.968013 Tz (Conditions: ) Tj 3.636111 0 Td 56.712963 Tz (10 ) Tj 0.836111 0 Td 82.638889 Tz (mL ) Tj 1.205556 0 Td 47.530864 Tz (1.0 ) Tj 0.991667 0 Td 106.944444 Tz (M ) Tj 0.777778 0 Td 48.611111 Tz (acetate ) Tj 2.197222 0 Td 48.611111 Tz (buffer ) Tj 1.905556 0 Td 43.75 Tz (at ) Tj 0.661111 0 Td 76.157407 Tz (pH ) Tj 1.069444 0 Td 44.560185 Tz (4.0, ) Tj 58.571429 0 0 58.571429 0 1912.566204 Tm 5.668293 0 Td 45.172764 Tz (ascorbic ) Tj 2.373171 0 Td 49.441057 Tz (acid=0.1 ) Tj 2.646341 0 Td 58.333333 Tz (M, ) Tj 1.109756 0 Td 49.085366 Tz (Ru\(bpy\), ) Tj 2.868293 0 Td 46.666667 Tz ("-0.5 ) Tj 1.604878 0 Td 66.395664 Tz (mM, ) Tj 1.468293 0 Td 51.693767 Tz (\(2=5.0 ) Tj 2.082927 0 Td 55.96206 Tz (uM, ) Tj 1.4 0 Td 39.837398 Tz (25 ) Tj 51.428571 0 0 51.428571 0 1872.00243 Tm 6.280556 0 Td 77.777778 Tz (LED ) Tj 1.575 0 Td 41.049383 Tz (light: ) Tj 1.672222 0 Td 61.574074 Tz (450 ) Tj 1.263889 0 Td 59.41358 Tz (nm. ) Tj 1.244444 0 Td 61.574074 Tz (The ) Tj 1.263889 0 Td 55.740741 Tz (arrow ) Tj 1.886111 0 Td 47.170782 Tz (indicates ) Tj 2.702778 0 Td 50.231481 Tz (addition ) Tj 2.566667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 60.185185 Tz (complex ) Tj 58.571429 0 0 58.571429 0 1830.148541 Tm 5.497561 0 Td 51.219512 Tz (2 ) Tj 0.546341 0 Td 42.682927 Tz (\(5.0 ) Tj 1.297561 0 Td 58.807588 Tz (uM\) ) Tj 1.263415 0 Td 52.168022 Tz (and ) Tj 1.382927 0 Td 64.02439 Tz (Ru\(bpy\)* ) Tj 3.346341 0 Td 40.54878 Tz (\(0.5 ) Tj 1.229268 0 Td 72.086721 Tz (mM\) ) Tj 1.502439 0 Td 40.406504 Tz (after ) Tj 1.45122 0 Td 45.528455 Tz (H. ) Tj 0.904878 0 Td 45.212285 Tz (evolution ) Tj 51.428571 0 0 51.428571 0 1789.614085 Tm 6.280556 0 Td 53.703704 Tz (stopped ) Tj 2.488889 0 Td 43.75 Tz (at ) Tj 0.777778 0 Td 49.331276 Tz (indicated ) Tj 2.897222 0 Td 48.611111 Tz (time. ) Tj 51.428571 0 0 51.428571 0 1749.745407 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.594444 0 Td 56.712963 Tz (15 ) Tj 0.933333 0 Td 49.421296 Tz (presents ) Tj 2.644444 0 Td 44.965278 Tz (relative ) Tj 2.391667 0 Td 47.800926 Tz (free ) Tj 1.380556 0 Td 54.012346 Tz (energy ) Tj 2.197222 0 Td 55.497685 Tz (diagrams ) Tj 2.877778 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 60.277778 Tz (postu ) Tj 51.428571 0 0 51.428571 0 1706.67696 Tm 6.261111 0 Td 47.314815 Tz (lated ) Tj 1.555556 0 Td 45.730453 Tz (catalytic ) Tj 2.644444 0 Td 50.231481 Tz (cycles ) Tj 1.944444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 90.740741 Tz (H ) Tj 0.952778 0 Td 51.131687 Tz (evolution ) Tj 2.916667 0 Td 59.953704 Tz (by ) Tj 0.875 0 Td 60.185185 Tz (complex ) Tj 2.683333 0 Td 42.12963 Tz (2. ) Tj 0.758333 0 Td 49.421296 Tz (Relative ) Tj 2.819444 0 Td 45.37037 Tz (30 ) Tj 52.857143 0 0 52.857143 0 1666.010853 Tm 6.091892 0 Td 46.509009 Tz (free ) Tj 1.324324 0 Td 48.873874 Tz (energies ) Tj 2.572973 0 Td 49.399399 Tz (are ) Tj 1.097297 0 Td 51.711712 Tz (given ) Tj 1.797297 0 Td 52.552553 Tz (per ) Tj 1.154054 0 Td 59.121622 Tz (mole ) Tj 1.645946 0 Td 53.603604 Tz (of ) Tj 0.851351 0 Td 81.981982 Tz (H ) Tj 0.945946 0 Td 51.851852 Tz (produced. ) Tj 52.857143 0 0 52.857143 0 1624.21262 Tm 6.82973 0 Td 52.815315 Tz (FIG. ) Tj 1.608108 0 Td 56.756757 Tz (16 ) Tj 1.021622 0 Td 36.261261 Tz (is ) Tj 0.756757 0 Td 50.45045 Tz (a ) Tj 0.624324 0 Td 47.297297 Tz (chart ) Tj 1.721622 0 Td 49.189189 Tz (presenting ) Tj 3.254054 0 Td 46.771772 Tz (cyclic ) Tj 2.005405 0 Td 60.435435 Tz (Voltammogram ) Tj 4.654054 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1581.269565 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.663889 0 Td 58.333333 Tz (2 ) Tj 0.544444 0 Td 42.12963 Tz (in ) Tj 0.777778 0 Td 46.450617 Tz (1.0 ) Tj 0.991667 0 Td 106.944444 Tz (M ) Tj 0.797222 0 Td 58.873457 Tz (sodium ) Tj 2.275 0 Td 55.452675 Tz (phosphate ) Tj 3.130556 0 Td 49.151235 Tz (buffer ) Tj 1.886111 0 Td 45.37037 Tz (at ) Tj 0.661111 0 Td 74.537037 Tz (pH ) Tj 1.069444 0 Td 44.560185 Tz (7.0. ) Tj 1.263889 0 Td 59.143519 Tz (Scan ) Tj 51.428571 0 0 51.428571 0 1538.165049 Tm 6.261111 0 Td 42.12963 Tz (rate, ) Tj 1.516667 0 Td 58.333333 Tz (100 ) Tj 1.225 0 Td 57.037037 Tz (mV/s. ) Tj 1.925 0 Td 59.722222 Tz (Working ) Tj 2.702778 0 Td 46.990741 Tz (electrode, ) Tj 3.013889 0 Td 50.771605 Tz (glassy ) Tj 2.022222 0 Td 50.925926 Tz (carbon; ) Tj 2.372222 0 Td 50.05144 Tz (reference ) Tj 48.367347 0 0 48.367347 0 1496.231332 Tm 6.657384 0 Td 50.309423 Tz (electrode, ) Tj 3.266667 0 Td 62.456048 Tz (Ag/AgCl; ) Tj 3.266667 0 Td 56.610408 Tz (counter ) Tj 2.605063 0 Td 50.309423 Tz (electrode, ) Tj 3.308017 0 Td 49.964838 Tz (Pt ) Tj 0.88903 0 Td 50.998594 Tz (wire. ) Tj 5.706329 0 Td 48.241913 Tz (35 ) Tj 51.428571 0 0 51.428571 0 1458.486631 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.652778 0 Td 56.712963 Tz (17 ) Tj 0.952778 0 Td 40.509259 Tz (is ) Tj 0.777778 0 Td 48.611111 Tz (chart ) Tj 1.730556 0 Td 50.231481 Tz (presenting ) Tj 3.305556 0 Td 48.112536 Tz (potocatalytic ) Tj 4.083333 0 Td 53.472222 Tz (H. ) Tj 1.030556 0 Td 53.472222 Tz (production ) Tj 51.428571 0 0 51.428571 0 1411.534091 Tm 6.261111 0 Td 55.092593 Tz (over ) Tj 1.613889 0 Td 54.282407 Tz (time ) Tj 1.613889 0 Td 46.990741 Tz (in ) Tj 0.933333 0 Td 48.611111 Tz (1.0 ) Tj 1.186111 0 Td 106.944444 Tz (M ) Tj 0.933333 0 Td 49.074074 Tz (acetate ) Tj 2.372222 0 Td 48.611111 Tz (buffer ) Tj 2.022222 0 Td 46.990741 Tz (at ) Tj 0.836111 0 Td 76.157407 Tz (pH ) Tj 1.244444 0 Td 50.771605 Tz (4.0 ) Tj 1.205556 0 Td 54.282407 Tz (with ) Tj 1.633333 0 Td 46.450617 Tz (0.1 ) Tj 1.244444 0 Td 106.944444 Tz (M ) Tj 58.571429 0 0 58.571429 0 1372.790076 Tm 5.497561 0 Td 44.461382 Tz (ascorbic ) Tj 2.339024 0 Td 40.406504 Tz (acid, ) Tj 1.434146 0 Td 43.631436 Tz (0.5 ) Tj 1.041463 0 Td 86.788618 Tz (mM ) Tj 1.434146 0 Td 54.918699 Tz (Ru\(bpy\)'', ) Tj 3.482927 0 Td 53.116531 Tz (and ) Tj 1.160976 0 Td 44.579946 Tz (5.0 ) Tj 1.041463 0 Td 69.715447 Tz (uM ) Tj 1.041463 0 Td 56.097561 Tz (Complex ) Tj 38.571429 0 0 38.571429 0 1336 Tm 8.348148 0 Td 77.777778 Tz (2 ) Tj 0.803704 0 Td 60.493827 Tz (at ) Tj 1.062963 0 Td 72.016461 Tz (22 ) Tj 1.659259 0 Td 71.296296 Tz (C. ) Tj 51.428571 0 0 51.428571 0 1288.19891 Tm 7.019444 0 Td 57.037037 Tz (FIGS. ) Tj 2.119444 0 Td 58.333333 Tz (18 ) Tj 1.069444 0 Td 49.421296 Tz (a-b\) ) Tj 1.516667 0 Td 50.925926 Tz (present ) Tj 2.488889 0 Td 54.012346 Tz (molecular ) Tj 3.266667 0 Td 46.666667 Tz (structures ) Tj 3.169444 0 Td 58.333333 Tz (of ) Tj 0.972222 0 Td 44.290123 Tz (\(a\) ) Tj 1.341667 0 Td 61.574074 Tz (Ni ) Tj 1.186111 0 Td 48.611111 Tz (40 ) Tj 51.428571 0 0 51.428571 0 1250.185567 Tm 6.280556 0 Td 65.174897 Tz (\(DPA-ABpy\)\(H2O\)IBF ) Tj 8.127778 0 Td 57.118056 Tz (\(complex ) Tj 3.013889 0 Td 51.851852 Tz (3\) ) Tj 0.875 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 46.450617 Tz (\(b\) ) Tj 1.283333 0 Td 77.237654 Tz (Co\(DPA ) Tj 51.428571 0 0 51.428571 0 1210.085714 Tm 6.261111 0 Td 78.240741 Tz (ABpy\)PF ) Tj 4.316667 0 Td 57.118056 Tz (\(complex ) Tj 2.936111 0 Td 43.209877 Tz (4\). ) Tj 51.428571 0 0 51.428571 0 1163.520913 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.497222 0 Td 56.712963 Tz (19 ) Tj 0.875 0 Td 59.62963 Tz (shows ) Tj 1.963889 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 73.45679 Tz (DFT ) Tj 1.477778 0 Td 54.012346 Tz (optimized ) Tj 3.052778 0 Td 47.530864 Tz (structure ) Tj 2.683333 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.030556 0 Td 47.800926 Tz (cationic ) Tj 51.428571 0 0 51.428571 0 1126.841379 Tm 6.261111 0 Td 55.632716 Tz (moiety ) Tj 2.255556 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 64.814815 Tz (DIO-Bpy ) Tj 2.955556 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 42.12963 Tz (5. ) Tj 51.428571 0 0 51.428571 0 1082.442231 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.633333 0 Td 59.953704 Tz (20 ) Tj 1.069444 0 Td 59.62963 Tz (shows ) Tj 2.119444 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 56.712963 Tz (UV-vis ) Tj 2.372222 0 Td 51.388889 Tz (Spectra ) Tj 2.469444 0 Td 59.953704 Tz (of ) Tj 0.991667 0 Td 57.523148 Tz (Ru-complexes ) Tj 4.491667 0 Td 51.851852 Tz (6 ) Tj 0.758333 0 Td 46.990741 Tz (45 ) Tj 51.428571 0 0 51.428571 0 1037 Tm 6.280556 0 Td 49.151235 Tz (\(Solid ) Tj 2.002778 0 Td 44.722222 Tz (line\) ) Tj 1.555556 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 58.333333 Tz (5 ) Tj 0.602778 0 Td 49.074074 Tz (\(dotted ) Tj 2.313889 0 Td 43.425926 Tz (line\) ) Tj 1.575 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 80.37037 Tz (CHC1. ) Tj 51.428571 0 0 51.428571 0 1001.428181 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.633333 0 Td 48.611111 Tz (21. ) Tj 1.225 0 Td 45.37037 Tz (\(a\) ) Tj 1.108333 0 Td 52.391975 Tz (Cyclic ) Tj 2.216667 0 Td 61.075499 Tz (Voltammograms ) Tj 5.075 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 55.092593 Tz (5 ) Tj 0.680556 0 Td 43.75 Tz (in ) Tj 0.855556 0 Td 55.452675 Tz (Phosphate ) Tj 51.428571 0 0 51.428571 0 954.464061 Tm 6.261111 0 Td 52.932099 Tz (Buffer ) Tj 2.022222 0 Td 43.75 Tz (at ) Tj 0.680556 0 Td 74.537037 Tz (pH ) Tj 1.069444 0 Td 58.333333 Tz (7 ) Tj 0.505556 0 Td 45.910494 Tz (\(solid ) Tj 1.827778 0 Td 44.722222 Tz (line\) ) Tj 1.458333 0 Td 60.493827 Tz (and ) Tj 1.244444 0 Td 45.37037 Tz (0.1 ) Tj 1.069444 0 Td 100.462963 Tz (MHNO ) Tj 2.819444 0 Td 49.074074 Tz (\(dotted ) Tj 2.216667 0 Td 42.669753 Tz (line\); ) Tj 1.711111 0 Td 46.450617 Tz (\(b\) ) Tj 51.428571 0 0 51.428571 0 913.758454 Tm 6.261111 0 Td 58.981481 Tz (Comparison ) Tj 3.713889 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 84.259259 Tz (CV ) Tj 1.147222 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 48.611111 Tz (the ) Tj 0.991667 0 Td 59.259259 Tz (Absence ) Tj 2.663889 0 Td 48.611111 Tz (\(dotted ) Tj 2.197222 0 Td 43.425926 Tz (line\) ) Tj 1.477778 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 53.472222 Tz (Presence ) Tj 51.428571 0 0 51.428571 0 871 Tm 6.280556 0 Td 45.910494 Tz (\(solid ) Tj 1.925 0 Td 44.722222 Tz (line\) ) Tj 1.633333 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 55.092593 Tz (5 ) Tj 0.641667 0 Td 43.75 Tz (\(1 ) Tj 0.894444 0 Td 81.018519 Tz (mM\) ) Tj 1.75 0 Td 46.990741 Tz (in ) Tj 0.855556 0 Td 46.450617 Tz (0.1 ) Tj 1.225 0 Td 100.462963 Tz (M ) Tj 0.952778 0 Td 82.638889 Tz (HNO. ) Tj 2.294444 0 Td 59.143519 Tz (Scan ) Tj 1.711111 0 Td 41.481481 Tz (rate, ) Tj 1.613889 0 Td 57.253086 Tz (100 ) Tj 1.497222 0 Td 45.37037 Tz (50 ) Tj 51.428571 0 0 51.428571 0 831.113939 Tm 6.261111 0 Td 58.333333 Tz (mV/s; ) Tj 2.002778 0 Td 57.87037 Tz (working ) Tj 2.644444 0 Td 47.638889 Tz (electrode, ) Tj 3.091667 0 Td 50.231481 Tz (glassy ) Tj 2.080556 0 Td 50.925926 Tz (carbon; ) Tj 2.391667 0 Td 52.777778 Tz (counter ) Tj 2.391667 0 Td 47.314815 Tz (electrode, ) Tj 51.428571 0 0 51.428571 0 790.153271 Tm 6.280556 0 Td 50.231481 Tz (Pt ) Tj 0.855556 0 Td 47.314815 Tz (wire; ) Tj 1.730556 0 Td 50.411523 Tz (reference ) Tj 2.916667 0 Td 47.638889 Tz (electrode, ) Tj 3.091667 0 Td 58.333333 Tz (Ag/AgCl. ) Tj 51.428571 0 0 51.428571 0 747.19797 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.477778 0 Td 49.691358 Tz (22. ) Tj 1.069444 0 Td 63.734568 Tz (Oxygen ) Tj 2.488889 0 Td 52.211934 Tz (Evolution ) Tj 3.033333 0 Td 50.231481 Tz (vs ) Tj 0.719444 0 Td 64.814815 Tz (Time ) Tj 1.691667 0 Td 45.37037 Tz (after ) Tj 1.477778 0 Td 53.06713 Tz (Addition ) Tj 2.702778 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 51.851852 Tz (0.33 ) Tj 58.571429 0 0 58.571429 0 706.074074 Tm 5.497561 0 Td 93.902439 Tz (M ) Tj 0.768293 0 Td 60.704607 Tz (Ce' ) Tj 1.4 0 Td 39.837398 Tz (to ) Tj 0.682927 0 Td 48.373984 Tz (3 ) Tj 0.529268 0 Td 75.406504 Tz (mL ) Tj 1.058537 0 Td 51.219512 Tz (of ) Tj 0.75122 0 Td 43.631436 Tz (0.2 ) Tj 1.02439 0 Td 85.365854 Tz (mM ) Tj 1.246341 0 Td 53.116531 Tz (Complexes ) Tj 3.090244 0 Td 48.373984 Tz (5 ) Tj 0.512195 0 Td 39.837398 Tz (in ) Tj 0.75122 0 Td 41.734417 Tz (1.0 ) Tj 0.973171 0 Td 91.056911 Tz (M ) Tj 0.768293 0 Td 73.272358 Tz (HNO. ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 38.571429 0 0 38.571429 0 634 Tm 14.337037 0 Td 97.762346 Tz (DETAILED ) Tj 5.055556 0 Td 95.454545 Tz (DESCRIPTION ) Tj 51.428571 0 0 51.428571 0 544.989583 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 50.411523 Tz (invention ) Tj 2.975 0 Td 51.851852 Tz (provides ) Tj 2.761111 0 Td 52.5 Tz (novel ) Tj 1.847222 0 Td 51.851852 Tz (metal ) Tj 1.808333 0 Td 57.253086 Tz (complexes ) Tj 3.383333 0 Td 48.611111 Tz (useful ) Tj 1.963889 0 Td 51.851852 Tz (as ) Tj 51.428571 0 0 51.428571 0 503.960212 Tm 6.261111 0 Td 46.090535 Tz (catalysts ) Tj 2.916667 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 55.740741 Tz (redox ) Tj 2.061111 0 Td 46.342593 Tz (reactions. ) Tj 3.208333 0 Td 48.611111 Tz (In ) Tj 0.991667 0 Td 44.486532 Tz (particular, ) Tj 3.325 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 51.131687 Tz (invention ) Tj 51.428571 0 0 51.428571 0 460.925749 Tm 6.261111 0 Td 51.446759 Tz (provides ) Tj 2.741667 0 Td 51.851852 Tz (novel ) Tj 1.788889 0 Td 45.37037 Tz (transition ) Tj 2.955556 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 39.969136 Tz (\(e.g., ) Tj 1.652778 0 Td 49.691358 Tz (cobalt ) Tj 2.002778 0 Td 50.231481 Tz (or ) Tj 0.797222 0 Td 47.685185 Tz (nickel\) ) Tj 2.197222 0 Td 63.194444 Tz (com- ) Tj 1.963889 0 Td 45.37037 Tz (60 ) Tj 51.428571 0 0 51.428571 0 423.753846 Tm 6.261111 0 Td 51.311728 Tz (plexes ) Tj 2.158333 0 Td 52.932099 Tz (Supported ) Tj 3.111111 0 Td 59.953704 Tz (by ) Tj 0.991667 0 Td 58.333333 Tz (a ) Tj 0.622222 0 Td 51.041667 Tz (pentadentate ) Tj 3.966667 0 Td 50.231481 Tz (ligand ) Tj 2.1 0 Td 51.203704 Tz (\(such ) Tj 1.827778 0 Td 43.209877 Tz (as, ) Tj 1.088889 0 Td 88.580247 Tz (DPA ) Tj 51.428571 0 0 51.428571 0 379.953307 Tm 6.280556 0 Td 64.814815 Tz (Bpy ) Tj 1.458333 0 Td 53.472222 Tz (or ) Tj 0.913889 0 Td 62.546296 Tz (DPA-ABpy\), ) Tj 4.025 0 Td 58.981481 Tz (which ) Tj 2.041667 0 Td 55.092593 Tz (can ) Tj 1.283333 0 Td 51.203704 Tz (serve ) Tj 1.788889 0 Td 50.231481 Tz (as ) Tj 0.894444 0 Td 46.090535 Tz (catalysts ) Tj 2.761111 0 Td 48.611111 Tz (for ) Tj 1.108333 0 Td 48.611111 Tz (effi ) Tj 52.857143 0 0 52.857143 0 338.663102 Tm 6.091892 0 Td 46.036036 Tz (cient ) Tj 1.645946 0 Td 81.981982 Tz (H ) Tj 0.945946 0 Td 49.504505 Tz (production/evolution ) Tj 6.205405 0 Td 55.18018 Tz (from ) Tj 1.589189 0 Td 54.954955 Tz (aqueous ) Tj 2.535135 0 Td 45.09009 Tz (solutions. ) Tj 40 0 0 40 0 301 Tm 8.075 0 Td 62.5 Tz (Definitions ) Tj 51.428571 0 0 51.428571 0 253.192741 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.283333 0 Td 54.282407 Tz (term ) Tj 1.477778 0 Td 48.611111 Tz (alkyl ) Tj 2.255556 0 Td 45.37037 Tz (refers ) Tj 1.808333 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 45.833333 Tz (radical ) Tj 2.1 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 48.251029 Tz (saturated ) Tj 2.722222 0 Td 46.450617 Tz (aliphatic ) Tj 2.994444 0 Td 43.75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 216.496847 Tm 6.261111 0 Td 51.388889 Tz (groups, ) Tj 2.566667 0 Td 51.131687 Tz (including ) Tj 3.15 0 Td 47.453704 Tz (straight-chain ) Tj 4.394444 0 Td 48.611111 Tz (alkyl ) Tj 1.866667 0 Td 51.388889 Tz (groups, ) Tj 2.586111 0 Td 60.358796 Tz (branched ) Tj 51.428571 0 0 51.428571 0 174.593407 Tm 6.261111 0 Td 51.851852 Tz (chain ) Tj 1.769444 0 Td 48.611111 Tz (alkyl ) Tj 1.672222 0 Td 51.388889 Tz (groups, ) Tj 2.391667 0 Td 49.907407 Tz (cycloalkyl ) Tj 3.227778 0 Td 44.191919 Tz (\(alicyclic\) ) Tj 3.130556 0 Td 51.388889 Tz (groups, ) Tj 2.372222 0 Td 47.962963 Tz (alkyl ) Tj 1.652778 0 Td 69.135802 Tz (Sub ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.805405 0 Td 69.369369 Tz (6 ) Tj 51.428571 0 0 51.428571 0 2917.831106 Tm 25.219444 0 Td 44.155093 Tz (stituted ) Tj 2.352778 0 Td 50.231481 Tz (cycloalkyl ) Tj 3.286111 0 Td 51.388889 Tz (groups, ) Tj 2.372222 0 Td 60.493827 Tz (and ) Tj 1.322222 0 Td 50.231481 Tz (cycloalkyl ) Tj 3.286111 0 Td 47.43266 Tz (Substituted ) Tj 3.344444 0 Td 49.259259 Tz (alkyl ) Tj 51.428571 0 0 51.428571 0 2873.642595 Tm 25.2 0 Td 50.925926 Tz (groups. ) Tj 2.333333 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 55.902778 Tz (term ) Tj 1.536111 0 Td 48.611111 Tz (alkyl ) Tj 1.691667 0 Td 47.222222 Tz (further ) Tj 2.177778 0 Td 49.826389 Tz (includes ) Tj 2.605556 0 Td 48.611111 Tz (alkyl ) Tj 1.633333 0 Td 51.851852 Tz (groups, ) Tj 2.391667 0 Td 59.62963 Tz (which ) Tj 51.428571 0 0 51.428571 0 2830.285369 Tm 25.2 0 Td 55.092593 Tz (can ) Tj 1.205556 0 Td 47.685185 Tz (further ) Tj 2.177778 0 Td 51.388889 Tz (include ) Tj 2.333333 0 Td 55.092593 Tz (oxygen, ) Tj 2.547222 0 Td 47.890947 Tz (nitrogen, ) Tj 2.8 0 Td 47.530864 Tz (Sulfur ) Tj 1.905556 0 Td 50.231481 Tz (or ) Tj 0.777778 0 Td 56.271044 Tz (phosphorous ) Tj 51.428571 0 0 51.428571 0 2785.383033 Tm 25.2 0 Td 57.685185 Tz (atoms ) Tj 2.041667 0 Td 50.05144 Tz (replacing ) Tj 3.033333 0 Td 57.253086 Tz (one ) Tj 1.361111 0 Td 50.231481 Tz (or ) Tj 0.894444 0 Td 62.384259 Tz (more ) Tj 1.788889 0 Td 53.703704 Tz (carbons ) Tj 2.566667 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 55.976431 Tz (hydrocarbon ) Tj 51.428571 0 0 51.428571 0 2744.172237 Tm 25.180556 0 Td 55.092593 Tz (backbone, ) Tj 3.344444 0 Td 40.833333 Tz (e.g., ) Tj 1.672222 0 Td 54.62963 Tz (oxygen, ) Tj 2.722222 0 Td 47.530864 Tz (nitrogen, ) Tj 2.955556 0 Td 48.070988 Tz (Sulfur ) Tj 2.080556 0 Td 53.472222 Tz (or ) Tj 0.991667 0 Td 55.976431 Tz (phosphorous ) Tj 34.285714 0 0 34.285714 0 2703 Tm 37.8 0 Td 78.587963 Tz (atOmS. ) Tj 51.428571 0 0 51.428571 0 2652.42743 Tm 25.919444 0 Td 66.435185 Tz (As ) Tj 0.991667 0 Td 55.092593 Tz (used ) Tj 1.458333 0 Td 48.148148 Tz (herein, ) Tj 2.197222 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 54.282407 Tz (term ) Tj 1.477778 0 Td 48.611111 Tz (aryl ) Tj 1.963889 0 Td 44.830247 Tz (refers ) Tj 1.808333 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 46.296296 Tz (radical ) Tj 2.1 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 47.800926 Tz (aryl ) Tj 51.428571 0 0 51.428571 0 2612.039024 Tm 25.2 0 Td 51.388889 Tz (groups, ) Tj 2.430556 0 Td 50.771605 Tz (including ) Tj 2.994444 0 Td 50.231481 Tz (5- ) Tj 0.836111 0 Td 59.41358 Tz (and ) Tj 1.341667 0 Td 60.925926 Tz (6-membered ) Tj 3.908333 0 Td 47.727273 Tz (single-ring ) Tj 3.383333 0 Td 53.472222 Tz (aromatic ) Tj 51.428571 0 0 51.428571 0 2565.638191 Tm 25.2 0 Td 54.552469 Tz (groups ) Tj 2.197222 0 Td 46.180556 Tz (that ) Tj 1.341667 0 Td 66.975309 Tz (may ) Tj 1.438889 0 Td 51.388889 Tz (include ) Tj 2.352778 0 Td 58.333333 Tz (from ) Tj 1.652778 0 Td 51.041667 Tz (Zero ) Tj 1.438889 0 Td 48.611111 Tz (to ) Tj 0.797222 0 Td 51.851852 Tz (four ) Tj 1.438889 0 Td 51.851852 Tz (heteroatoms, ) Tj 3.986111 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 2524.177891 Tm 25.2 0 Td 55.092593 Tz (example, ) Tj 3.052778 0 Td 53.472222 Tz (benzene, ) Tj 3.013889 0 Td 47.395833 Tz (pyrrole, ) Tj 2.722222 0 Td 47.530864 Tz (furan, ) Tj 2.119444 0 Td 51.203704 Tz (thiophene, ) Tj 3.5 0 Td 50.555556 Tz (imidazole, ) Tj 51.428571 0 0 51.428571 0 2478.351418 Tm 25.180556 0 Td 53.20216 Tz (benzoxazole, ) Tj 4.258333 0 Td 50.231481 Tz (benzothiazole, ) Tj 4.627778 0 Td 43.930041 Tz (triazole, ) Tj 2.8 0 Td 44.722222 Tz (tetrazole, ) Tj 3.111111 0 Td 49.331276 Tz (pyrazole, ) Tj 51.428571 0 0 51.428571 0 2438.849879 Tm 25.2 0 Td 48.251029 Tz (pyridine, ) Tj 2.8 0 Td 50.05144 Tz (pyrazine, ) Tj 2.897222 0 Td 51.203704 Tz (pyridazine ) Tj 3.286111 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 50.968013 Tz (pyrimidine, ) Tj 3.558333 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 41.481481 Tz (like. ) Tj 51.428571 0 0 51.428571 0 2393.22716 Tm 25.2 0 Td 55.092593 Tz (Aryl ) Tj 1.575 0 Td 54.012346 Tz (groups ) Tj 2.216667 0 Td 48.611111 Tz (also ) Tj 1.419444 0 Td 51.388889 Tz (include ) Tj 2.372222 0 Td 50.87963 Tz (polycyclic ) Tj 3.286111 0 Td 52.5 Tz (fused ) Tj 1.827778 0 Td 52.662037 Tz (aromatic ) Tj 2.761111 0 Td 55.632716 Tz (groups ) Tj 51.428571 0 0 51.428571 0 2350.438903 Tm 25.219444 0 Td 54.282407 Tz (Such ) Tj 1.497222 0 Td 51.851852 Tz (as ) Tj 0.855556 0 Td 50.05144 Tz (naphthyl, ) Tj 2.916667 0 Td 47.890947 Tz (quinolyl, ) Tj 2.8 0 Td 46.585648 Tz (indolyl, ) Tj 2.45 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 51.851852 Tz (the ) Tj 1.147222 0 Td 40.833333 Tz (like. ) Tj 1.419444 0 Td 60.277778 Tz (Those ) Tj 2.002778 0 Td 46.990741 Tz (aryl ) Tj 51.428571 0 0 51.428571 0 2305.205919 Tm 25.2 0 Td 54.552469 Tz (groups ) Tj 2.158333 0 Td 55.092593 Tz (having ) Tj 2.177778 0 Td 53.619529 Tz (heteroatoms ) Tj 3.733333 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 48.611111 Tz (ring ) Tj 1.361111 0 Td 47.170782 Tz (structure ) Tj 2.761111 0 Td 66.975309 Tz (may ) Tj 1.380556 0 Td 49.421296 Tz (also ) Tj 1.361111 0 Td 59.953704 Tz (be ) Tj 51.428571 0 0 51.428571 0 2263.029754 Tm 25.2 0 Td 48.206019 Tz (referred ) Tj 2.644444 0 Td 46.990741 Tz (to ) Tj 0.913889 0 Td 50.231481 Tz (as ) Tj 0.952778 0 Td 48.611111 Tz (aryl ) Tj 1.827778 0 Td 49.074074 Tz (heterocycles, ) Tj 4.491667 0 Td 49.608262 Tz (heteroaryls' ) Tj 4.219444 0 Td 53.472222 Tz (or ) Tj 0.952778 0 Td 60.763889 Tz (het ) Tj 51.428571 0 0 51.428571 0 2215.583732 Tm 25.2 0 Td 50.694444 Tz (eroaromatics. ) Tj 4.375 0 Td 64.814815 Tz (The ) Tj 1.283333 0 Td 53.06713 Tz (aromatic ) Tj 2.702778 0 Td 49.421296 Tz (ring ) Tj 1.322222 0 Td 56.17284 Tz (can ) Tj 1.166667 0 Td 58.333333 Tz (be ) Tj 0.836111 0 Td 48.021886 Tz (substituted ) Tj 3.305556 0 Td 43.75 Tz (at ) Tj 0.661111 0 Td 59.41358 Tz (one ) Tj 1.225 0 Td 51.851852 Tz (or ) Tj 51.428571 0 0 51.428571 0 2173.06383 Tm 25.2 0 Td 62.384259 Tz (more ) Tj 1.905556 0 Td 47.800926 Tz (ring ) Tj 1.536111 0 Td 48.611111 Tz (positions ) Tj 3.013889 0 Td 52.662037 Tz (with ) Tj 1.691667 0 Td 54.282407 Tz (Such ) Tj 1.711111 0 Td 47.530864 Tz (substituents ) Tj 3.830556 0 Td 48.611111 Tz (as ) Tj 1.011111 0 Td 51.49177 Tz (described ) Tj 51.428571 0 0 51.428571 0 2133.306569 Tm 25.2 0 Td 52.932099 Tz (above, ) Tj 2.119444 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 54.6875 Tz (example, ) Tj 2.858333 0 Td 51.041667 Tz (halogen, ) Tj 2.683333 0 Td 51.851852 Tz (hydroxyl, ) Tj 2.994444 0 Td 50.925926 Tz (alkoxy, ) Tj 2.333333 0 Td 53.877315 Tz (alkylcar ) Tj 51.428571 0 0 51.428571 0 2092 Tm 25.180556 0 Td 53.652263 Tz (bonyloxy, ) Tj 3.072222 0 Td 51.244213 Tz (arylcarbonyloxy, ) Tj 5.133333 0 Td 53.11214 Tz (alkoxycarbonyloxy, ) Tj 5.911111 0 Td 56.064815 Tz (aryloxycar ) Tj 51.428571 0 0 51.428571 0 2048 Tm 25.180556 0 Td 53.652263 Tz (bonyloxy, ) Tj 3.597222 0 Td 49.691358 Tz (carboxylate, ) Tj 4.297222 0 Td 49.537037 Tz (alkylcarbonyl, ) Tj 4.861111 0 Td 52.283951 Tz (alkoxycarbonyl, ) Tj 51.428571 0 0 51.428571 0 2004 Tm 25.2 0 Td 53.935185 Tz (aminocarbonyl, ) Tj 4.744444 0 Td 49.151235 Tz (alkylthiocarbonyl, ) Tj 5.483333 0 Td 52.175926 Tz (phosphate, ) Tj 3.325 0 Td 54.012346 Tz (phosphonato, ) Tj 51.428571 0 0 51.428571 0 1959.090575 Tm 25.2 0 Td 51.851852 Tz (phosphinato, ) Tj 4.005556 0 Td 51.851852 Tz (cyano, ) Tj 2.138889 0 Td 60.277778 Tz (amino ) Tj 2.1 0 Td 49.583333 Tz (\(including ) Tj 3.188889 0 Td 48.611111 Tz (alkyl ) Tj 1.730556 0 Td 55.092593 Tz (amino, ) Tj 2.236111 0 Td 57.253086 Tz (dialky ) Tj 51.428571 0 0 51.428571 0 1915.38842 Tm 25.2 0 Td 52.314815 Tz (lamino, ) Tj 2.469444 0 Td 51.851852 Tz (arylamino, ) Tj 3.402778 0 Td 51.041667 Tz (diarylamino, ) Tj 3.947222 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 50.231481 Tz (alkylarylamino\), ) Tj 5.075 0 Td 70.216049 Tz (acy ) Tj 51.428571 0 0 51.428571 0 1873.040745 Tm 25.2 0 Td 55.632716 Tz (lamino ) Tj 2.275 0 Td 49.907407 Tz (\(including ) Tj 3.227778 0 Td 52.875244 Tz (alkylcarbonylamino, ) Tj 6.261111 0 Td 52.572016 Tz (arylcarbonylamino, ) Tj 51.428571 0 0 51.428571 0 1826.034696 Tm 25.2 0 Td 56.532922 Tz (carbamoyl ) Tj 3.344444 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 47.395833 Tz (ureido\), ) Tj 2.547222 0 Td 53.472222 Tz (amidino, ) Tj 2.877778 0 Td 51.851852 Tz (imino, ) Tj 2.177778 0 Td 48.021886 Tz (Sulfhydryl, ) Tj 3.461111 0 Td 56.388889 Tz (alkyl ) Tj 51.428571 0 0 51.428571 0 1781.721871 Tm 25.180556 0 Td 44.074074 Tz (thio, ) Tj 1.730556 0 Td 45.37037 Tz (arylthio, ) Tj 2.858333 0 Td 49.016204 Tz (thiocarboxylate, ) Tj 5.152778 0 Td 43.930041 Tz (Sulfates, ) Tj 2.780556 0 Td 48.287037 Tz (Sulfonato, ) Tj 3.325 0 Td 54.444444 Tz (Sulfa ) Tj 51.428571 0 0 51.428571 0 1739.295918 Tm 25.2 0 Td 55.740741 Tz (moyl, ) Tj 2.119444 0 Td 52.662037 Tz (Sulfonamido, ) Tj 4.277778 0 Td 42.12963 Tz (nitro, ) Tj 1.925 0 Td 48.003472 Tz (trifluoromethyl, ) Tj 5.036111 0 Td 52.932099 Tz (cyano, ) Tj 2.333333 0 Td 48.611111 Tz (azido, ) Tj 51.428571 0 0 51.428571 0 1694.409836 Tm 25.180556 0 Td 48.611111 Tz (heterocyclyl, ) Tj 4.122222 0 Td 46.342593 Tz (alkylaryl, ) Tj 3.15 0 Td 53.472222 Tz (or ) Tj 0.952778 0 Td 56.712963 Tz (an ) Tj 1.030556 0 Td 53.06713 Tz (aromatic ) Tj 2.936111 0 Td 50.231481 Tz (or ) Tj 0.913889 0 Td 52.083333 Tz (heteroaromatic ) Tj 52.857143 0 0 52.857143 0 1650.376731 Tm 24.518919 0 Td 49.54955 Tz (moiety. ) Tj 2.459459 0 Td 52.815315 Tz (Aryl ) Tj 1.627027 0 Td 53.603604 Tz (groups ) Tj 2.327027 0 Td 53.603604 Tz (can ) Tj 1.343243 0 Td 47.297297 Tz (also ) Tj 1.513514 0 Td 56.756757 Tz (be ) Tj 1.078378 0 Td 50.45045 Tz (fused ) Tj 1.872973 0 Td 53.603604 Tz (or ) Tj 0.945946 0 Td 52.252252 Tz (bridged ) Tj 2.591892 0 Td 52.027027 Tz (with ) Tj 51.428571 0 0 51.428571 0 1606.868354 Tm 25.2 0 Td 45.37037 Tz (alicyclic ) Tj 2.702778 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 49.151235 Tz (heterocyclic ) Tj 3.772222 0 Td 47.962963 Tz (rings ) Tj 1.691667 0 Td 58.333333 Tz (which ) Tj 1.963889 0 Td 50.771605 Tz (are ) Tj 1.166667 0 Td 48.611111 Tz (not ) Tj 1.108333 0 Td 52.662037 Tz (aromatic ) Tj 2.761111 0 Td 53.472222 Tz (so ) Tj 0.875 0 Td 50.231481 Tz (as ) Tj 51.428571 0 0 51.428571 0 1562.810345 Tm 25.180556 0 Td 46.990741 Tz (to ) Tj 0.855556 0 Td 56.712963 Tz (form ) Tj 1.633333 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 52.932099 Tz (polycycle ) Tj 3.111111 0 Td 39.969136 Tz (\(e.g., ) Tj 1.672222 0 Td 41.157407 Tz (tetralin\). ) Tj 51.428571 0 0 51.428571 0 1518.246073 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 54.282407 Tz (term ) Tj 1.497222 0 Td 51.851852 Tz (carboxylate ) Tj 4.297222 0 Td 44.290123 Tz (refers ) Tj 1.808333 0 Td 45.37037 Tz (to ) Tj 0.758333 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 55.092593 Tz (moiety ) Tj 2.197222 0 Td 51.851852 Tz (derived ) Tj 2.372222 0 Td 58.333333 Tz (from ) Tj 1.594444 0 Td 58.333333 Tz (a ) Tj 51.428571 0 0 51.428571 0 1479.188119 Tm 25.2 0 Td 50.87963 Tz (carboxylic ) Tj 3.305556 0 Td 52.391975 Tz (group, ) Tj 2.119444 0 Td 49.691358 Tz (for ) Tj 1.088889 0 Td 55.092593 Tz (example, ) Tj 2.877778 0 Td 58.333333 Tz (an ) Tj 0.952778 0 Td 57.309942 Tz (alkyl-C\(O\)C\)group. ) Tj 40 0 0 40 0 1436 Tm 33.325 0 Td 81.944444 Tz (The ) Tj 1.9 0 Td 70.833333 Tz (term ) Tj 2.175 0 Td 60.9375 Tz ("chiral' ) Tj 3.4 0 Td 57.638889 Tz (refers ) Tj 2.575 0 Td 58.333333 Tz (to ) Tj 1.175 0 Td 69.907407 Tz (molecules ) Tj 4.25 0 Td 75 Tz (which ) Tj 2.7 0 Td 73.958333 Tz (have ) Tj 2.2 0 Td 65.277778 Tz (the ) Tj 51.428571 0 0 51.428571 0 1389.973589 Tm 25.2 0 Td 51.041667 Tz (property ) Tj 2.683333 0 Td 55.092593 Tz (of ) Tj 0.816667 0 Td 51.54321 Tz (non-Superimposability ) Tj 6.688889 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 51.311728 Tz (mirror ) Tj 2.002778 0 Td 59.62963 Tz (image ) Tj 1.983333 0 Td 56.712963 Tz (part ) Tj 48.571429 0 0 48.571429 0 1343 Tm 26.723529 0 Td 45.465686 Tz (ner, ) Tj 1.358824 0 Td 56.960784 Tz (while ) Tj 1.976471 0 Td 51.470588 Tz (the ) Tj 1.173529 0 Td 57.47549 Tz (term ) Tj 1.626471 0 Td 51.470588 Tz (achiral' ) Tj 3.047059 0 Td 48.039216 Tz (refers ) Tj 1.997059 0 Td 48.039216 Tz (to ) Tj 0.864706 0 Td 57.189542 Tz (molecules ) Tj 3.335294 0 Td 62.45098 Tz (which ) Tj 2.120588 0 Td 53.75817 Tz (are ) Tj 51.428571 0 0 51.428571 0 1302.478939 Tm 25.219444 0 Td 54.166667 Tz (Superimposable ) Tj 4.802778 0 Td 58.333333 Tz (on ) Tj 0.933333 0 Td 46.018519 Tz (their ) Tj 1.633333 0 Td 51.311728 Tz (mirror ) Tj 2.061111 0 Td 59.62963 Tz (image ) Tj 2.002778 0 Td 45.775463 Tz (partner. ) Tj 51.428571 0 0 51.428571 0 1257.102302 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.875 0 Td 42.939815 Tz (this ) Tj 1.341667 0 Td 46.843434 Tz (disclosure, ) Tj 3.422222 0 Td 51.58179 Tz ("comprises. ) Tj 4.005556 0 Td 52.350427 Tz (comprising. ) Tj 4.375 0 Td 56.30787 Tz (contain ) Tj 51.428571 0 0 51.428571 0 1213.604651 Tm 25.2 0 Td 51.851852 Tz (ing ) Tj 1.672222 0 Td 58.333333 Tz (and ) Tj 1.458333 0 Td 55.092593 Tz (having ) Tj 3.033333 0 Td 58.333333 Tz (and ) Tj 1.477778 0 Td 50.771605 Tz (the ) Tj 1.322222 0 Td 44.560185 Tz (like ) Tj 1.477778 0 Td 54.012346 Tz (can ) Tj 1.419444 0 Td 57.523148 Tz (have ) Tj 1.769444 0 Td 50.771605 Tz (the ) Tj 1.361111 0 Td 58.796296 Tz (meaning ) Tj 51.428571 0 0 51.428571 0 1167.135878 Tm 25.2 0 Td 50.636574 Tz (ascribed ) Tj 2.936111 0 Td 46.990741 Tz (to ) Tj 1.088889 0 Td 59.953704 Tz (them ) Tj 1.983333 0 Td 45.37037 Tz (in ) Tj 1.108333 0 Td 51.851852 Tz (U.S. ) Tj 1.769444 0 Td 50.231481 Tz (patent ) Tj 2.333333 0 Td 56.17284 Tz (law ) Tj 1.536111 0 Td 60.493827 Tz (and ) Tj 1.594444 0 Td 57.253086 Tz (can ) Tj 1.555556 0 Td 65.625 Tz (mean ) Tj 51.428571 0 0 51.428571 0 1126.843602 Tm 25.2 0 Td 49.494949 Tz (includes, ) Tj 3.422222 0 Td 49.691358 Tz (including, ) Tj 3.752778 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 42.12963 Tz (like: ) Tj 1.477778 0 Td 49.494949 Tz (consisting ) Tj 3.422222 0 Td 46.843434 Tz (essentially ) Tj 51.428571 0 0 51.428571 0 1082.352697 Tm 25.2 0 Td 56.712963 Tz (of ) Tj 1.361111 0 Td 53.472222 Tz (or ) Tj 1.069444 0 Td 48.251029 Tz (consists ) Tj 3.052778 0 Td 47.260802 Tz (essentially' ) Tj 3.869444 0 Td 50.231481 Tz (likewise ) Tj 2.858333 0 Td 52.932099 Tz (has ) Tj 1.438889 0 Td 48.611111 Tz (the ) Tj 1.322222 0 Td 59.259259 Tz (meaning ) Tj 51.428571 0 0 51.428571 0 1038.004082 Tm 25.2 0 Td 50.636574 Tz (ascribed ) Tj 2.761111 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 51.851852 Tz (U.S. ) Tj 1.613889 0 Td 49.691358 Tz (patent ) Tj 2.119444 0 Td 56.17284 Tz (law ) Tj 1.380556 0 Td 58.333333 Tz (and ) Tj 1.4 0 Td 48.611111 Tz (the ) Tj 1.225 0 Td 54.282407 Tz (term ) Tj 1.652778 0 Td 38.888889 Tz (is ) Tj 0.797222 0 Td 54.208754 Tz (open-ended, ) Tj 51.428571 0 0 51.428571 0 993.636704 Tm 25.2 0 Td 53.06713 Tz (allowing ) Tj 2.761111 0 Td 47.530864 Tz (for ) Tj 1.05 0 Td 47.530864 Tz (the ) Tj 1.030556 0 Td 53.877315 Tz (presence ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 61.574074 Tz (more ) Tj 1.652778 0 Td 51.041667 Tz (than ) Tj 1.477778 0 Td 44.560185 Tz (that ) Tj 1.283333 0 Td 58.333333 Tz (which ) Tj 1.944444 0 Td 42.12963 Tz (is ) Tj 0.7 0 Td 47.222222 Tz (recited ) Tj 51.428571 0 0 51.428571 0 948.729223 Tm 25.219444 0 Td 51.851852 Tz (So ) Tj 0.933333 0 Td 55.092593 Tz (long ) Tj 1.575 0 Td 51.851852 Tz (as ) Tj 0.933333 0 Td 49.907407 Tz (basic ) Tj 1.827778 0 Td 51.851852 Tz (or ) Tj 0.913889 0 Td 53.148148 Tz (novel ) Tj 1.905556 0 Td 46.234568 Tz (characteristics ) Tj 4.472222 0 Td 59.953704 Tz (of ) Tj 0.913889 0 Td 45.37037 Tz (that ) Tj 1.4 0 Td 58.981481 Tz (which ) Tj 2.080556 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 907.129032 Tm 25.2 0 Td 47.222222 Tz (recited ) Tj 2.275 0 Td 40.509259 Tz (is ) Tj 0.816667 0 Td 50.771605 Tz (not ) Tj 1.225 0 Td 57.407407 Tz (changed ) Tj 2.702778 0 Td 58.333333 Tz (by ) Tj 1.030556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 53.06713 Tz (presence ) Tj 2.877778 0 Td 55.092593 Tz (of ) Tj 0.894444 0 Td 62.384259 Tz (more ) Tj 1.788889 0 Td 51.851852 Tz (than ) Tj 1.555556 0 Td 46.180556 Tz (that ) Tj 51.428571 0 0 51.428571 0 860.824176 Tm 25.180556 0 Td 59.62963 Tz (which ) Tj 2.041667 0 Td 38.888889 Tz (is ) Tj 0.738889 0 Td 44.560185 Tz (recited, ) Tj 2.391667 0 Td 50.771605 Tz (but ) Tj 1.147222 0 Td 53.06713 Tz (excludes ) Tj 2.8 0 Td 48.611111 Tz (prior ) Tj 1.672222 0 Td 43.209877 Tz (art ) Tj 1.011111 0 Td 56.442901 Tz (embodiments. ) Tj 40 0 0 40 0 825 Tm 33.325 0 Td 81.944444 Tz (The ) Tj 1.9 0 Td 70.833333 Tz (term ) Tj 2.175 0 Td 66.666667 Tz ("diastereomers' ) Tj 6.475 0 Td 58.333333 Tz (refers ) Tj 2.575 0 Td 58.333333 Tz (to ) Tj 1.175 0 Td 65.384615 Tz (stereoisomers ) Tj 5.575 0 Td 69.791667 Tz (with ) Tj 51.428571 0 0 51.428571 0 774.924812 Tm 25.180556 0 Td 60.493827 Tz (two ) Tj 1.380556 0 Td 51.851852 Tz (or ) Tj 0.855556 0 Td 61.574074 Tz (more ) Tj 1.730556 0 Td 48.611111 Tz (centers ) Tj 2.294444 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 56.565657 Tz (dissymmetry ) Tj 3.986111 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 61.574074 Tz (whose ) Tj 2.119444 0 Td 54.012346 Tz (molecules ) Tj 51.428571 0 0 51.428571 0 731.68254 Tm 25.2 0 Td 49.691358 Tz (are ) Tj 1.166667 0 Td 49.691358 Tz (not ) Tj 1.147222 0 Td 51.851852 Tz (mirror ) Tj 2.080556 0 Td 57.253086 Tz (images ) Tj 2.313889 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 59.41358 Tz (one ) Tj 1.283333 0 Td 48.206019 Tz (another. ) Tj 51.428571 0 0 51.428571 0 689.173735 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 54.282407 Tz (term ) Tj 1.575 0 Td 54.6875 Tz (halogen ) Tj 3.188889 0 Td 50.231481 Tz (designates ) Tj 3.247222 0 Td 70.216049 Tz (F. ) Tj 1.516667 0 Td 66.435185 Tz (Cl, ) Tj 1.847222 0 Td 82.098765 Tz (Br ) Tj 1.691667 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 63.734568 Tz (I. ) Tj 51.428571 0 0 51.428571 0 645.186047 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.497222 0 Td 55.092593 Tz (term ) Tj 1.711111 0 Td 51.851852 Tz (hydrate ) Tj 3.208333 0 Td 44.830247 Tz (refers ) Tj 2.022222 0 Td 42.12963 Tz (to ) Tj 0.913889 0 Td 51.851852 Tz (a ) Tj 0.7 0 Td 52.5 Tz (metal ) Tj 1.944444 0 Td 60.185185 Tz (complex ) Tj 2.897222 0 Td 56.712963 Tz (of ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 48.571429 0 0 48.571429 0 601 Tm 26.682353 0 Td 53.75817 Tz (invention ) Tj 3.252941 0 Td 54.901961 Tz (or ) Tj 0.926471 0 Td 61.764706 Tz (a ) Tj 0.679412 0 Td 45.465686 Tz (salt ) Tj 1.4 0 Td 49.32598 Tz (thereof, ) Tj 2.697059 0 Td 61.764706 Tz (which ) Tj 2.202941 0 Td 50.490196 Tz (further ) Tj 2.408824 0 Td 53.186275 Tz (includes ) Tj 2.861765 0 Td 61.764706 Tz (a ) Tj 0.720588 0 Td 55.759804 Tz (stoi ) Tj 51.428571 0 0 51.428571 0 555.364508 Tm 25.2 0 Td 51.527778 Tz (chiometric ) Tj 3.305556 0 Td 51.851852 Tz (or ) Tj 0.797222 0 Td 50.591564 Tz (non-stoichiometric ) Tj 5.677778 0 Td 59.953704 Tz (amount ) Tj 2.372222 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 54.444444 Tz (water ) Tj 1.808333 0 Td 60.925926 Tz (bound ) Tj 1.983333 0 Td 61.574074 Tz (by ) Tj 40 0 0 40 0 519 Tm 32.4 0 Td 68.055556 Tz (non-covalent ) Tj 5.2 0 Td 65.47619 Tz (intermolecular ) Tj 5.75 0 Td 59.52381 Tz (forces. ) Tj 51.428571 0 0 51.428571 0 470.592751 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 54.282407 Tz (term ) Tj 1.575 0 Td 54.73251 Tz (hydroxyl ) Tj 3.558333 0 Td 59.62963 Tz (means ) Tj 2.061111 0 Td 80.208333 Tz (OH. ) Tj 40 0 0 40 0 432 Tm 33.325 0 Td 81.944444 Tz (The ) Tj 1.775 0 Td 68.75 Tz (term ) Tj 1.95 0 Td 70.138889 Tz ("heteroatom' ) Tj 5.35 0 Td 62.5 Tz (as ) Tj 1.05 0 Td 71.875 Tz (used ) Tj 1.975 0 Td 65.277778 Tz (herein ) Tj 2.675 0 Td 78.333333 Tz (means ) Tj 2.625 0 Td 75 Tz (an ) Tj 1.175 0 Td 78.125 Tz (atom ) Tj 2.2 0 Td 72.916667 Tz (of ) Tj 51.428571 0 0 51.428571 0 382.05598 Tm 25.2 0 Td 57.253086 Tz (any ) Tj 1.361111 0 Td 55.092593 Tz (element ) Tj 2.625 0 Td 49.907407 Tz (other ) Tj 1.75 0 Td 52.662037 Tz (than ) Tj 1.575 0 Td 54.552469 Tz (carbon ) Tj 2.294444 0 Td 53.472222 Tz (or ) Tj 0.913889 0 Td 53.652263 Tz (hydrogen. ) Tj 3.266667 0 Td 55.681818 Tz (Heteroatoms ) Tj 51.428571 0 0 51.428571 0 341.313043 Tm 25.2 0 Td 48.206019 Tz (include, ) Tj 2.566667 0 Td 55.092593 Tz (Such ) Tj 1.555556 0 Td 44.290123 Tz (as, ) Tj 1.069444 0 Td 47.890947 Tz (nitrogen, ) Tj 2.819444 0 Td 55.555556 Tz (oxygen, ) Tj 2.586111 0 Td 47.530864 Tz (Sulfur ) Tj 1.905556 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 53.324916 Tz (phosphorus. ) Tj 51.428571 0 0 51.428571 0 295.888604 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 54.282407 Tz (term ) Tj 1.477778 0 Td 49.331276 Tz (isotopic ) Tj 2.838889 0 Td 55.632716 Tz (forms ) Tj 2.216667 0 Td 46.018519 Tz (refer ) Tj 1.536111 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 46.990741 Tz (variants ) Tj 2.430556 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 46.990741 Tz (particular ) Tj 51.428571 0 0 51.428571 0 252.99754 Tm 25.2 0 Td 54.6875 Tz (chemical ) Tj 2.8 0 Td 51.851852 Tz (element. ) Tj 2.663889 0 Td 51.851852 Tz (All ) Tj 1.166667 0 Td 49.016204 Tz (isotopes ) Tj 2.586111 0 Td 55.092593 Tz (of ) Tj 0.777778 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 53.148148 Tz (given ) Tj 1.788889 0 Td 56.018519 Tz (element ) Tj 2.527778 0 Td 51.851852 Tz (share ) Tj 1.730556 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 212.307305 Tm 25.219444 0 Td 61.574074 Tz (same ) Tj 1.730556 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 49.016204 Tz (protons, ) Tj 2.586111 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 50 Tz (isotope ) Tj 2.333333 0 Td 43.981481 Tz (differs ) Tj 2.080556 0 Td 58.333333 Tz (from ) Tj 1.633333 0 Td 50.771605 Tz (the ) Tj 40 0 0 40 0 176 Tm 32.4 0 Td 63.194444 Tz (others ) Tj 2.625 0 Td 56.25 Tz (in ) Tj 1 0 Td 48.611111 Tz (its ) Tj 1.225 0 Td 79.861111 Tz (number ) Tj 3.175 0 Td 72.916667 Tz (of ) Tj 1.125 0 Td 62.037037 Tz (neutrons. ) Tj ET Q endstream endobj 268 0 obj << /Length 1 >> stream q endstream endobj 269 0 obj << /Length 35849 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 51.428571 0 0 51.428571 0 2968 Tm 14.777778 0 Td 77.777778 Tz (7 ) Tj 48.571429 0 0 48.571429 0 2915 Tm 7.411765 0 Td 70.343137 Tz (As ) Tj 1.276471 0 Td 58.333333 Tz (used ) Tj 1.791176 0 Td 50.490196 Tz (herein, ) Tj 2.552941 0 Td 58.333333 Tz (redox ) Tj 2.511765 0 Td 51.813725 Tz (reactions' ) Tj 3.561765 0 Td 48.72549 Tz (refer ) Tj 1.832353 0 Td 49.754902 Tz (to ) Tj 1.029412 0 Td 58.333333 Tz (reduction ) Tj 48.571429 0 0 48.571429 0 2874 Tm 6.629412 0 Td 53.75817 Tz (oxidation ) Tj 3.314706 0 Td 49.411765 Tz (reactions, ) Tj 3.397059 0 Td 46.323529 Tz (in ) Tj 0.967647 0 Td 62.45098 Tz (which ) Tj 2.285294 0 Td 50 Tz (certain ) Tj 2.491176 0 Td 61.764706 Tz (atoms ) Tj 2.264706 0 Td 48.039216 Tz (in ) Tj 0.988235 0 Td 57.904412 Tz (chemical ) Tj 51.428571 0 0 51.428571 0 2831.241552 Tm 6.261111 0 Td 50.231481 Tz (reagents ) Tj 2.683333 0 Td 52.662037 Tz (involved ) Tj 2.761111 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 47.800926 Tz (reaction ) Tj 2.527778 0 Td 58.333333 Tz (have ) Tj 1.633333 0 Td 45.37037 Tz (their ) Tj 1.594444 0 Td 50.411523 Tz (oxidation ) Tj 2.975 0 Td 44.722222 Tz (state ) Tj 51.428571 0 0 51.428571 0 2796 Tm 6.261111 0 Td 53.877315 Tz (changed. ) Tj 48.571429 0 0 48.571429 0 2749 Tm 7.411765 0 Td 70.343137 Tz (As ) Tj 1.091176 0 Td 58.333333 Tz (used ) Tj 1.585294 0 Td 50.490196 Tz (herein, ) Tj 2.326471 0 Td 60.04902 Tz (a ) Tj 0.926471 0 Td 48.382353 Tz (transition ) Tj 3.15 0 Td 56.045752 Tz (metal' ) Tj 2.244118 0 Td 48.611111 Tz (refers ) Tj 1.976471 0 Td 48.039216 Tz (to ) Tj 0.844118 0 Td 51.470588 Tz (the ) Tj 1.111765 0 Td 58.823529 Tz (element ) Tj 51.428571 0 0 51.428571 0 2708.247821 Tm 6.261111 0 Td 50.231481 Tz (as ) Tj 0.738889 0 Td 55.092593 Tz (appear ) Tj 2.138889 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 58.873457 Tz (Groups ) Tj 2.294444 0 Td 55.092593 Tz (3 ) Tj 0.544444 0 Td 53.240741 Tz (through ) Tj 2.469444 0 Td 53.472222 Tz (12 ) Tj 0.797222 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 47.530864 Tz (the ) Tj 1.05 0 Td 49.826389 Tz (Periodic ) Tj 2.527778 0 Td 54.444444 Tz (Table ) Tj 1.75 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 2665.145679 Tm 6.280556 0 Td 52.932099 Tz (Elements, ) Tj 3.072222 0 Td 51.851852 Tz (or ) Tj 0.777778 0 Td 58.333333 Tz (an ) Tj 0.913889 0 Td 46.990741 Tz (isotopic ) Tj 2.488889 0 Td 57.523148 Tz (form ) Tj 1.613889 0 Td 45.775463 Tz (thereof. ) Tj 2.411111 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 45.694444 Tz (transition ) Tj 2.975 0 Td 51.851852 Tz (metals ) Tj 51.428571 0 0 51.428571 0 2623.437252 Tm 6.261111 0 Td 47.800926 Tz (include, ) Tj 2.644444 0 Td 49.691358 Tz (for ) Tj 1.186111 0 Td 55.092593 Tz (example, ) Tj 2.994444 0 Td 46.990741 Tz (iron ) Tj 1.497222 0 Td 45.37037 Tz (\(Fe\), ) Tj 1.691667 0 Td 50.231481 Tz (cobalt ) Tj 2.119444 0 Td 49.907407 Tz (\(Co\), ) Tj 1.866667 0 Td 48.070988 Tz (nickel ) Tj 2.080556 0 Td 45.37037 Tz (\(Ni\). ) Tj 51.428571 0 0 51.428571 0 2582.652393 Tm 6.261111 0 Td 55.092593 Tz (ruthenium ) Tj 3.305556 0 Td 50.555556 Tz (\(Ru\), ) Tj 1.847222 0 Td 58.333333 Tz (rhodium ) Tj 2.8 0 Td 49.907407 Tz (\(Rh\), ) Tj 1.866667 0 Td 59.053498 Tz (manganese ) Tj 3.5 0 Td 55.740741 Tz (\(Mn\), ) Tj 2.002778 0 Td 59.41358 Tz (techne ) Tj 51.428571 0 0 51.428571 0 2541.567686 Tm 6.241667 0 Td 55.902778 Tz (tium ) Tj 1.613889 0 Td 45.37037 Tz (\(Tc\), ) Tj 1.613889 0 Td 52.932099 Tz (palladium ) Tj 3.169444 0 Td 51.851852 Tz (\(Pd\) ) Tj 1.458333 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 42.939815 Tz (etc. ) Tj 40 0 0 40 0 2505 Tm 9 0 Td 80.555556 Tz (The ) Tj 1.725 0 Td 69.791667 Tz (term ) Tj 1.925 0 Td 64.814815 Tz ("solvate ) Tj 3.75 0 Td 64.583333 Tz (as ) Tj 1.05 0 Td 71.875 Tz (used ) Tj 1.975 0 Td 64.583333 Tz (herein ) Tj 2.625 0 Td 58.333333 Tz (refers ) Tj 2.4 0 Td 56.25 Tz (to ) Tj 0.975 0 Td 63.095238 Tz (solvate ) Tj 2.925 0 Td 71.666667 Tz (forms ) Tj 51.428571 0 0 51.428571 0 2459.23609 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 57.613169 Tz (complexes ) Tj 3.363889 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 50.462963 Tz (present ) Tj 2.352778 0 Td 48.611111 Tz (invention. ) Tj 51.428571 0 0 51.428571 0 2419.270588 Tm 6.261111 0 Td 56.388889 Tz (Metal ) Tj 1.944444 0 Td 60.493827 Tz (Complexes ) Tj 51.428571 0 0 51.428571 0 2375.929293 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.283333 0 Td 50.411523 Tz (invention ) Tj 2.877778 0 Td 52.662037 Tz (provides ) Tj 2.722222 0 Td 52.5 Tz (metal ) Tj 1.730556 0 Td 57.613169 Tz (complexes ) Tj 3.286111 0 Td 45.37037 Tz (that ) Tj 1.244444 0 Td 49.691358 Tz (are ) Tj 1.069444 0 Td 48.611111 Tz (useful ) Tj 1.905556 0 Td 50.231481 Tz (as ) Tj 51.428571 0 0 51.428571 0 2333.960212 Tm 6.261111 0 Td 46.090535 Tz (catalysts ) Tj 2.916667 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 55.740741 Tz (redox ) Tj 2.061111 0 Td 46.342593 Tz (reactions. ) Tj 3.208333 0 Td 48.611111 Tz (In ) Tj 0.991667 0 Td 44.486532 Tz (particular, ) Tj 3.325 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 51.131687 Tz (invention ) Tj 51.428571 0 0 51.428571 0 2295.333333 Tm 6.261111 0 Td 51.446759 Tz (provides ) Tj 2.722222 0 Td 51.851852 Tz (metal ) Tj 1.769444 0 Td 56.893004 Tz (complexes ) Tj 3.227778 0 Td 51.851852 Tz (as ) Tj 0.797222 0 Td 43.569959 Tz (efficient ) Tj 2.527778 0 Td 45.37037 Tz (catalysts ) Tj 2.683333 0 Td 47.530864 Tz (for ) Tj 0.991667 0 Td 57.928241 Tz (hydrogen ) Tj 51.428571 0 0 51.428571 0 2251.169268 Tm 6.261111 0 Td 50.084175 Tz (production. ) Tj 3.538889 0 Td 46.990741 Tz (In ) Tj 0.777778 0 Td 46.296296 Tz (certain ) Tj 2.119444 0 Td 56.983025 Tz (embodiments, ) Tj 4.258333 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 52.5 Tz (metal ) Tj 1.75 0 Td 57.613169 Tz (complexes ) Tj 3.305556 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 2209.741148 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.411523 Tz (invention ) Tj 2.916667 0 Td 51.851852 Tz (are ) Tj 1.108333 0 Td 43.930041 Tz (efficient ) Tj 2.566667 0 Td 46.788194 Tz (electrocatalysts ) Tj 4.725 0 Td 47.530864 Tz (for ) Tj 1.05 0 Td 54.73251 Tz (producing ) Tj 3.208333 0 Td 56.712963 Tz (H2 ) Tj 51.428571 0 0 51.428571 0 2166.226933 Tm 6.261111 0 Td 58.333333 Tz (from ) Tj 1.633333 0 Td 56.712963 Tz (an ) Tj 0.894444 0 Td 56.944444 Tz (aqueous ) Tj 2.605556 0 Td 46.450617 Tz (solution. ) Tj 2.8 0 Td 45.37037 Tz (In ) Tj 0.797222 0 Td 49.907407 Tz (other ) Tj 1.672222 0 Td 57.253086 Tz (embodiments, ) Tj 4.336111 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2126.698393 Tm 6.261111 0 Td 57.613169 Tz (complexes ) Tj 3.383333 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 50.411523 Tz (invention ) Tj 3.013889 0 Td 49.691358 Tz (are ) Tj 1.147222 0 Td 43.569959 Tz (efficient ) Tj 2.586111 0 Td 49.537037 Tz (photocatalysts ) Tj 4.472222 0 Td 47.530864 Tz (for ) Tj 52.857143 0 0 52.857143 0 2085.127103 Tm 6.091892 0 Td 53.603604 Tz (producing ) Tj 3.140541 0 Td 81.981982 Tz (H ) Tj 0.964865 0 Td 55.968468 Tz (from ) Tj 1.608108 0 Td 53.603604 Tz (an ) Tj 0.87027 0 Td 55.405405 Tz (aqueous ) Tj 2.572973 0 Td 44.844845 Tz (solution. ) Tj 51.428571 0 0 51.428571 0 2043.321178 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.555556 0 Td 53.148148 Tz (metal ) Tj 2.022222 0 Td 57.613169 Tz (complexes ) Tj 3.558333 0 Td 56.712963 Tz (of ) Tj 0.991667 0 Td 50.771605 Tz (the ) Tj 1.341667 0 Td 48.611111 Tz (invention, ) Tj 3.344444 0 Td 48.611111 Tz (for ) Tj 1.244444 0 Td 55.092593 Tz (example, ) Tj 51.428571 0 0 51.428571 0 2002.26245 Tm 6.261111 0 Td 55.902778 Tz (comprise ) Tj 3.091667 0 Td 45.37037 Tz (at ) Tj 0.972222 0 Td 44.722222 Tz (least ) Tj 1.788889 0 Td 57.253086 Tz (one ) Tj 1.438889 0 Td 46.018519 Tz (transition ) Tj 3.247222 0 Td 52.5 Tz (metal ) Tj 2.002778 0 Td 59.41358 Tz (complexed ) Tj 3.636111 0 Td 54.282407 Tz (with ) Tj 51.428571 0 0 51.428571 0 1960.028133 Tm 6.280556 0 Td 67.12963 Tz (DPA-Bpy ) Tj 3.091667 0 Td 50.231481 Tz (or ) Tj 0.875 0 Td 36.728395 Tz (its ) Tj 0.952778 0 Td 48.287037 Tz (derivative ) Tj 3.169444 0 Td 45.775463 Tz (thereof. ) Tj 2.527778 0 Td 43.75 Tz (In ) Tj 0.816667 0 Td 44.486532 Tz (particular, ) Tj 3.208333 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 48.148148 Tz (certain ) Tj 51.428571 0 0 51.428571 0 1916.34026 Tm 6.261111 0 Td 56.983025 Tz (embodiments, ) Tj 4.511111 0 Td 50.771605 Tz (the ) Tj 1.302778 0 Td 50.771605 Tz (invention ) Tj 3.15 0 Td 52.256944 Tz (provides ) Tj 2.975 0 Td 52.5 Tz (novel ) Tj 1.983333 0 Td 50.231481 Tz (cobalt ) Tj 2.216667 0 Td 55.092593 Tz (\(Co\) ) Tj 51.428571 0 0 51.428571 0 1878.505967 Tm 6.261111 0 Td 54.768519 Tz (complexes, ) Tj 3.5 0 Td 58.333333 Tz (which ) Tj 1.944444 0 Td 55.497685 Tz (comprise ) Tj 2.838889 0 Td 68.055556 Tz (Co ) Tj 1.011111 0 Td 59.773663 Tz (complexed ) Tj 3.422222 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 54.768519 Tz (N,N-Bis\(2- ) Tj 51.428571 0 0 51.428571 0 1839.079137 Tm 6.261111 0 Td 51.992754 Tz (pyridinylmethyl\)-2,2'-Bipyridine-6-methanamine ) Tj 15.594444 0 Td 77.777778 Tz (\(DPA ) Tj 51.428571 0 0 51.428571 0 1799 Tm 6.280556 0 Td 53.796296 Tz (Bpy\), ) Tj 2.605556 0 Td 49.453704 Tz (N,N-bis\(\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 1754.945241 Tm 6.261111 0 Td 53.337191 Tz (pyridin-2-yl\)methanamine ) Tj 8.322222 0 Td 56.712963 Tz (\(DIQ-Bpy\), ) Tj 4.044444 0 Td 51.851852 Tz (or ) Tj 1.244444 0 Td 51.851852 Tz (a ) Tj 0.972222 0 Td 48.287037 Tz (derivative ) Tj 48.571429 0 0 48.571429 0 1710 Tm 6.608824 0 Td 49.32598 Tz (thereof. ) Tj 2.758824 0 Td 49.754902 Tz (In ) Tj 0.926471 0 Td 49.509804 Tz (certain ) Tj 2.429412 0 Td 60.620915 Tz (embodiments, ) Tj 4.735294 0 Td 50.612745 Tz (said ) Tj 1.544118 0 Td 51.470588 Tz (derivative ) Tj 3.438235 0 Td 60.04902 Tz (of ) Tj 0.988235 0 Td 93.79085 Tz (DPA ) Tj 51.428571 0 0 51.428571 0 1669.77749 Tm 6.280556 0 Td 64.814815 Tz (Bpy ) Tj 1.497222 0 Td 40.509259 Tz (is ) Tj 0.816667 0 Td 67.592593 Tz (DPA-Bpy ) Tj 3.130556 0 Td 51.527778 Tz (containing ) Tj 3.363889 0 Td 60.493827 Tz (one ) Tj 1.380556 0 Td 55.092593 Tz (or ) Tj 0.952778 0 Td 61.574074 Tz (more ) Tj 1.769444 0 Td 46.118234 Tz (substituents. ) Tj 3.947222 0 Td 51.851852 Tz (In ) Tj 52.857143 0 0 52.857143 0 1624.42132 Tm 6.091892 0 Td 45.945946 Tz (certain ) Tj 2.232432 0 Td 55.442943 Tz (embodiments, ) Tj 4.294595 0 Td 48.348348 Tz (the ) Tj 1.172973 0 Td 47.297297 Tz (derivative ) Tj 3.140541 0 Td 56.756757 Tz (of ) Tj 0.927027 0 Td 63.063063 Tz (DIQ-Bpy ) Tj 2.951351 0 Td 39.414414 Tz (is ) Tj 0.794595 0 Td 81.981982 Tz (DIQ ) Tj 51.428571 0 0 51.428571 0 1584.818859 Tm 6.280556 0 Td 65.895062 Tz (Bpy ) Tj 1.438889 0 Td 51.527778 Tz (containing ) Tj 3.344444 0 Td 57.253086 Tz (one ) Tj 1.302778 0 Td 51.851852 Tz (or ) Tj 0.855556 0 Td 61.574074 Tz (more ) Tj 1.730556 0 Td 46.118234 Tz (substituents, ) Tj 3.830556 0 Td 41.481481 Tz (e.g., ) Tj 1.516667 0 Td 47.530864 Tz (Substituents ) Tj 51.428571 0 0 51.428571 0 1544.96343 Tm 6.261111 0 Td 59.953704 Tz (on ) Tj 0.952778 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 49.96142 Tz (isoquinoline ) Tj 3.830556 0 Td 45.833333 Tz (ring\(s\) ) Tj 2.158333 0 Td 52.932099 Tz (and/or ) Tj 2.119444 0 Td 59.953704 Tz (on ) Tj 0.952778 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 50.462963 Tz (pyridyl ) Tj 2.372222 0 Td 45.833333 Tz (ring\(s\) ) Tj 2.197222 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 1506.574179 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.225 0 Td 51.118099 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyri ) Tj 51.428571 0 0 51.428571 0 1465 Tm 6.261111 0 Td 54.282407 Tz (din-2-yl\)methanamine ) Tj 6.766667 0 Td 50.462963 Tz (moiety. ) Tj 51.428571 0 0 51.428571 0 1416.370518 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.875 0 Td 46.296296 Tz (certain ) Tj 2.216667 0 Td 56.983025 Tz (embodiments, ) Tj 4.394444 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 50.05144 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.8 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1377.214953 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 54.62963 Tz (formula ) Tj 2.547222 0 Td 39.969136 Tz (\(I\) ) Tj 40 0 0 40 0 1257 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 1210 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.926471 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 47.696078 Tz (transition ) Tj 3.191176 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 1173.527141 Tm 7 0 Td 84.259259 Tz (G ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.738889 0 Td 51.587302 Tz (N,N-bis\(2-pyridinylmethyl\)-2,2'-bipyridine-6-meth ) Tj 51.428571 0 0 51.428571 0 1130.833333 Tm 6.261111 0 Td 58.333333 Tz (anamine ) Tj 2.780556 0 Td 58.333333 Tz (\(DPA-Bpy\), ) Tj 3.830556 0 Td 51.666667 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6- ) Tj 51.428571 0 0 51.428571 0 1090.5086 Tm 6.280556 0 Td 51.169591 Tz (\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 12.230556 0 Td 59.053498 Tz (\(DIQ-Bpy\) ) Tj 3.733333 0 Td 53.472222 Tz (or ) Tj 1.166667 0 Td 55.092593 Tz (a ) Tj 48.571429 0 0 48.571429 0 1043 Tm 6.629412 0 Td 51.470588 Tz (derivative ) Tj 3.355882 0 Td 52.45098 Tz (thereof ) Tj 51.428571 0 0 51.428571 0 1004.309278 Tm 6.980556 0 Td 50.231481 Tz (Y, ) Tj 0.855556 0 Td 48.611111 Tz (for ) Tj 1.030556 0 Td 55.092593 Tz (each ) Tj 1.555556 0 Td 50.673401 Tz (occurrence, ) Tj 3.558333 0 Td 52.599715 Tz (independently ) Tj 4.336111 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 55.555556 Tz (halogen ) Tj 2.527778 0 Td 56.388889 Tz (group ) Tj 51.428571 0 0 51.428571 0 960.123711 Tm 6.261111 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 53.796296 Tz (water ) Tj 1.847222 0 Td 55.632716 Tz (moiety ) Tj 2.275 0 Td 35.648148 Tz (\(i.e., ) Tj 1.594444 0 Td 56.388889 Tz (H2O\): ) Tj 51.428571 0 0 51.428571 0 919.468705 Tm 6.980556 0 Td 59.953704 Tz (X, ) Tj 0.952778 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 51.262626 Tz (occurrence, ) Tj 3.616667 0 Td 52.849003 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 49.691358 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 877.418006 Tm 7 0 Td 90.740741 Tz (m ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 51.851852 Tz (the ) Tj 1.205556 0 Td 61.574074 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 835.463576 Tm 7 0 Td 58.333333 Tz (n ) Tj 0.622222 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 52.391975 Tz (anions ) Tj 2.138889 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 794 Tm 7.432353 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 41.176471 Tz (is ) Tj 0.761765 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 54.901961 Tz (or ) Tj 0.885294 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50 Tz (neutral ) Tj 2.408824 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 751.989418 Tm 7 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 38.888889 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 61.033951 Tz (number ) Tj 2.430556 0 Td 55.092593 Tz (of ) Tj 0.816667 0 Td 47.685185 Tz (neutral ) Tj 2.255556 0 Td 54.012346 Tz (molecules ) Tj 3.111111 0 Td 55.092593 Tz (per ) Tj 1.205556 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 715.072165 Tm 7 0 Td 53.877315 Tz (provided ) Tj 2.916667 0 Td 45.37037 Tz (that ) Tj 1.4 0 Td 64.814815 Tz (when ) Tj 1.886111 0 Td 84.259259 Tz (G ) Tj 0.836111 0 Td 40.509259 Tz (is ) Tj 0.797222 0 Td 50.957854 Tz (N,N-bis\(2-pyridinylmethyl\)-2, ) Tj 51.428571 0 0 51.428571 0 673.408322 Tm 6.261111 0 Td 52.451989 Tz (2'-bipyridine-6-methanamine ) Tj 8.769444 0 Td 58.009259 Tz (\(DPA-Bpy\), ) Tj 3.713889 0 Td 106.944444 Tz (M ) Tj 0.894444 0 Td 38.888889 Tz (is ) Tj 0.777778 0 Td 49.691358 Tz (not ) Tj 1.166667 0 Td 54.012346 Tz (Ru. ) Tj 51.428571 0 0 51.428571 0 630.045743 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.836111 0 Td 46.759259 Tz (certain ) Tj 2.236111 0 Td 56.712963 Tz (embodiments, ) Tj 4.375 0 Td 84.259259 Tz (G ) Tj 0.797222 0 Td 37.268519 Tz (is ) Tj 0.719444 0 Td 51.592593 Tz (N,N-bis\(isoquinolin-1-yl\) ) Tj 51.428571 0 0 51.428571 0 591.152941 Tm 6.261111 0 Td 51.311728 Tz (methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 15.711111 0 Td 72.916667 Tz (\(DIQ ) Tj 51.428571 0 0 51.428571 0 546.261965 Tm 6.280556 0 Td 53.148148 Tz (Bpy\). ) Tj 1.963889 0 Td 48.611111 Tz (In ) Tj 0.913889 0 Td 51.203704 Tz (other ) Tj 1.808333 0 Td 57.253086 Tz (embodiments, ) Tj 4.433333 0 Td 87.5 Tz (G ) Tj 0.894444 0 Td 37.268519 Tz (is ) Tj 0.797222 0 Td 55.25463 Tz (N,N-bis\(2-pyridinylm ) Tj 51.428571 0 0 51.428571 0 509 Tm 6.261111 0 Td 50.861626 Tz (ethyl\)-2,2'-bipyridine-6-methanamine ) Tj 11.219444 0 Td 58.009259 Tz (\(DPA-Bpy\). ) Tj 48.571429 0 0 48.571429 0 461 Tm 7.432353 0 Td 49.754902 Tz (In ) Tj 0.885294 0 Td 50 Tz (certain ) Tj 2.408824 0 Td 60.334967 Tz (embodiments, ) Tj 4.632353 0 Td 53.75817 Tz (the ) Tj 1.235294 0 Td 48.039216 Tz (transition ) Tj 3.232353 0 Td 56.27451 Tz (metal ) Tj 1.997059 0 Td 60.04902 Tz (of ) Tj 0.926471 0 Td 51.470588 Tz (the ) Tj 1.235294 0 Td 62.908497 Tz (for ) Tj 51.428571 0 0 51.428571 0 418 Tm 6.261111 0 Td 59.953704 Tz (mula ) Tj 1.691667 0 Td 39.969136 Tz (\(I\) ) Tj 0.991667 0 Td 38.888889 Tz (is ) Tj 0.719444 0 Td 56.17284 Tz (Co, ) Tj 1.263889 0 Td 49.691358 Tz (Ni, ) Tj 1.205556 0 Td 54.012346 Tz (Ru, ) Tj 1.205556 0 Td 53.472222 Tz (or ) Tj 0.894444 0 Td 47.530864 Tz (Fe. ) Tj 48.571429 0 0 48.571429 0 378 Tm 7.432353 0 Td 52.328431 Tz (Suitable ) Tj 2.738235 0 Td 56.045752 Tz (anions ) Tj 2.305882 0 Td 50.326797 Tz (for ) Tj 1.173529 0 Td 56.045752 Tz (use ) Tj 1.235294 0 Td 54.901961 Tz (as ) Tj 0.926471 0 Td 92.647059 Tz (X ) Tj 0.844118 0 Td 50.612745 Tz (include, ) Tj 2.697059 0 Td 58.333333 Tz (such ) Tj 1.647059 0 Td 46.895425 Tz (as, ) Tj 1.111765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 49.754902 Tz (fluorine ) Tj 51.428571 0 0 51.428571 0 335 Tm 6.261111 0 Td 46.180556 Tz (ion, ) Tj 1.341667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 49.421296 Tz (chlorine ) Tj 2.625 0 Td 49.691358 Tz (ion ) Tj 1.127778 0 Td 35.648148 Tz (\(i.e., ) Tj 1.536111 0 Td 59.143519 Tz (Cl\), ) Tj 1.633333 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 58.333333 Tz (bromine ) Tj 2.663889 0 Td 46.180556 Tz (ion, ) Tj 1.322222 0 Td 55.092593 Tz (an ) Tj 0.933333 0 Td 50.771605 Tz (iodine ) Tj 2.061111 0 Td 44.560185 Tz (ion, ) Tj 51.428571 0 0 51.428571 0 295.824769 Tm 6.261111 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 45.37037 Tz (Sulfide ) Tj 2.177778 0 Td 45.37037 Tz (ion, ) Tj 1.322222 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 53.796296 Tz (oxide ) Tj 1.866667 0 Td 44.560185 Tz (ion, ) Tj 1.322222 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 54.73251 Tz (hydroxide ) Tj 3.188889 0 Td 46.180556 Tz (ion, ) Tj 1.322222 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 53.703704 Tz (hydride ) Tj 2.508333 0 Td 44.560185 Tz (ion, ) Tj 51.428571 0 0 51.428571 0 253.786632 Tm 6.261111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 42.12963 Tz (Sulfite ) Tj 1.963889 0 Td 46.180556 Tz (ion, ) Tj 1.302778 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 55.092593 Tz (phosphate ) Tj 3.188889 0 Td 45.37037 Tz (ion, ) Tj 1.302778 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 54.62963 Tz (cyanide ) Tj 2.508333 0 Td 44.560185 Tz (ion, ) Tj 1.302778 0 Td 56.712963 Tz (an ) Tj 0.875 0 Td 48.611111 Tz (acetate ) Tj 2.275 0 Td 44.560185 Tz (ion, ) Tj 51.428571 0 0 51.428571 0 211.586685 Tm 6.261111 0 Td 55.092593 Tz (a ) Tj 0.680556 0 Td 52.211934 Tz (carbonate ) Tj 3.169444 0 Td 46.180556 Tz (ion, ) Tj 1.458333 0 Td 51.851852 Tz (a ) Tj 0.661111 0 Td 46.296296 Tz (sulfate ) Tj 2.294444 0 Td 46.180556 Tz (ion, ) Tj 1.438889 0 Td 58.333333 Tz (a ) Tj 0.7 0 Td 43.981481 Tz (nitrate ) Tj 2.216667 0 Td 44.560185 Tz (ion, ) Tj 1.419444 0 Td 58.333333 Tz (a ) Tj 0.680556 0 Td 57.928241 Tz (hydrogen ) Tj 51.428571 0 0 51.428571 0 170.589711 Tm 6.261111 0 Td 52.572016 Tz (carbonate ) Tj 3.188889 0 Td 44.560185 Tz (ion, ) Tj 1.4 0 Td 58.333333 Tz (a ) Tj 0.641667 0 Td 46.180556 Tz (trifluoroacetate ) Tj 4.783333 0 Td 45.37037 Tz (ion, ) Tj 1.4 0 Td 58.333333 Tz (an ) Tj 1.05 0 Td 52.256944 Tz (2-ethylhexanoate ) Tj 40 0 0 40 0 1310 Tm 29.8 0 Td 37.5 Tz (\(I\) ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.786486 0 Td 72.522523 Tz (8 ) Tj 51.428571 0 0 51.428571 0 2914.747815 Tm 25.2 0 Td 46.180556 Tz (ion, ) Tj 1.341667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 51.557239 Tz (thiocyanide ) Tj 3.655556 0 Td 44.560185 Tz (ion, ) Tj 1.322222 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 50.636574 Tz (trifluoromethane ) Tj 5.075 0 Td 49.691358 Tz (Sulfonate ) Tj 2.916667 0 Td 45.37037 Tz (ion, ) Tj 1.322222 0 Td 59.953704 Tz (an ) Tj 51.428571 0 0 51.428571 0 2873.215496 Tm 25.2 0 Td 48.070988 Tz (acetyl ) Tj 1.963889 0 Td 48.935185 Tz (acetonate, ) Tj 3.15 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 48.229847 Tz (tetrafuloroborate ) Tj 5.172222 0 Td 44.560185 Tz (ion, ) Tj 1.322222 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 56.25 Tz (hexafluorophos ) Tj 51.428571 0 0 51.428571 0 2826.836129 Tm 25.2 0 Td 52.5 Tz (phate ) Tj 1.847222 0 Td 49.691358 Tz (ion ) Tj 1.225 0 Td 36.188272 Tz (\(i.e., ) Tj 1.594444 0 Td 75.347222 Tz (PF\), ) Tj 2.061111 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 50.326797 Tz (tetrafluoroborate ) Tj 5.405556 0 Td 50.771605 Tz (ion ) Tj 1.225 0 Td 35.108025 Tz (\(i.e., ) Tj 1.613889 0 Td 76.967593 Tz (BF\), ) Tj 51.428571 0 0 51.428571 0 2787.478908 Tm 25.2 0 Td 58.333333 Tz (and ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 52.614379 Tz (tetraphenylborate ) Tj 5.619444 0 Td 44.560185 Tz (ion. ) Tj 51.428571 0 0 51.428571 0 2726.920635 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.836111 0 Td 46.759259 Tz (certain ) Tj 2.177778 0 Td 57.253086 Tz (embodiments, ) Tj 4.355556 0 Td 87.5 Tz (X ) Tj 0.777778 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 49.016204 Tz (selected ) Tj 2.566667 0 Td 58.333333 Tz (from ) Tj 1.633333 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 56.388889 Tz (group ) Tj 1.925 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 2685.325365 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.719444 0 Td 49.826389 Tz (chloride ) Tj 2.8 0 Td 44.560185 Tz (ion, ) Tj 1.497222 0 Td 55.092593 Tz (a ) Tj 0.7 0 Td 53.38694 Tz (hexafluorophosphate ) Tj 6.494444 0 Td 45.37037 Tz (ion, ) Tj 1.497222 0 Td 51.851852 Tz (a ) Tj 0.7 0 Td 45.959596 Tz (tetrafluoro ) Tj 48.571429 0 0 48.571429 0 2641 Tm 26.661765 0 Td 54.330065 Tz (borate ) Tj 2.285294 0 Td 48.039216 Tz (ion, ) Tj 1.461765 0 Td 61.764706 Tz (a ) Tj 0.658824 0 Td 61.764706 Tz (bromide ) Tj 2.923529 0 Td 47.181373 Tz (ion, ) Tj 1.461765 0 Td 60.04902 Tz (an ) Tj 1.070588 0 Td 53.186275 Tz (iodide ) Tj 2.244118 0 Td 48.039216 Tz (ion, ) Tj 1.461765 0 Td 61.764706 Tz (an ) Tj 1.070588 0 Td 57.647059 Tz (oxide ) Tj 2.058824 0 Td 48.039216 Tz (ion, ) Tj 1.482353 0 Td 58.333333 Tz (a ) Tj 51.428571 0 0 51.428571 0 2600.277641 Tm 25.180556 0 Td 55.092593 Tz (hydroxide ) Tj 3.130556 0 Td 46.180556 Tz (ion, ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 53.703704 Tz (hydride ) Tj 2.411111 0 Td 46.180556 Tz (ion, ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.505556 0 Td 54.73251 Tz (phosphate ) Tj 3.130556 0 Td 45.37037 Tz (ion, ) Tj 1.263889 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 53.703704 Tz (cyanide ) Tj 2.430556 0 Td 44.560185 Tz (ion, ) Tj 48.571429 0 0 48.571429 0 2553 Tm 26.682353 0 Td 60.04902 Tz (an ) Tj 0.947059 0 Td 50.980392 Tz (acetate ) Tj 2.347059 0 Td 48.039216 Tz (ion, ) Tj 1.358824 0 Td 61.764706 Tz (a ) Tj 0.576471 0 Td 55.664488 Tz (carbonate ) Tj 3.232353 0 Td 46.323529 Tz (ion, ) Tj 1.358824 0 Td 58.333333 Tz (a ) Tj 0.576471 0 Td 48.529412 Tz (Sulfate ) Tj 2.244118 0 Td 48.897059 Tz (ion, ) Tj 1.379412 0 Td 58.333333 Tz (a ) Tj 0.576471 0 Td 46.078431 Tz (nitrate ) Tj 2.182353 0 Td 47.181373 Tz (ion, ) Tj 1.358824 0 Td 58.333333 Tz (a ) Tj 51.428571 0 0 51.428571 0 2512.969843 Tm 25.2 0 Td 52.256944 Tz (2-ethylhexanoate ) Tj 5.191667 0 Td 46.180556 Tz (ion, ) Tj 1.302778 0 Td 56.712963 Tz (an ) Tj 0.894444 0 Td 48.070988 Tz (acetyl ) Tj 1.925 0 Td 48.611111 Tz (acetonate, ) Tj 3.111111 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 49.494949 Tz (tetraphenyl ) Tj 40 0 0 40 0 2472 Tm 32.375 0 Td 65.972222 Tz (borate ) Tj 2.7 0 Td 57.291667 Tz (ion. ) Tj 51.428571 0 0 51.428571 0 2409.734417 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 47.222222 Tz (certain ) Tj 2.313889 0 Td 59.217172 Tz (embodiments ) Tj 4.2 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 48.611111 Tz (the ) Tj 1.225 0 Td 51.851852 Tz (metal ) Tj 1.886111 0 Td 57.613169 Tz (complexes ) Tj 3.441667 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 2364 Tm 25.2 0 Td 54.62963 Tz (formula ) Tj 2.488889 0 Td 37.268519 Tz (\(I\), ) Tj 1.088889 0 Td 87.5 Tz (X ) Tj 0.719444 0 Td 37.268519 Tz (is ) Tj 0.661111 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 61.574074 Tz (same ) Tj 1.652778 0 Td 49.691358 Tz (for ) Tj 1.011111 0 Td 55.902778 Tz (each ) Tj 1.536111 0 Td 53.472222 Tz (occurrence ) Tj 3.344444 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 64.814815 Tz (Cl. ) Tj 1.4 0 Td 50.231481 Tz (In ) Tj 48.571429 0 0 48.571429 0 2323 Tm 26.682353 0 Td 53.529412 Tz (other ) Tj 1.832353 0 Td 60.04902 Tz (embodiments, ) Tj 4.55 0 Td 96.078431 Tz (X ) Tj 0.823529 0 Td 41.176471 Tz (is ) Tj 0.741176 0 Td 53.75817 Tz (the ) Tj 1.194118 0 Td 66.053922 Tz (same ) Tj 1.832353 0 Td 51.470588 Tz (for ) Tj 1.132353 0 Td 58.333333 Tz (each ) Tj 1.647059 0 Td 56.617647 Tz (occurrence ) Tj 3.623529 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 2277 Tm 25.2 0 Td 38.888889 Tz (is ) Tj 0.719444 0 Td 86.419753 Tz (PF. ) Tj 51.428571 0 0 51.428571 0 2225.299742 Tm 25.9 0 Td 51.851852 Tz (Y, ) Tj 0.855556 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 54.282407 Tz (each ) Tj 1.555556 0 Td 50.673401 Tz (occurrence, ) Tj 3.558333 0 Td 52.599715 Tz (independently ) Tj 4.336111 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 55.092593 Tz (halogen ) Tj 2.527778 0 Td 55.740741 Tz (group ) Tj 51.428571 0 0 51.428571 0 2178.114839 Tm 25.219444 0 Td 51.203704 Tz (\(such ) Tj 1.711111 0 Td 44.290123 Tz (as, ) Tj 1.030556 0 Td 40.509259 Tz (F, ) Tj 0.661111 0 Td 48.611111 Tz (Cl, ) Tj 1.108333 0 Td 45.37037 Tz (Br, ) Tj 1.05 0 Td 37.268519 Tz (I\) ) Tj 0.602778 0 Td 55.092593 Tz (or ) Tj 0.816667 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 53.796296 Tz (water ) Tj 1.808333 0 Td 50 Tz (moiety. ) Tj 2.333333 0 Td 46.990741 Tz (In ) Tj 0.758333 0 Td 59.41358 Tz (one ) Tj 1.244444 0 Td 57.449495 Tz (embodiment, ) Tj 52.857143 0 0 52.857143 0 2133 Tm 24.5 0 Td 91.441441 Tz (Y ) Tj 0.737838 0 Td 37.837838 Tz (is ) Tj 0.7 0 Td 47.297297 Tz (C1. ) Tj 1.116216 0 Td 47.297297 Tz (In ) Tj 0.794595 0 Td 51.351351 Tz (another ) Tj 2.364865 0 Td 56.183456 Tz (embodiment, ) Tj 3.897297 0 Td 88.288288 Tz (Y ) Tj 0.756757 0 Td 37.837838 Tz (is ) Tj 0.737838 0 Td 58.333333 Tz (H.O. ) Tj 51.428571 0 0 51.428571 0 2078 Tm 25.938889 0 Td 71.296296 Tz (L ) Tj 0.583333 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 54.166667 Tz (formula ) Tj 2.488889 0 Td 39.969136 Tz (\(I\) ) Tj 0.894444 0 Td 40.509259 Tz (is ) Tj 0.680556 0 Td 46.450617 Tz (either ) Tj 1.808333 0 Td 52.391975 Tz (absent ) Tj 2.061111 0 Td 53.472222 Tz (or ) Tj 0.777778 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 47.222222 Tz (neutral ) Tj 2.216667 0 Td 51.851852 Tz (molecule. ) Tj 51.428571 0 0 51.428571 0 2036.950131 Tm 25.219444 0 Td 59.143519 Tz (Examples ) Tj 3.247222 0 Td 55.092593 Tz (of ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 46.759259 Tz (neutral ) Tj 2.411111 0 Td 54.6875 Tz (molecule ) Tj 2.994444 0 Td 48.206019 Tz (include, ) Tj 2.683333 0 Td 49.691358 Tz (for ) Tj 1.225 0 Td 54.6875 Tz (example, ) Tj 51.428571 0 0 51.428571 0 1991.963899 Tm 25.2 0 Td 50.854701 Tz (alkyl-cyanide ) Tj 4.180556 0 Td 51.851852 Tz (\(such ) Tj 1.769444 0 Td 45.37037 Tz (as, ) Tj 1.011111 0 Td 44.212963 Tz (acetonitrile\), ) Tj 3.947222 0 Td 49.151235 Tz (water, ) Tj 2.022222 0 Td 52.932099 Tz (methanol, ) Tj 3.052778 0 Td 61.574074 Tz (etha ) Tj 51.428571 0 0 51.428571 0 1952.742092 Tm 25.2 0 Td 46.180556 Tz (nol, ) Tj 1.4 0 Td 50.378788 Tz (n-propanol, ) Tj 3.616667 0 Td 50.05144 Tz (isopropyl ) Tj 2.975 0 Td 48.611111 Tz (alcohol, ) Tj 2.605556 0 Td 53.376906 Tz (2-methoxyethanol, ) Tj 5.794444 0 Td 44.560185 Tz (1.1- ) Tj 51.428571 0 0 51.428571 0 1908.782772 Tm 25.2 0 Td 53.877315 Tz (dimethyl ) Tj 2.955556 0 Td 48.611111 Tz (ethanol, ) Tj 2.702778 0 Td 51.851852 Tz (ethylene ) Tj 2.838889 0 Td 47.685185 Tz (glycol, ) Tj 2.411111 0 Td 53.596866 Tz (N,N'-dimethyl ) Tj 4.569444 0 Td 66.111111 Tz (forma ) Tj 51.428571 0 0 51.428571 0 1864.645356 Tm 25.2 0 Td 53.796296 Tz (mide, ) Tj 2.080556 0 Td 53.596866 Tz (N,N'-dimethyl ) Tj 4.608333 0 Td 52.175926 Tz (acetamide, ) Tj 3.558333 0 Td 52.133655 Tz (N-methyl-2-pyrrolidone, ) Tj 51.428571 0 0 51.428571 0 1817.289697 Tm 25.2 0 Td 53.877315 Tz (dimethyl ) Tj 2.877778 0 Td 47.638889 Tz (sulfoxide, ) Tj 3.15 0 Td 49.826389 Tz (acetone, ) Tj 2.663889 0 Td 52.441077 Tz (chloroform, ) Tj 3.733333 0 Td 44.373219 Tz (acetonitrile, ) Tj 3.752778 0 Td 71.296296 Tz (ben ) Tj 51.428571 0 0 51.428571 0 1777.772512 Tm 25.2 0 Td 43.425926 Tz (Zonitrile, ) Tj 2.8 0 Td 43.75 Tz (triethyl ) Tj 2.313889 0 Td 54.552469 Tz (amine, ) Tj 2.158333 0 Td 48.611111 Tz (pyridine, ) Tj 2.838889 0 Td 49.691358 Tz (pyrazine, ) Tj 2.897222 0 Td 52.777778 Tz (diazabicyclo2. ) Tj 51.428571 0 0 51.428571 0 1733.590244 Tm 25.2 0 Td 48.905724 Tz (2.2]octane, ) Tj 3.597222 0 Td 46.383102 Tz (4,4'-bipyridine, ) Tj 4.822222 0 Td 48.813657 Tz (tetrahydrofuran, ) Tj 5.075 0 Td 47.685185 Tz (diethyl ) Tj 2.372222 0 Td 43.75 Tz (ether, ) Tj 51.428571 0 0 51.428571 0 1688.286064 Tm 25.2 0 Td 57.253086 Tz (dimethoxy ) Tj 3.325 0 Td 50 Tz (ethane, ) Tj 2.372222 0 Td 52.146465 Tz (methylethyl ) Tj 3.675 0 Td 44.830247 Tz (ether, ) Tj 1.847222 0 Td 59.41358 Tz (and ) Tj 1.4 0 Td 48.881173 Tz (1,4-dioxane, ) Tj 3.791667 0 Td 59.41358 Tz (and ) Tj 52.857143 0 0 52.857143 0 1642.847458 Tm 24.518919 0 Td 48.243243 Tz (preferably ) Tj 3.140541 0 Td 46.246246 Tz (water, ) Tj 1.948649 0 Td 51.151151 Tz (methanol, ) Tj 2.97027 0 Td 47.297297 Tz (ethanol, ) Tj 2.478378 0 Td 49.399399 Tz (isopropyl ) Tj 2.875676 0 Td 47.297297 Tz (alcohol, ) Tj 2.478378 0 Td 60.960961 Tz (eth ) Tj 51.428571 0 0 51.428571 0 1602.257325 Tm 25.180556 0 Td 53.148148 Tz (ylene ) Tj 2.119444 0 Td 47.685185 Tz (glycol, ) Tj 2.547222 0 Td 53.596866 Tz (N,N'-dimethyl ) Tj 4.744444 0 Td 55.416667 Tz (formamide, ) Tj 3.908333 0 Td 53.347578 Tz (N,N'-dimethyl ) Tj 51.428571 0 0 51.428571 0 1556.566265 Tm 25.2 0 Td 52.175926 Tz (acetamide, ) Tj 3.577778 0 Td 52.133655 Tz (N-methyl-2-pyrrolidone, ) Tj 7.641667 0 Td 52.441077 Tz (chloroform, ) Tj 3.888889 0 Td 56.018519 Tz (acetoni ) Tj 51.428571 0 0 51.428571 0 1512.7543 Tm 25.180556 0 Td 37.808642 Tz (trile, ) Tj 1.652778 0 Td 46.616809 Tz (benzonitrile, ) Tj 3.927778 0 Td 43.75 Tz (triethyl ) Tj 2.372222 0 Td 54.552469 Tz (amine, ) Tj 2.216667 0 Td 48.611111 Tz (pyridine, ) Tj 2.877778 0 Td 50.05144 Tz (pyrazine, ) Tj 2.994444 0 Td 59.953704 Tz (diaz ) Tj 51.428571 0 0 51.428571 0 1473 Tm 25.2 0 Td 51.388889 Tz (abicyclo2.2.2]octane, ) Tj 7.388889 0 Td 46.383102 Tz (4,4'-bipyridine, ) Tj 5.347222 0 Td 49.016204 Tz (tetrahydrofuran, ) Tj 51.428571 0 0 51.428571 0 1424.518812 Tm 25.2 0 Td 57.253086 Tz (dimethoxy ) Tj 3.325 0 Td 50 Tz (ethane, ) Tj 2.333333 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 49.421296 Tz (1,4-dioxane. ) Tj 52.857143 0 0 52.857143 0 1366.920439 Tm 25.237838 0 Td 47.297297 Tz (In ) Tj 0.851351 0 Td 56.756757 Tz (one ) Tj 1.267568 0 Td 56.470106 Tz (embodiment, ) Tj 4.010811 0 Td 66.216216 Tz (L ) Tj 0.681081 0 Td 42.567568 Tz (in ) Tj 0.794595 0 Td 48.348348 Tz (the ) Tj 1.116216 0 Td 53.153153 Tz (formula ) Tj 2.535135 0 Td 38.888889 Tz (\(I\) ) Tj 0.964865 0 Td 37.837838 Tz (is ) Tj 0.737838 0 Td 68.975225 Tz (\(C\)alkyl ) Tj 51.428571 0 0 51.428571 0 1324.833948 Tm 25.2 0 Td 54.166667 Tz (cyanide ) Tj 2.508333 0 Td 40.509259 Tz (\(e.g., ) Tj 1.691667 0 Td 44.373219 Tz (acetonitrile; ) Tj 3.733333 0 Td 79.62963 Tz (CHCN\). ) Tj 51.428571 0 0 51.428571 0 1266 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.836111 0 Td 58.333333 Tz (one ) Tj 1.283333 0 Td 57.449495 Tz (embodiment, ) Tj 4.063889 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 54.62963 Tz (formula ) Tj 2.566667 0 Td 39.969136 Tz (\(I\) ) Tj 0.972222 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 43.75 Tz (0. ) Tj 0.797222 0 Td 48.611111 Tz (In ) Tj 0.816667 0 Td 53.240741 Tz (another ) Tj 48.571429 0 0 48.571429 0 1224 Tm 26.682353 0 Td 60.828877 Tz (embodiment, ) Tj 4.302941 0 Td 58.333333 Tz (a ) Tj 0.597059 0 Td 41.176471 Tz (is ) Tj 0.823529 0 Td 41.176471 Tz (1. ) Tj 51.428571 0 0 51.428571 0 1168.540682 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.913889 0 Td 45.775463 Tz (specific ) Tj 2.508333 0 Td 57.253086 Tz (embodiments, ) Tj 4.433333 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 50.411523 Tz (invention ) Tj 3.033333 0 Td 52.256944 Tz (provides ) Tj 2.838889 0 Td 49.691358 Tz (cobalt ) Tj 51.428571 0 0 51.428571 0 1119.554753 Tm 25.2 0 Td 54.768519 Tz (complexes, ) Tj 3.441667 0 Td 55.092593 Tz (such ) Tj 1.497222 0 Td 43.209877 Tz (as, ) Tj 0.933333 0 Td 63.069801 Tz (Co\(DPA-Bpy\)C1 ) Tj 5.308333 0 Td 48.611111 Tz (\(or ) Tj 0.991667 0 Td 62.789352 Tz (Complex ) Tj 3.227778 0 Td 48.611111 Tz (1\) ) Tj 0.991667 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 1066.719424 Tm 25.394444 0 Td 66.435185 Tz (Co\(DPA-Bpy\)\(Cl\)Cl.\(CHCN\) ) Tj 9.722222 0 Td 50.231481 Tz (\(see ) Tj 1.361111 0 Td 53.472222 Tz (FIG. ) Tj 1.497222 0 Td 45.37037 Tz (1 ) Tj 0.486111 0 Td 48.611111 Tz (for ) Tj 0.991667 0 Td 36.728395 Tz (its ) Tj 0.855556 0 Td 65.354938 Tz (molecu ) Tj 51.428571 0 0 51.428571 0 1010 Tm 25.2 0 Td 44.290123 Tz (lar ) Tj 1.011111 0 Td 44.486532 Tz (structure\). ) Tj 52.857143 0 0 52.857143 0 948.933589 Tm 25.218919 0 Td 62.012012 Tz (The ) Tj 1.305405 0 Td 45.545546 Tz (structure ) Tj 2.62973 0 Td 55.18018 Tz (of ) Tj 0.756757 0 Td 60.880111 Tz (Co\(DPA-Bpy\)C1 ) Tj 5.202703 0 Td 37.837838 Tz (is ) Tj 0.605405 0 Td 52.815315 Tz (provided ) Tj 2.705405 0 Td 48.873874 Tz (as ) Tj 0.794595 0 Td 46.903153 Tz (follows: ) Tj 40 0 0 40 0 353 Tm 49.75 0 Td 56.25 Tz (\(X\), ) Tj 1.428571 0 0 1.428571 0 812 Tm 962.5 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 270 0 obj << /Length 1 >> stream q endstream endobj 271 0 obj << /Length 33014 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 51.428571 0 0 51.428571 0 2914.370518 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.875 0 Td 46.296296 Tz (certain ) Tj 2.216667 0 Td 56.983025 Tz (embodiments, ) Tj 4.394444 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 50.05144 Tz (invention ) Tj 2.994444 0 Td 52.256944 Tz (provides ) Tj 2.8 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2875.099099 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 54.62963 Tz (formula ) Tj 2.547222 0 Td 39.699074 Tz (\(II\) ) Tj 40 0 0 40 0 2144 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 2096 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.947059 0 Td 41.176471 Tz (is ) Tj 0.782353 0 Td 58.333333 Tz (Co, ) Tj 1.358824 0 Td 58.333333 Tz (Ru, ) Tj 1.297059 0 Td 53.75817 Tz (Ni, ) Tj 1.255882 0 Td 53.186275 Tz (or ) Tj 0.885294 0 Td 52.614379 Tz (Fe: ) Tj 52.857143 0 0 52.857143 0 2056.031662 Tm 6.82973 0 Td 48.873874 Tz (R. ) Tj 0.87027 0 Td 48.348348 Tz (for ) Tj 1.059459 0 Td 54.391892 Tz (each ) Tj 1.608108 0 Td 49.303849 Tz (occurrence, ) Tj 3.518919 0 Td 51.178101 Tz (independently ) Tj 4.256757 0 Td 39.414414 Tz (is ) Tj 0.775676 0 Td 52.027027 Tz (H. ) Tj 0.908108 0 Td 59.90991 Tz (\(C\)alkyl, ) Tj 51.428571 0 0 51.428571 0 2016.786826 Tm 6.261111 0 Td 52.932099 Tz (cyano, ) Tj 2.080556 0 Td 44.074074 Tz (aryl, ) Tj 1.477778 0 Td 50.925926 Tz (benzyl, ) Tj 2.313889 0 Td 55.092593 Tz (amino, ) Tj 2.197222 0 Td 39.293981 Tz (nitrile, ) Tj 2.061111 0 Td 49.691358 Tz (carboxylate, ) Tj 3.733333 0 Td 51.851852 Tz (hydroxyl, ) Tj 3.013889 0 Td 51.851852 Tz (or ) Tj 42.857143 0 0 42.857143 0 1971 Tm 7.513333 0 Td 51.851852 Tz (ester, ) Tj 51.428571 0 0 51.428571 0 1930.468705 Tm 6.980556 0 Td 59.953704 Tz (X, ) Tj 0.952778 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 51.262626 Tz (occurrence, ) Tj 3.616667 0 Td 52.849003 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 49.691358 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 1888.246246 Tm 7 0 Td 58.333333 Tz (Z ) Tj 0.583333 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 54.012346 Tz (per ) Tj 1.225 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex; ) Tj 2.936111 0 Td 59.41358 Tz (and ) Tj 51.428571 0 0 51.428571 0 1847.459504 Tm 6.980556 0 Td 61.574074 Tz (b ) Tj 0.641667 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 52.391975 Tz (anions ) Tj 2.138889 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 1804.92 Tm 7 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 39.537037 Tz (salt, ) Tj 1.438889 0 Td 49.074074 Tz (solvate ) Tj 2.294444 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 52.777778 Tz (hydrate ) Tj 2.469444 0 Td 45.775463 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 1762 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.836111 0 Td 46.759259 Tz (certain ) Tj 2.236111 0 Td 56.712963 Tz (embodiments, ) Tj 4.375 0 Td 103.703704 Tz (M ) Tj 0.875 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 53.703704 Tz (formula ) Tj 2.566667 0 Td 38.888889 Tz (\(II\) ) Tj 1.225 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 57.253086 Tz (Co. ) Tj 1.322222 0 Td 51.851852 Tz (In ) Tj 51.428571 0 0 51.428571 0 1720 Tm 6.261111 0 Td 51.203704 Tz (other ) Tj 1.711111 0 Td 57.253086 Tz (embodiments, ) Tj 4.375 0 Td 106.944444 Tz (M ) Tj 0.913889 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 54.166667 Tz (formula ) Tj 2.547222 0 Td 39.699074 Tz (\(II\) ) Tj 1.225 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 48.611111 Tz (Ni. ) Tj 51.428571 0 0 51.428571 0 1678 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.797222 0 Td 58.333333 Tz (one ) Tj 1.263889 0 Td 57.744108 Tz (embodiment, ) Tj 4.044444 0 Td 58.333333 Tz (Z ) Tj 0.563889 0 Td 42.12963 Tz (in ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 54.62963 Tz (formula ) Tj 2.488889 0 Td 41.319444 Tz (\(II\) ) Tj 1.205556 0 Td 38.888889 Tz (is ) Tj 0.777778 0 Td 35.648148 Tz (1. ) Tj 0.7 0 Td 46.990741 Tz (In ) Tj 0.777778 0 Td 53.240741 Tz (another ) Tj 52.857143 0 0 52.857143 0 1636 Tm 6.091892 0 Td 56.183456 Tz (embodiment, ) Tj 3.897297 0 Td 81.981982 Tz (X ) Tj 0.681081 0 Td 37.837838 Tz (is ) Tj 0.624324 0 Td 50.45045 Tz (the ) Tj 1.040541 0 Td 61.486486 Tz (same ) Tj 1.645946 0 Td 45.195195 Tz (for ) Tj 0.983784 0 Td 53.603604 Tz (each ) Tj 1.494595 0 Td 51.396396 Tz (occurrence ) Tj 3.254054 0 Td 56.756757 Tz (and ) Tj 1.210811 0 Td 36.261261 Tz (is ) Tj 0.662162 0 Td 81.981982 Tz (PF. ) Tj 48.571429 0 0 48.571429 0 1596 Tm 6.65 0 Td 51.470588 Tz (In ) Tj 0.864706 0 Td 38.431373 Tz (still ) Tj 1.420588 0 Td 55.392157 Tz (another ) Tj 2.532353 0 Td 61.452763 Tz (embodiment, ) Tj 4.282353 0 Td 96.078431 Tz (X ) Tj 0.844118 0 Td 41.176471 Tz (is ) Tj 0.761765 0 Td 52.614379 Tz (the ) Tj 1.194118 0 Td 66.053922 Tz (same ) Tj 1.832353 0 Td 50.326797 Tz (for ) Tj 1.132353 0 Td 57.47549 Tz (each ) Tj 1.667647 0 Td 64.509804 Tz (occur ) Tj 52.857143 0 0 52.857143 0 1552 Tm 6.072973 0 Td 51.081081 Tz (rence ) Tj 1.778378 0 Td 57.807808 Tz (and ) Tj 1.267568 0 Td 39.414414 Tz (is ) Tj 0.737838 0 Td 87.237237 Tz (BF. ) Tj 51.428571 0 0 51.428571 0 1516.359116 Tm 7.019444 0 Td 57.253086 Tz (For ) Tj 1.477778 0 Td 55.092593 Tz (example, ) Tj 3.169444 0 Td 48.611111 Tz (the ) Tj 1.4 0 Td 50.771605 Tz (invention ) Tj 3.208333 0 Td 53.06713 Tz (provides ) Tj 3.208333 0 Td 64.225589 Tz (Co\(DPA-Bpy\) ) Tj 52.857143 0 0 52.857143 0 1472.033792 Tm 6.110811 0 Td 69.019019 Tz (\(OH\)\(PF\), ) Tj 4.048649 0 Td 55.005005 Tz (\("complex ) Tj 3.178378 0 Td 77.252252 Tz (2\) ) Tj 1.135135 0 Td 51.238739 Tz (with ) Tj 1.494595 0 Td 48.348348 Tz (the ) Tj 1.097297 0 Td 51.151151 Tz (following ) Tj 2.97027 0 Td 43.828829 Tz (structure: ) Tj 51.428571 0 0 51.428571 0 785.461255 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.302778 0 Td 50.411523 Tz (invention ) Tj 2.877778 0 Td 48.611111 Tz (also ) Tj 1.322222 0 Td 51.851852 Tz (provides ) Tj 2.916667 0 Td 69.189815 Tz (NiCDPA-ABpy\)\(OH\)\(BF\) ) Tj 51.428571 0 0 51.428571 0 742.041825 Tm 6.280556 0 Td 56.532922 Tz (\("complex ) Tj 3.266667 0 Td 52.932099 Tz (3'\) ) Tj 1.186111 0 Td 51.851852 Tz (with ) Tj 1.477778 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 47.530864 Tz (structure ) Tj 2.761111 0 Td 51.49177 Tz (presented ) Tj 3.013889 0 Td 46.990741 Tz (in ) Tj 0.836111 0 Td 53.472222 Tz (FIG. ) Tj 1.575 0 Td 50.231481 Tz (18a. ) Tj 1.438889 0 Td 64.814815 Tz (As ) Tj 51.428571 0 0 51.428571 0 698.487032 Tm 6.280556 0 Td 62.222222 Tz (shown ) Tj 2.197222 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 54.282407 Tz (FIG. ) Tj 1.672222 0 Td 51.851852 Tz (18a, ) Tj 1.575 0 Td 48.611111 Tz (the ) Tj 1.186111 0 Td 59.953704 Tz (Ni ) Tj 1.05 0 Td 50.231481 Tz (center ) Tj 2.1 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 59.722222 Tz (complex ) Tj 2.8 0 Td 58.333333 Tz (3 ) Tj 0.719444 0 Td 38.888889 Tz (is ) Tj 0.816667 0 Td 43.75 Tz (in ) Tj 0.836111 0 Td 61.574074 Tz (an ) Tj 51.428571 0 0 51.428571 0 659.410691 Tm 6.261111 0 Td 50.231481 Tz (octahedral ) Tj 3.344444 0 Td 53.292181 Tz (geometry, ) Tj 3.208333 0 Td 53.472222 Tz (with ) Tj 1.613889 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 49.691358 Tz (6th ) Tj 1.225 0 Td 50.771605 Tz (ligand ) Tj 2.119444 0 Td 55.092593 Tz (being ) Tj 1.963889 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 50.462963 Tz (solvent ) Tj 40 0 0 40 0 622 Tm 8.05 0 Td 67.12963 Tz (molecule. ) Tj 51.428571 0 0 51.428571 0 578.945055 Tm 7 0 Td 47.222222 Tz (Alternatively, ) Tj 4.55 0 Td 50.771605 Tz (the ) Tj 1.477778 0 Td 50.411523 Tz (invention ) Tj 3.325 0 Td 51.851852 Tz (provides ) Tj 3.305556 0 Td 61.574074 Tz (NiCDPA-Bpy\) ) Tj 51.428571 0 0 51.428571 0 533.396476 Tm 6.280556 0 Td 69.135802 Tz (\(H2O\)\(BF\) ) Tj 4.219444 0 Td 48.611111 Tz (as ) Tj 0.836111 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.092593 Tz (complex. ) Tj 51.428571 0 0 51.428571 0 491.677083 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.341667 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 47.800926 Tz (also ) Tj 1.4 0 Td 51.851852 Tz (provides ) Tj 2.722222 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 52.5 Tz (metal ) Tj 1.808333 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 54.62963 Tz (formula ) Tj 51.428571 0 0 51.428571 0 448 Tm 6.280556 0 Td 37.268519 Tz (\(III\): ) Tj 51.428571 0 0 51.428571 0 335.915254 Tm 6.261111 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 38.240741 Tz (salt, ) Tj 1.438889 0 Td 48.611111 Tz (solvate ) Tj 2.275 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 52.314815 Tz (hydrate ) Tj 2.45 0 Td 46.180556 Tz (thereof; ) Tj 40 0 0 40 0 300 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 252 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.926471 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 47.696078 Tz (transition ) Tj 3.191176 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 216.527141 Tm 7 0 Td 84.259259 Tz (G ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.738889 0 Td 51.587302 Tz (N,N-bis\(2-pyridinylmethyl\)-2,2'-bipyridine-6-meth ) Tj 51.428571 0 0 51.428571 0 173.779661 Tm 6.261111 0 Td 58.333333 Tz (anamine ) Tj 3.130556 0 Td 58.333333 Tz (\(DPA-Bpy\), ) Tj 4.219444 0 Td 49.56427 Tz (6'-\(\(bis\(pyridin-2-ylmethyl\)amino\) ) Tj 40 0 0 40 0 395 Tm 29.325 0 Td 38.333333 Tz (\(III\) ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.578378 0 Td 74.099099 Tz (10 ) Tj 51.428571 0 0 51.428571 0 2920.030612 Tm 25.2 0 Td 51.927218 Tz (methyl\)-N,N-dimethyl-2,2'-bipyridin-6-amine ) Tj 15.613889 0 Td 76.967593 Tz (\(DPA ) Tj 51.428571 0 0 51.428571 0 2878 Tm 25.2 0 Td 59.953704 Tz (ABpy\), ) Tj 2.605556 0 Td 50.529101 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 2831.940182 Tm 25.2 0 Td 53.337191 Tz (pyridin-2-yl\)methanamine ) Tj 8.302778 0 Td 57.037037 Tz (\(DIQ-Bpy\), ) Tj 4.063889 0 Td 51.851852 Tz (or ) Tj 1.205556 0 Td 55.092593 Tz (a ) Tj 1.011111 0 Td 48.287037 Tz (derivative ) Tj 48.571429 0 0 48.571429 0 2784 Tm 26.661765 0 Td 49.754902 Tz (thereof; ) Tj 51.428571 0 0 51.428571 0 2742.319042 Tm 25.9 0 Td 51.851852 Tz (Y, ) Tj 0.816667 0 Td 47.530864 Tz (for ) Tj 0.972222 0 Td 55.902778 Tz (each ) Tj 1.516667 0 Td 50.968013 Tz (occurrence, ) Tj 3.558333 0 Td 52.350427 Tz (independently ) Tj 4.277778 0 Td 38.888889 Tz (is ) Tj 0.602778 0 Td 49.074074 Tz (absent, ) Tj 2.236111 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 55.092593 Tz (halogen ) Tj 51.428571 0 0 51.428571 0 2699.780781 Tm 25.2 0 Td 56.388889 Tz (group ) Tj 1.963889 0 Td 50.231481 Tz (or ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 55.092593 Tz (water ) Tj 1.886111 0 Td 51.851852 Tz (moiety; ) Tj 51.428571 0 0 51.428571 0 2653.45706 Tm 25.9 0 Td 59.953704 Tz (X, ) Tj 0.972222 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 50.968013 Tz (occurrence, ) Tj 3.616667 0 Td 52.599715 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (an ) Tj 0.933333 0 Td 50.231481 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 2610.425806 Tm 25.919444 0 Td 90.740741 Tz (m ) Tj 0.836111 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 61.033951 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 2566.476821 Tm 25.919444 0 Td 58.333333 Tz (n ) Tj 0.641667 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 52.932099 Tz (anions ) Tj 2.158333 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.902778 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 2522 Tm 27.464706 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 42.892157 Tz (is ) Tj 0.782353 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 53.186275 Tz (or ) Tj 0.864706 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50.490196 Tz (neutral ) Tj 2.429412 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 2478.917001 Tm 25.919444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 46.296296 Tz (neutral ) Tj 2.236111 0 Td 54.012346 Tz (molecules ) Tj 3.15 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 59.259259 Tz (complex ) Tj 51.428571 0 0 51.428571 0 2436.025907 Tm 25.219444 0 Td 39.429012 Tz (\(e.g., ) Tj 1.711111 0 Td 42.12963 Tz (0, ) Tj 0.855556 0 Td 35.648148 Tz (1, ) Tj 0.7 0 Td 53.472222 Tz (or ) Tj 0.875 0 Td 42.12963 Tz (2\); ) Tj 51.428571 0 0 51.428571 0 2395.087855 Tm 25.919444 0 Td 53.877315 Tz (provided ) Tj 2.916667 0 Td 45.37037 Tz (that ) Tj 1.419444 0 Td 64.00463 Tz (when ) Tj 1.866667 0 Td 84.259259 Tz (G ) Tj 0.855556 0 Td 38.888889 Tz (is ) Tj 0.797222 0 Td 50.957854 Tz (N,N-bis\(2-pyridinylmethyl\)-2, ) Tj 51.428571 0 0 51.428571 0 2352.483791 Tm 25.2 0 Td 52.451989 Tz (2'-bipyridine-6-methanamine ) Tj 8.75 0 Td 57.523148 Tz (\(DPA-Bpy'\), ) Tj 4.413889 0 Td 103.703704 Tz (M ) Tj 0.855556 0 Td 38.888889 Tz (is ) Tj 0.777778 0 Td 49.691358 Tz (not ) Tj 1.166667 0 Td 54.012346 Tz (Ru. ) Tj 51.428571 0 0 51.428571 0 2304.491803 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.816667 0 Td 46.759259 Tz (certain ) Tj 2.216667 0 Td 56.983025 Tz (embodiments, ) Tj 4.316667 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 48.611111 Tz (derivative ) Tj 3.111111 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 53.364198 Tz (N,N-bis\(\(isoqui ) Tj 51.428571 0 0 51.428571 0 2266 Tm 25.2 0 Td 50.591564 Tz (nolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\)methan ) Tj 51.428571 0 0 51.428571 0 2219.48294 Tm 25.2 0 Td 59.62963 Tz (amine ) Tj 2.061111 0 Td 59.773663 Tz (\(DIQ-Bpy\) ) Tj 3.538889 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 51.851852 Tz (a ) Tj 0.602778 0 Td 64.409722 Tz (compound ) Tj 3.363889 0 Td 55.092593 Tz (having ) Tj 2.294444 0 Td 57.253086 Tz (one ) Tj 1.341667 0 Td 50.231481 Tz (or ) Tj 0.875 0 Td 59.41358 Tz (two ) Tj 1.380556 0 Td 69.135802 Tz (Sub ) Tj 51.428571 0 0 51.428571 0 2172.357934 Tm 25.219444 0 Td 44.290123 Tz (stituents ) Tj 2.605556 0 Td 51.851852 Tz (\(such ) Tj 1.75 0 Td 50.231481 Tz (as ) Tj 0.797222 0 Td 51.203704 Tz (those ) Tj 1.769444 0 Td 47.260802 Tz (Substituents ) Tj 3.616667 0 Td 51.49177 Tz (described ) Tj 2.975 0 Td 51.851852 Tz (Supra ) Tj 1.769444 0 Td 47.530864 Tz (for ) Tj 1.030556 0 Td 46.990741 Tz (aryl ) Tj 51.428571 0 0 51.428571 0 2131.526445 Tm 25.2 0 Td 52.777778 Tz (groups\) ) Tj 2.411111 0 Td 58.333333 Tz (on ) Tj 0.875 0 Td 59.41358 Tz (one ) Tj 1.244444 0 Td 51.851852 Tz (or ) Tj 0.758333 0 Td 53.472222 Tz (both ) Tj 1.458333 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.030556 0 Td 49.691358 Tz (pyridinyl ) Tj 2.858333 0 Td 48.611111 Tz (rings ) Tj 1.633333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 53.877315 Tz (2-pyridi ) Tj 51.428571 0 0 51.428571 0 2088.660099 Tm 25.2 0 Td 54.372428 Tz (nylmethyl ) Tj 3.091667 0 Td 51.851852 Tz (groups, ) Tj 2.352778 0 Td 53.472222 Tz (or ) Tj 0.777778 0 Td 61.574074 Tz (on ) Tj 0.913889 0 Td 57.253086 Tz (one ) Tj 1.205556 0 Td 51.851852 Tz (or ) Tj 0.738889 0 Td 54.282407 Tz (both ) Tj 1.497222 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 48.971193 Tz (pyridinyl ) Tj 2.838889 0 Td 47.962963 Tz (rings ) Tj 1.633333 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 2044.321513 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 48.611111 Tz (6-\(pyridin-2-yl\)pyridine ) Tj 7.155556 0 Td 52.391975 Tz (group. ) Tj 2.119444 0 Td 48.611111 Tz (In ) Tj 0.777778 0 Td 46.759259 Tz (certain ) Tj 2.158333 0 Td 56.983025 Tz (embodiments, ) Tj 51.428571 0 0 51.428571 0 2005.118192 Tm 25.2 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 48.611111 Tz (derivative ) Tj 3.15 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 50.925926 Tz (N,N-bis\(2-pyridinylmethyl\)-2,2'-bipyridine ) Tj 51.428571 0 0 51.428571 0 1962.502945 Tm 25.219444 0 Td 57.834758 Tz (6-methanamine ) Tj 4.822222 0 Td 61.213992 Tz (\(DPA-Bpy\) ) Tj 3.616667 0 Td 53.472222 Tz (or ) Tj 0.952778 0 Td 47.916667 Tz (6'-\(\(bis\(pyridin-2-ylmethyl\) ) Tj 51.428571 0 0 51.428571 0 1922.146067 Tm 25.2 0 Td 52.579365 Tz (amino\)methyl\)-N,N-dimethyl-2,2'-bipyridin-6-amine ) Tj 15.613889 0 Td 76.967593 Tz (\(DPA ) Tj 51.428571 0 0 51.428571 0 1877.59204 Tm 25.2 0 Td 64.814815 Tz (ABpy\) ) Tj 2.197222 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 64.00463 Tz (compound ) Tj 3.247222 0 Td 55.632716 Tz (having ) Tj 2.197222 0 Td 59.41358 Tz (one ) Tj 1.263889 0 Td 53.472222 Tz (or ) Tj 0.797222 0 Td 60.493827 Tz (two ) Tj 1.322222 0 Td 47.530864 Tz (Substituents ) Tj 3.636111 0 Td 52.5 Tz (\(such ) Tj 51.428571 0 0 51.428571 0 1834.478049 Tm 25.2 0 Td 50.231481 Tz (as ) Tj 0.758333 0 Td 51.851852 Tz (those ) Tj 1.730556 0 Td 47.800926 Tz (Substituents ) Tj 3.616667 0 Td 51.49177 Tz (described ) Tj 2.955556 0 Td 51.851852 Tz (Supra ) Tj 1.75 0 Td 47.530864 Tz (for ) Tj 0.991667 0 Td 47.800926 Tz (aryl ) Tj 1.302778 0 Td 53.240741 Tz (groups\) ) Tj 2.430556 0 Td 58.333333 Tz (on ) Tj 0.875 0 Td 59.41358 Tz (one ) Tj 51.428571 0 0 51.428571 0 1796.168901 Tm 25.2 0 Td 53.472222 Tz (or ) Tj 0.991667 0 Td 53.472222 Tz (both ) Tj 1.672222 0 Td 59.953704 Tz (of ) Tj 1.05 0 Td 48.611111 Tz (the ) Tj 1.263889 0 Td 49.331276 Tz (pyridinyl ) Tj 3.072222 0 Td 47.314815 Tz (rings ) Tj 1.827778 0 Td 59.953704 Tz (of ) Tj 1.011111 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 51.851852 Tz (2-pyridinylmethyl ) Tj 51.428571 0 0 51.428571 0 1752.649718 Tm 25.2 0 Td 51.388889 Tz (groups, ) Tj 2.508333 0 Td 53.472222 Tz (or ) Tj 0.991667 0 Td 58.333333 Tz (on ) Tj 1.069444 0 Td 58.333333 Tz (one ) Tj 1.4 0 Td 51.851852 Tz (or ) Tj 0.952778 0 Td 53.472222 Tz (both ) Tj 1.652778 0 Td 58.333333 Tz (of ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 49.691358 Tz (pyridinyl ) Tj 3.052778 0 Td 47.962963 Tz (rings ) Tj 1.808333 0 Td 58.333333 Tz (of ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1716 Tm 25.2 0 Td 48.752013 Tz (2,2'-bipyridin-6-amine. ) Tj 51.428571 0 0 51.428571 0 1666 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 54.62963 Tz (formula ) Tj 2.625 0 Td 37.808642 Tz (\(III\), ) Tj 1.672222 0 Td 48.611111 Tz (the ) Tj 1.205556 0 Td 44.722222 Tz (transition ) Tj 3.033333 0 Td 53.148148 Tz (metal ) Tj 1.905556 0 Td 59.62963 Tz (\(M\) ) Tj 2.041667 0 Td 57.253086 Tz (can ) Tj 1.341667 0 Td 46.450617 Tz (be, ) Tj 1.166667 0 Td 48.611111 Tz (for ) Tj 52.857143 0 0 52.857143 0 1624.581395 Tm 24.518919 0 Td 53.603604 Tz (example, ) Tj 2.951351 0 Td 53.603604 Tz (Co, ) Tj 1.437838 0 Td 50.45045 Tz (Ru, ) Tj 1.324324 0 Td 48.348348 Tz (Ni, ) Tj 1.248649 0 Td 52.027027 Tz (or ) Tj 1.002703 0 Td 45.195195 Tz (Fe. ) Tj 1.22973 0 Td 47.297297 Tz (In ) Tj 0.927027 0 Td 57.807808 Tz (one ) Tj 1.4 0 Td 56.470106 Tz (embodiment, ) Tj 4.105405 0 Td 81.981982 Tz (G ) Tj 0.908108 0 Td 36.261261 Tz (is ) Tj 51.428571 0 0 51.428571 0 1585.628294 Tm 25.219444 0 Td 61.168981 Tz (DPA-Bpy. ) Tj 3.227778 0 Td 46.990741 Tz (In ) Tj 0.797222 0 Td 53.240741 Tz (another ) Tj 2.430556 0 Td 58.038721 Tz (embodiment, ) Tj 4.063889 0 Td 87.5 Tz (G ) Tj 0.777778 0 Td 42.12963 Tz (is ) Tj 0.777778 0 Td 63.374486 Tz (DPA-ABpy. ) Tj 48.571429 0 0 48.571429 0 1542 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 0.947059 0 Td 50 Tz (certain ) Tj 2.45 0 Td 60.04902 Tz (embodiments, ) Tj 4.632353 0 Td 99.509804 Tz (Y ) Tj 0.885294 0 Td 41.176471 Tz (is ) Tj 0.844118 0 Td 50.490196 Tz (absent. ) Tj 2.511765 0 Td 49.754902 Tz (In ) Tj 0.947059 0 Td 54.215686 Tz (other ) Tj 1.914706 0 Td 71.486928 Tz (embodi ) Tj 51.428571 0 0 51.428571 0 1501.391061 Tm 25.2 0 Td 52.932099 Tz (ments, ) Tj 2.138889 0 Td 87.5 Tz (Y ) Tj 0.758333 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 55.092593 Tz (water ) Tj 1.905556 0 Td 49.537037 Tz (moiety. ) Tj 51.428571 0 0 51.428571 0 1457.553846 Tm 25.9 0 Td 90.740741 Tz (X ) Tj 0.7 0 Td 57.253086 Tz (can ) Tj 1.166667 0 Td 58.333333 Tz (be ) Tj 0.836111 0 Td 58.333333 Tz (any ) Tj 1.205556 0 Td 50.771605 Tz (ion ) Tj 1.069444 0 Td 51.851852 Tz (as ) Tj 0.758333 0 Td 58.981481 Tz (above ) Tj 1.925 0 Td 47.43266 Tz (delineated. ) Tj 3.344444 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 58.333333 Tz (one ) Tj 1.205556 0 Td 57.449495 Tz (embodiment, ) Tj 51.428571 0 0 51.428571 0 1415 Tm 25.2 0 Td 84.259259 Tz (X ) Tj 0.7 0 Td 38.888889 Tz (is ) Tj 0.641667 0 Td 85.339506 Tz (PF. ) Tj 1.75 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 52.777778 Tz (another ) Tj 2.352778 0 Td 57.744108 Tz (embodiment, ) Tj 3.966667 0 Td 84.259259 Tz (X ) Tj 0.7 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 87.5 Tz (BF. ) Tj 1.808333 0 Td 46.180556 Tz (Further, ) Tj 2.391667 0 Td 90.740741 Tz (X ) Tj 0.680556 0 Td 58.333333 Tz (can ) Tj 40 0 0 40 0 1382 Tm 32.375 0 Td 77.083333 Tz (be ) Tj 1.375 0 Td 62.5 Tz (the ) Tj 1.575 0 Td 80.208333 Tz (same ) Tj 2.375 0 Td 66.666667 Tz (or ) Tj 1.225 0 Td 58.333333 Tz (different ) Tj 3.575 0 Td 62.5 Tz (for ) Tj 1.55 0 Td 69.791667 Tz (each ) Tj 2.15 0 Td 68.333333 Tz (occurrence ) Tj 4.575 0 Td 56.25 Tz (in ) Tj 1.15 0 Td 70.833333 Tz (a ) Tj 0.9 0 Td 67.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1340 Tm 25.2 0 Td 55.497685 Tz (complex. ) Tj 51.428571 0 0 51.428571 0 1294.408696 Tm 25.938889 0 Td 53.619529 Tz (Exemplified ) Tj 3.733333 0 Td 53.148148 Tz (metal ) Tj 1.730556 0 Td 57.973251 Tz (complexes ) Tj 3.305556 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 54.166667 Tz (formula ) Tj 2.469444 0 Td 40.185185 Tz (\(III\) ) Tj 1.361111 0 Td 48.206019 Tz (include, ) Tj 2.488889 0 Td 48.611111 Tz (for ) Tj 51.428571 0 0 51.428571 0 1255.984281 Tm 25.2 0 Td 55.092593 Tz (example, ) Tj 3.091667 0 Td 69.513889 Tz (Ni\(DPA-ABpy\)\(OH\)\(BF\) ) Tj 8.866667 0 Td 56.532922 Tz (\("complex ) Tj 3.286111 0 Td 52.932099 Tz (3\) ) Tj 1.147222 0 Td 60.493827 Tz (and ) Tj 52.857143 0 0 52.857143 0 1211.990196 Tm 24.708108 0 Td 65.103339 Tz (Co\(DPA-ABpy\)\(PF\), ) Tj 6.867568 0 Td 55.355355 Tz (\("complex ) Tj 3.178378 0 Td 44.932432 Tz (4'\), ) Tj 1.286486 0 Td 50.45045 Tz (or ) Tj 0.794595 0 Td 53.603604 Tz (a ) Tj 0.510811 0 Td 38.468468 Tz (salt, ) Tj 1.362162 0 Td 48.198198 Tz (solvate ) Tj 2.213514 0 Td 52.027027 Tz (or ) Tj 51.428571 0 0 51.428571 0 1168.373626 Tm 25.180556 0 Td 52.777778 Tz (hydrate ) Tj 2.391667 0 Td 45.775463 Tz (thereof. ) Tj 2.372222 0 Td 64.814815 Tz (As ) Tj 0.972222 0 Td 42.628205 Tz (illustration, ) Tj 3.519444 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 47.170782 Tz (structure ) Tj 2.702778 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 55.092593 Tz (4 ) Tj 0.525 0 Td 38.888889 Tz (is ) Tj 51.428571 0 0 51.428571 0 1125.372599 Tm 25.180556 0 Td 54.282407 Tz (provided ) Tj 2.780556 0 Td 48.611111 Tz (in ) Tj 0.777778 0 Td 55.092593 Tz (FIG. ) Tj 1.516667 0 Td 51.851852 Tz (18b. ) Tj 1.4 0 Td 66.435185 Tz (As ) Tj 0.972222 0 Td 56.17284 Tz (can ) Tj 1.205556 0 Td 58.333333 Tz (be ) Tj 0.855556 0 Td 53.472222 Tz (seen ) Tj 1.497222 0 Td 57.523148 Tz (from ) Tj 1.613889 0 Td 54.282407 Tz (FIG. ) Tj 1.536111 0 Td 51.041667 Tz (18b, ) Tj 1.419444 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 69.675926 Tz (Co ) Tj 51.428571 0 0 51.428571 0 1089.487273 Tm 25.2 0 Td 50.231481 Tz (center ) Tj 1.963889 0 Td 43.75 Tz (in ) Tj 0.738889 0 Td 59.259259 Tz (complex ) Tj 2.663889 0 Td 61.574074 Tz (4 ) Tj 0.525 0 Td 52.391975 Tz (adopts ) Tj 2.080556 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 46.990741 Tz (trigonal ) Tj 2.430556 0 Td 53.324916 Tz (bipyramidal ) Tj 3.694444 0 Td 52.932099 Tz (geometry. ) Tj 51.428571 0 0 51.428571 0 1044.082667 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 49.421296 Tz (also ) Tj 1.438889 0 Td 52.256944 Tz (provides ) Tj 2.8 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 57.613169 Tz (complexes ) Tj 3.383333 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1001.422222 Tm 25.2 0 Td 58.333333 Tz (form ) Tj 1.75 0 Td 58.333333 Tz (of ) Tj 0.972222 0 Td 39.969136 Tz (salts, ) Tj 1.808333 0 Td 46.090535 Tz (Solvates, ) Tj 2.838889 0 Td 48.971193 Tz (hydrates, ) Tj 2.994444 0 Td 51.851852 Tz (or ) Tj 0.952778 0 Td 50.854701 Tz (stereoisomers ) Tj 4.316667 0 Td 58.333333 Tz (of ) Tj 0.933333 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 960.440154 Tm 25.2 0 Td 53.796296 Tz (metal ) Tj 1.886111 0 Td 56.893004 Tz (complexes ) Tj 3.305556 0 Td 51.851852 Tz (as ) Tj 0.894444 0 Td 51.131687 Tz (described ) Tj 2.975 0 Td 47.685185 Tz (herein. ) Tj 51.428571 0 0 51.428571 0 920.214953 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 52.5 Tz (metal ) Tj 1.827778 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 50.05144 Tz (invention ) Tj 2.994444 0 Td 66.975309 Tz (may ) Tj 1.477778 0 Td 56.712963 Tz (form ) Tj 1.594444 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 50.925926 Tz (layered ) Tj 51.428571 0 0 51.428571 0 877.511515 Tm 25.2 0 Td 45.833333 Tz (crystal ) Tj 2.138889 0 Td 39.699074 Tz (lattice. ) Tj 2.158333 0 Td 45.37037 Tz (In ) Tj 0.758333 0 Td 46.759259 Tz (certain ) Tj 2.158333 0 Td 56.712963 Tz (embodiments, ) Tj 4.258333 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 53.148148 Tz (metal ) Tj 1.769444 0 Td 57.613169 Tz (complexes ) Tj 51.428571 0 0 51.428571 0 834.568434 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 50.771605 Tz (invention ) Tj 2.955556 0 Td 47.685185 Tz (further ) Tj 2.177778 0 Td 50.925926 Tz (include ) Tj 2.352778 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 57.253086 Tz (complexes ) Tj 3.325 0 Td 42.12963 Tz (in ) Tj 0.719444 0 Td 58.981481 Tz (which ) Tj 1.983333 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 797.425743 Tm 25.2 0 Td 51.446759 Tz (metal-containing ) Tj 5.191667 0 Td 60.133745 Tz (compound, ) Tj 3.538889 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 58.796296 Tz (example ) Tj 2.702778 0 Td 58.333333 Tz (a ) Tj 0.641667 0 Td 41.319444 Tz (salt ) Tj 1.244444 0 Td 53.472222 Tz (or ) Tj 0.875 0 Td 52.777778 Tz (another ) Tj 51.428571 0 0 51.428571 0 754.212608 Tm 25.2 0 Td 53.796296 Tz (metal ) Tj 1.808333 0 Td 55.902778 Tz (complex, ) Tj 2.877778 0 Td 40.509259 Tz (is ) Tj 0.7 0 Td 51.041667 Tz (incorporated ) Tj 3.888889 0 Td 44.560185 Tz (into ) Tj 1.302778 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 45.833333 Tz (crystal ) Tj 2.138889 0 Td 42.592593 Tz (lattice ) Tj 1.983333 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 710.275649 Tm 25.2 0 Td 53.796296 Tz (metal ) Tj 1.788889 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 47.962963 Tz (invention. ) Tj 3.111111 0 Td 46.990741 Tz (In ) Tj 0.738889 0 Td 43.75 Tz (this ) Tj 1.244444 0 Td 47.314815 Tz (case, ) Tj 1.594444 0 Td 46.990741 Tz (in ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 55.092593 Tz (formulae ) Tj 51.428571 0 0 51.428571 0 669.844444 Tm 25.219444 0 Td 38.888889 Tz (\(I\) ) Tj 0.933333 0 Td 45.37037 Tz (to ) Tj 0.797222 0 Td 38.348765 Tz (\(III\), ) Tj 1.613889 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 50 Tz (portion ) Tj 2.352778 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 49.691358 Tz (cobalt ) Tj 2.002778 0 Td 55.092593 Tz (can ) Tj 1.205556 0 Td 59.953704 Tz (be ) Tj 0.952778 0 Td 51.041667 Tz (replaced ) Tj 2.644444 0 Td 61.574074 Tz (by ) Tj 0.952778 0 Td 51.851852 Tz (other ) Tj 48.571429 0 0 48.571429 0 628 Tm 26.682353 0 Td 56.960784 Tz (metal ) Tj 1.873529 0 Td 49.411765 Tz (ions, ) Tj 1.647059 0 Td 56.617647 Tz (or ) Tj 0.823529 0 Td 50.490196 Tz (further ) Tj 2.285294 0 Td 57.95207 Tz (metalions ) Tj 3.314706 0 Td 58.333333 Tz (can ) Tj 1.235294 0 Td 52.156863 Tz (enter ) Tj 1.729412 0 Td 48.897059 Tz (into ) Tj 1.358824 0 Td 58.333333 Tz (a ) Tj 0.535294 0 Td 65.196078 Tz (more ) Tj 1.729412 0 Td 54.901961 Tz (or ) Tj 0.823529 0 Td 47.181373 Tz (less ) Tj 51.428571 0 0 51.428571 0 587.776772 Tm 25.2 0 Td 57.361111 Tz (pronounced ) Tj 3.694444 0 Td 46.548822 Tz (interaction ) Tj 3.344444 0 Td 52.662037 Tz (with ) Tj 1.516667 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.092593 Tz (complex. ) Tj 51.428571 0 0 51.428571 0 543.715047 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.438889 0 Td 46.666667 Tz (structures ) Tj 3.091667 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 53.148148 Tz (metal ) Tj 1.866667 0 Td 57.973251 Tz (complexes ) Tj 3.422222 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 1.205556 0 Td 50.771605 Tz (invention ) Tj 51.428571 0 0 51.428571 0 505.407125 Tm 25.2 0 Td 69.135802 Tz (may ) Tj 1.633333 0 Td 50.462963 Tz (include ) Tj 2.45 0 Td 56.712963 Tz (asymmetric ) Tj 3.811111 0 Td 53.472222 Tz (carbon ) Tj 2.294444 0 Td 52.932099 Tz (atoms. ) Tj 2.255556 0 Td 52.391975 Tz (Accordingly, ) Tj 4.122222 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 462.286747 Tm 25.2 0 Td 53.703704 Tz (isomers ) Tj 2.430556 0 Td 47.222222 Tz (arising ) Tj 2.158333 0 Td 58.333333 Tz (from ) Tj 1.594444 0 Td 55.092593 Tz (Such ) Tj 1.497222 0 Td 59.41358 Tz (asymmetry ) Tj 3.441667 0 Td 39.969136 Tz (\(e.g., ) Tj 1.633333 0 Td 51.203704 Tz (racemates, ) Tj 3.247222 0 Td 60.763889 Tz (race ) Tj 51.428571 0 0 51.428571 0 418.847619 Tm 25.2 0 Td 59.41358 Tz (mic ) Tj 1.322222 0 Td 49.691358 Tz (mixtures, ) Tj 2.916667 0 Td 48.070988 Tz (single ) Tj 1.925 0 Td 51.58179 Tz (enantiomers, ) Tj 3.927778 0 Td 48.935185 Tz (individual ) Tj 3.15 0 Td 50 Tz (diastereomers, ) Tj 51.428571 0 0 51.428571 0 376.853199 Tm 25.2 0 Td 50.925926 Tz (diastereomeric ) Tj 4.608333 0 Td 50.771605 Tz (mixtures\) ) Tj 3.033333 0 Td 49.691358 Tz (are ) Tj 1.166667 0 Td 52.256944 Tz (included ) Tj 2.819444 0 Td 50.771605 Tz (within ) Tj 2.119444 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 55.092593 Tz (scope ) Tj 1.925 0 Td 58.333333 Tz (of ) Tj 48.571429 0 0 48.571429 0 337 Tm 26.661765 0 Td 46.323529 Tz (this ) Tj 1.379412 0 Td 51.813725 Tz (invention, ) Tj 3.397059 0 Td 52.614379 Tz (unless ) Tj 2.161765 0 Td 52.233115 Tz (indicated ) Tj 3.088235 0 Td 52.5 Tz (otherwise. ) Tj 51.428571 0 0 51.428571 0 295.094028 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 52.5 Tz (metal ) Tj 1.75 0 Td 57.253086 Tz (complexes ) Tj 3.266667 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 50.771605 Tz (invention ) Tj 2.916667 0 Td 57.253086 Tz (can ) Tj 1.186111 0 Td 58.333333 Tz (be ) Tj 0.836111 0 Td 52.662037 Tz (obtained ) Tj 2.663889 0 Td 50.771605 Tz (by: ) Tj 51.428571 0 0 51.428571 0 257.548112 Tm 25.219444 0 Td 50.231481 Tz (synthesizing ) Tj 3.85 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 50.231481 Tz (ligand ) Tj 2.041667 0 Td 52.031893 Tz (organo-chemically; ) Tj 5.891667 0 Td 58.333333 Tz (and ) Tj 1.341667 0 Td 56.17284 Tz (mixing ) Tj 2.236111 0 Td 51.851852 Tz (the ) Tj 51.428571 0 0 51.428571 0 213.109974 Tm 25.2 0 Td 50.771605 Tz (ligand ) Tj 2.022222 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 47.800926 Tz (reaction ) Tj 2.566667 0 Td 53.148148 Tz (agent ) Tj 1.788889 0 Td 45.37037 Tz (that ) Tj 1.322222 0 Td 51.851852 Tz (provides ) Tj 2.702778 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 52.5 Tz (metal ) Tj 1.788889 0 Td 59.953704 Tz (atom ) Tj 1.711111 0 Td 46.990741 Tz (in ) Tj 40 0 0 40 0 176 Tm 32.4 0 Td 70.833333 Tz (a ) Tj 0.75 0 Td 61.979167 Tz (reaction ) Tj 3.325 0 Td 59.895833 Tz (solvent. ) Tj 1.428571 0 0 1.428571 0 1353 Tm 280.7 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 272 0 obj << /Length 1 >> stream q endstream endobj 273 0 obj << /Length 47150 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 14.602778 0 Td 66.435185 Tz (11 ) Tj 51.428571 0 0 51.428571 0 2914.702811 Tm 7.019444 0 Td 53.703704 Tz (Isomers ) Tj 2.527778 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 57.253086 Tz (complexes ) Tj 3.344444 0 Td 61.574074 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 49.691358 Tz (invention ) Tj 2.975 0 Td 54.012346 Tz (can ) Tj 1.263889 0 Td 58.333333 Tz (be ) Tj 51.428571 0 0 51.428571 0 2876.448878 Tm 6.261111 0 Td 51.851852 Tz (obtained ) Tj 2.761111 0 Td 46.990741 Tz (in ) Tj 0.836111 0 Td 46.866097 Tz (Substantially ) Tj 3.927778 0 Td 54.282407 Tz (pure ) Tj 1.555556 0 Td 58.333333 Tz (form ) Tj 1.672222 0 Td 59.953704 Tz (by ) Tj 0.991667 0 Td 45.730453 Tz (classical ) Tj 2.761111 0 Td 49.907407 Tz (separation ) Tj 51.428571 0 0 51.428571 0 2835.635934 Tm 6.241667 0 Td 52.175926 Tz (techniques ) Tj 3.325 0 Td 52.932099 Tz (and/or ) Tj 2.061111 0 Td 61.574074 Tz (by ) Tj 0.972222 0 Td 51.041667 Tz (Stereochemically ) Tj 5.113889 0 Td 49.259259 Tz (controlled ) Tj 3.169444 0 Td 46.990741 Tz (synthesis. ) Tj 51.428571 0 0 51.428571 0 2792.436457 Tm 6.280556 0 Td 57.253086 Tz (For ) Tj 1.263889 0 Td 55.497685 Tz (example, ) Tj 2.975 0 Td 46.759259 Tz (optical ) Tj 2.255556 0 Td 53.703704 Tz (isomers ) Tj 2.566667 0 Td 68.055556 Tz (may ) Tj 1.536111 0 Td 58.333333 Tz (be ) Tj 0.972222 0 Td 53.06713 Tz (prepared ) Tj 2.838889 0 Td 58.333333 Tz (from ) Tj 1.711111 0 Td 45.37037 Tz (their ) Tj 51.428571 0 0 51.428571 0 2753.589447 Tm 6.261111 0 Td 49.259259 Tz (respective ) Tj 3.344444 0 Td 47.530864 Tz (optically ) Tj 2.955556 0 Td 48.611111 Tz (active ) Tj 2.138889 0 Td 50.231481 Tz (precursors ) Tj 3.422222 0 Td 59.953704 Tz (by ) Tj 1.108333 0 Td 50.771605 Tz (the ) Tj 1.302778 0 Td 53.148148 Tz (procedures ) Tj 51.428571 0 0 51.428571 0 2706.724138 Tm 6.261111 0 Td 51.851852 Tz (described ) Tj 2.975 0 Td 54.012346 Tz (above, ) Tj 2.158333 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 58.333333 Tz (by ) Tj 0.952778 0 Td 50.05144 Tz (resolving ) Tj 2.897222 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 54.166667 Tz (racemic ) Tj 2.527778 0 Td 49.691358 Tz (mixtures. ) Tj 2.897222 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 2666.765306 Tm 6.261111 0 Td 48.287037 Tz (resolution ) Tj 3.15 0 Td 55.092593 Tz (can ) Tj 1.205556 0 Td 59.953704 Tz (be ) Tj 0.952778 0 Td 47.685185 Tz (carried ) Tj 2.236111 0 Td 51.851852 Tz (out ) Tj 1.166667 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 53.472222 Tz (presence ) Tj 2.8 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 50.05144 Tz (resolving ) Tj 51.428571 0 0 51.428571 0 2629.367901 Tm 6.261111 0 Td 48.611111 Tz (agent, ) Tj 1.983333 0 Td 61.574074 Tz (by ) Tj 1.011111 0 Td 56.25 Tz (chromatography ) Tj 4.997222 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 61.574074 Tz (by ) Tj 1.011111 0 Td 51.041667 Tz (repeated ) Tj 2.683333 0 Td 45.58642 Tz (crystallization ) Tj 4.375 0 Td 51.851852 Tz (or ) Tj 51.428571 0 0 51.428571 0 2582.943834 Tm 6.241667 0 Td 61.574074 Tz (by ) Tj 0.952778 0 Td 64.00463 Tz (some ) Tj 1.769444 0 Td 54.79798 Tz (combination ) Tj 3.830556 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 49.907407 Tz (these ) Tj 1.672222 0 Td 52.175926 Tz (techniques ) Tj 3.363889 0 Td 58.333333 Tz (which ) Tj 1.963889 0 Td 50.771605 Tz (are ) Tj 1.088889 0 Td 68.055556 Tz (known ) Tj 51.428571 0 0 51.428571 0 2540.462033 Tm 6.241667 0 Td 45.37037 Tz (to ) Tj 0.855556 0 Td 50.555556 Tz (those ) Tj 1.75 0 Td 46.296296 Tz (skilled ) Tj 2.197222 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 38.078704 Tz (art. ) Tj 1.225 0 Td 50.925926 Tz (Further ) Tj 2.372222 0 Td 44.444444 Tz (details ) Tj 2.138889 0 Td 51.131687 Tz (regarding ) Tj 3.013889 0 Td 55.632716 Tz (resolu ) Tj 51.428571 0 0 51.428571 0 2498.32626 Tm 6.241667 0 Td 47.314815 Tz (tions ) Tj 1.730556 0 Td 55.092593 Tz (can ) Tj 1.283333 0 Td 59.953704 Tz (be ) Tj 1.011111 0 Td 56.388889 Tz (found ) Tj 1.983333 0 Td 45.37037 Tz (in ) Tj 0.855556 0 Td 50.636574 Tz (Jacques, ) Tj 2.741667 0 Td 43.75 Tz (et ) Tj 0.797222 0 Td 37.268519 Tz (al., ) Tj 1.244444 0 Td 52.932099 Tz (Enantiomers, ) Tj 4.2 0 Td 68.055556 Tz (Race ) Tj 51.428571 0 0 51.428571 0 2456.953642 Tm 6.280556 0 Td 49.691358 Tz (mates, ) Tj 2.177778 0 Td 63.734568 Tz (and ) Tj 1.477778 0 Td 50.378788 Tz (Resolutions ) Tj 3.675 0 Td 53.148148 Tz (\(John ) Tj 1.925 0 Td 58.333333 Tz (Wiley ) Tj 2.061111 0 Td 90.740741 Tz (& ) Tj 0.913889 0 Td 52.5 Tz (Sons, ) Tj 1.944444 0 Td 50.231481 Tz (1981\). ) Tj 2.138889 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 2417.925466 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.866667 0 Td 57.253086 Tz (complexes ) Tj 3.325 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 44.560185 Tz (this ) Tj 1.341667 0 Td 50.05144 Tz (invention ) Tj 2.994444 0 Td 66.975309 Tz (may ) Tj 1.419444 0 Td 49.421296 Tz (also ) Tj 1.438889 0 Td 56.712963 Tz (be ) Tj 0.913889 0 Td 51.262626 Tz (represented ) Tj 51.428571 0 0 51.428571 0 2374.250318 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.855556 0 Td 49.826389 Tz (multiple ) Tj 2.625 0 Td 51.851852 Tz (tautomeric ) Tj 3.383333 0 Td 51.851852 Tz (forms, ) Tj 2.138889 0 Td 43.75 Tz (in ) Tj 0.816667 0 Td 53.472222 Tz (Such ) Tj 1.575 0 Td 46.990741 Tz (instances, ) Tj 3.072222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 61.574074 Tz (inven ) Tj 51.428571 0 0 51.428571 0 2332.471503 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.458333 0 Td 51.131687 Tz (expressly ) Tj 3.072222 0 Td 50.231481 Tz (includes ) Tj 2.722222 0 Td 39.969136 Tz (all ) Tj 1.05 0 Td 51.851852 Tz (tautomeric ) Tj 3.461111 0 Td 55.092593 Tz (forms ) Tj 1.963889 0 Td 61.574074 Tz (of ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2295.228571 Tm 6.261111 0 Td 57.613169 Tz (complexes ) Tj 3.286111 0 Td 51.49177 Tz (described ) Tj 2.897222 0 Td 51.311728 Tz (herein ) Tj 2.022222 0 Td 39.969136 Tz (\(e.g., ) Tj 1.613889 0 Td 48.287037 Tz (alkylation ) Tj 3.072222 0 Td 56.712963 Tz (of ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 49.421296 Tz (ring ) Tj 1.322222 0 Td 56.712963 Tz (system ) Tj 51.428571 0 0 51.428571 0 2251.649123 Tm 6.261111 0 Td 69.135802 Tz (may ) Tj 1.652778 0 Td 45.37037 Tz (result ) Tj 1.983333 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 48.611111 Tz (alkylation ) Tj 3.305556 0 Td 45.37037 Tz (at ) Tj 0.933333 0 Td 50.231481 Tz (multiple ) Tj 2.8 0 Td 40.509259 Tz (sites, ) Tj 1.847222 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 51.131687 Tz (invention ) Tj 51.428571 0 0 51.428571 0 2209.642072 Tm 6.261111 0 Td 50.771605 Tz (expressly ) Tj 3.013889 0 Td 49.826389 Tz (includes ) Tj 2.625 0 Td 41.049383 Tz (all ) Tj 1.011111 0 Td 54.282407 Tz (Such ) Tj 1.575 0 Td 48.206019 Tz (reaction ) Tj 2.566667 0 Td 48.287037 Tz (products\). ) Tj 51.428571 0 0 51.428571 0 2167.42524 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.875 0 Td 47.530864 Tz (addition, ) Tj 2.877778 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.905556 0 Td 56.893004 Tz (complexes ) Tj 3.402778 0 Td 56.712963 Tz (of ) Tj 0.875 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 50.05144 Tz (invention ) Tj 3.072222 0 Td 68.055556 Tz (may ) Tj 51.428571 0 0 51.428571 0 2123.832675 Tm 6.261111 0 Td 51.388889 Tz (contain ) Tj 2.411111 0 Td 59.41358 Tz (one ) Tj 1.322222 0 Td 53.472222 Tz (or ) Tj 0.933333 0 Td 60.763889 Tz (more ) Tj 1.75 0 Td 54.552469 Tz (double ) Tj 2.236111 0 Td 53.472222 Tz (or ) Tj 0.894444 0 Td 42.669753 Tz (triple ) Tj 1.788889 0 Td 58.333333 Tz (bonds ) Tj 2.041667 0 Td 43.75 Tz (in ) Tj 0.816667 0 Td 45.37037 Tz (their ) Tj 1.613889 0 Td 55.092593 Tz (struc ) Tj 51.428571 0 0 51.428571 0 2083.618321 Tm 6.241667 0 Td 44.290123 Tz (tures. ) Tj 1.788889 0 Td 55.092593 Tz (Thus, ) Tj 1.847222 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 51.851852 Tz (metal ) Tj 1.788889 0 Td 57.253086 Tz (complexes ) Tj 3.305556 0 Td 55.092593 Tz (can ) Tj 1.244444 0 Td 53.796296 Tz (occur ) Tj 1.808333 0 Td 46.990741 Tz (as ) Tj 0.836111 0 Td 42.939815 Tz (cis- ) Tj 1.244444 0 Td 51.851852 Tz (or ) Tj 0.797222 0 Td 55.092593 Tz (trans ) Tj 48.571429 0 0 48.571429 0 2042 Tm 6.629412 0 Td 56.617647 Tz (or ) Tj 0.844118 0 Td 58.333333 Tz (E- ) Tj 0.885294 0 Td 54.901961 Tz (or ) Tj 0.823529 0 Td 58.762255 Tz (Z-double ) Tj 3.005882 0 Td 54.473039 Tz (isomeric ) Tj 2.8 0 Td 54.901961 Tz (forms, ) Tj 2.182353 0 Td 61.764706 Tz (which ) Tj 2.017647 0 Td 53.75817 Tz (are ) Tj 1.152941 0 Td 54.901961 Tz (included ) Tj 2.820588 0 Td 55.473856 Tz (within ) Tj 51.428571 0 0 51.428571 0 2000.832884 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 55.092593 Tz (scope ) Tj 1.886111 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 43.75 Tz (this ) Tj 1.302778 0 Td 48.287037 Tz (invention. ) Tj 51.428571 0 0 51.428571 0 1959.781671 Tm 7.019444 0 Td 46.990741 Tz (Further, ) Tj 2.527778 0 Td 39.969136 Tz (all ) Tj 0.991667 0 Td 45.37037 Tz (crystal ) Tj 2.216667 0 Td 55.740741 Tz (forms ) Tj 1.944444 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 57.613169 Tz (complexes ) Tj 3.383333 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 51.428571 0 0 51.428571 0 1917.501892 Tm 6.261111 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 49.691358 Tz (are ) Tj 1.127778 0 Td 48.611111 Tz (also ) Tj 1.438889 0 Td 50.05144 Tz (expressly ) Tj 2.994444 0 Td 52.256944 Tz (included ) Tj 2.780556 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.462963 Tz (present ) Tj 2.352778 0 Td 61.574074 Tz (inven ) Tj 40 0 0 40 0 1882 Tm 8.025 0 Td 55.833333 Tz (tion. ) Tj 51.428571 0 0 51.428571 0 1834.791946 Tm 7 0 Td 87.5 Tz (A ) Tj 0.738889 0 Td 52.5 Tz (metal ) Tj 1.827778 0 Td 59.722222 Tz (complex ) Tj 2.761111 0 Td 55.092593 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 50.411523 Tz (invention ) Tj 2.994444 0 Td 55.092593 Tz (can ) Tj 1.205556 0 Td 61.574074 Tz (be ) Tj 0.952778 0 Td 53.06713 Tz (prepared ) Tj 2.761111 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 59.953704 Tz (an ) Tj 51.428571 0 0 51.428571 0 1794.238825 Tm 6.261111 0 Td 51.041667 Tz (acid ) Tj 1.4 0 Td 63.194444 Tz (by ) Tj 0.991667 0 Td 48.206019 Tz (reacting ) Tj 2.527778 0 Td 47.530864 Tz (the ) Tj 1.108333 0 Td 46.180556 Tz (free ) Tj 1.302778 0 Td 55.092593 Tz (base ) Tj 1.497222 0 Td 57.523148 Tz (form ) Tj 1.633333 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 64.409722 Tz (compound ) Tj 3.286111 0 Td 52.662037 Tz (with ) Tj 1.497222 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 1753.700389 Tm 6.280556 0 Td 46.990741 Tz (Suitable ) Tj 2.586111 0 Td 50.411523 Tz (inorganic ) Tj 3.091667 0 Td 51.851852 Tz (or ) Tj 0.972222 0 Td 50.925926 Tz (organic ) Tj 2.469444 0 Td 46.018519 Tz (acid. ) Tj 1.75 0 Td 46.990741 Tz (Alternatively, ) Tj 4.277778 0 Td 58.333333 Tz (a ) Tj 0.719444 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 1711.315716 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.858333 0 Td 56.712963 Tz (of ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 50.411523 Tz (invention ) Tj 3.111111 0 Td 54.012346 Tz (can ) Tj 1.341667 0 Td 56.712963 Tz (be ) Tj 1.030556 0 Td 53.06713 Tz (prepared ) Tj 2.897222 0 Td 48.611111 Tz (as ) Tj 0.933333 0 Td 58.333333 Tz (a ) Tj 0.7 0 Td 54.282407 Tz (base ) Tj 1.633333 0 Td 63.194444 Tz (by ) Tj 51.428571 0 0 51.428571 0 1668.742015 Tm 6.261111 0 Td 49.016204 Tz (reacting ) Tj 2.547222 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 47.800926 Tz (free ) Tj 1.283333 0 Td 50.555556 Tz (basic ) Tj 1.691667 0 Td 58.333333 Tz (form ) Tj 1.594444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 64.00463 Tz (compound ) Tj 3.247222 0 Td 53.472222 Tz (with ) Tj 1.438889 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 46.990741 Tz (suitable ) Tj 52.857143 0 0 52.857143 0 1628.115242 Tm 6.091892 0 Td 49.049049 Tz (inorganic ) Tj 2.856757 0 Td 50.45045 Tz (or ) Tj 0.775676 0 Td 50 Tz (organic ) Tj 2.308108 0 Td 46.666667 Tz (base. ) Tj 1.683784 0 Td 52.552553 Tz (For ) Tj 1.097297 0 Td 53.603604 Tz (example, ) Tj 2.762162 0 Td 56.756757 Tz (a ) Tj 0.567568 0 Td 51.081081 Tz (metal ) Tj 1.721622 0 Td 58.108108 Tz (complex ) Tj 2.62973 0 Td 56.756757 Tz (of ) Tj 40 0 0 40 0 1590 Tm 8.025 0 Td 65.277778 Tz (the ) Tj 1.45 0 Td 64.814815 Tz (invention ) Tj 3.775 0 Td 56.25 Tz (in ) Tj 0.975 0 Td 72.916667 Tz (an ) Tj 1.1 0 Td 66.666667 Tz (acid ) Tj 1.85 0 Td 63.541667 Tz (addition ) Tj 3.325 0 Td 54.166667 Tz (salt ) Tj 1.55 0 Td 75 Tz (form ) Tj 2.075 0 Td 70.833333 Tz (can ) Tj 1.55 0 Td 75 Tz (be ) Tj 1.15 0 Td 68.981481 Tz (converted ) Tj 51.428571 0 0 51.428571 0 1543.80704 Tm 6.241667 0 Td 46.990741 Tz (to ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 53.347578 Tz (corresponding ) Tj 4.433333 0 Td 47.800926 Tz (free ) Tj 1.419444 0 Td 54.282407 Tz (base ) Tj 1.594444 0 Td 58.333333 Tz (by ) Tj 1.011111 0 Td 46.585648 Tz (treating ) Tj 2.508333 0 Td 54.282407 Tz (with ) Tj 1.555556 0 Td 58.333333 Tz (a ) Tj 0.661111 0 Td 46.990741 Tz (suitable ) Tj 51.428571 0 0 51.428571 0 1502.382746 Tm 6.241667 0 Td 55.092593 Tz (base ) Tj 1.555556 0 Td 40.509259 Tz (\(e.g., ) Tj 1.711111 0 Td 68.865741 Tz (ammonium ) Tj 3.538889 0 Td 55.452675 Tz (hydroxide ) Tj 3.247222 0 Td 46.090535 Tz (Solution, ) Tj 2.741667 0 Td 58.873457 Tz (Sodium ) Tj 2.372222 0 Td 64.274691 Tz (hydrox ) Tj 51.428571 0 0 51.428571 0 1458.28839 Tm 6.261111 0 Td 44.560185 Tz (ide, ) Tj 1.225 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 40.509259 Tz (like\). ) Tj 1.633333 0 Td 84.259259 Tz (A ) Tj 0.641667 0 Td 53.148148 Tz (metal ) Tj 1.75 0 Td 59.722222 Tz (complex ) Tj 2.683333 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 50.05144 Tz (invention ) Tj 2.877778 0 Td 46.990741 Tz (in ) Tj 0.738889 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 54.282407 Tz (base ) Tj 51.428571 0 0 51.428571 0 1417.074789 Tm 6.261111 0 Td 49.421296 Tz (addition ) Tj 2.527778 0 Td 42.12963 Tz (salt ) Tj 1.186111 0 Td 57.523148 Tz (form ) Tj 1.555556 0 Td 55.092593 Tz (can ) Tj 1.147222 0 Td 58.333333 Tz (be ) Tj 0.836111 0 Td 53.292181 Tz (converted ) Tj 3.013889 0 Td 46.990741 Tz (to ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 53.596866 Tz (corresponding ) Tj 4.336111 0 Td 46.990741 Tz (free ) Tj 51.428571 0 0 51.428571 0 1378.102815 Tm 6.261111 0 Td 51.041667 Tz (acid ) Tj 1.4 0 Td 58.333333 Tz (by ) Tj 0.875 0 Td 46.990741 Tz (treating ) Tj 2.430556 0 Td 53.472222 Tz (with ) Tj 1.458333 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 47.395833 Tz (Suitable ) Tj 2.411111 0 Td 51.851852 Tz (acid ) Tj 1.438889 0 Td 40.509259 Tz (\(e.g., ) Tj 1.633333 0 Td 51.851852 Tz (hydrochloric ) Tj 3.908333 0 Td 45.37037 Tz (acid, ) Tj 51.428571 0 0 51.428571 0 1332 Tm 6.261111 0 Td 39.969136 Tz (etc.\). ) Tj 51.428571 0 0 51.428571 0 1294.657431 Tm 7 0 Td 47.222222 Tz (Alternatively, ) Tj 4.141667 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 42.939815 Tz (salt ) Tj 1.186111 0 Td 55.740741 Tz (forms ) Tj 1.827778 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 51.851852 Tz (the ) Tj 1.069444 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 57.253086 Tz (complexes ) Tj 3.266667 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1252.320562 Tm 6.261111 0 Td 50.771605 Tz (invention ) Tj 3.013889 0 Td 55.092593 Tz (can ) Tj 1.244444 0 Td 58.333333 Tz (be ) Tj 0.933333 0 Td 53.06713 Tz (prepared ) Tj 2.819444 0 Td 53.148148 Tz (using ) Tj 1.827778 0 Td 42.12963 Tz (salts ) Tj 1.555556 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 45.37037 Tz (starting ) Tj 2.469444 0 Td 67.24537 Tz (mate ) Tj 40 0 0 40 0 1216 Tm 8.05 0 Td 53.333333 Tz (rials ) Tj 1.925 0 Td 68.75 Tz (or ) Tj 1.125 0 Td 61.904762 Tz (intermediates. ) Tj 51.428571 0 0 51.428571 0 1167.61596 Tm 7.019444 0 Td 50.411523 Tz (Protected ) Tj 2.897222 0 Td 47.727273 Tz (derivatives ) Tj 3.325 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 53.148148 Tz (metal ) Tj 1.730556 0 Td 58.333333 Tz (complexes ) Tj 3.286111 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 60.925926 Tz (inven ) Tj 51.428571 0 0 51.428571 0 1125.666667 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.361111 0 Td 54.012346 Tz (can ) Tj 1.166667 0 Td 58.333333 Tz (be ) Tj 0.933333 0 Td 64.00463 Tz (made ) Tj 1.691667 0 Td 61.574074 Tz (by ) Tj 0.972222 0 Td 60.277778 Tz (means ) Tj 2.002778 0 Td 66.759259 Tz (known ) Tj 2.177778 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 51.203704 Tz (those ) Tj 1.730556 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 51.446759 Tz (ordinary ) Tj 2.683333 0 Td 41.481481 Tz (skill ) Tj 51.428571 0 0 51.428571 0 1087.719212 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 38.078704 Tz (art. ) Tj 1.127778 0 Td 84.259259 Tz (A ) Tj 0.661111 0 Td 48.206019 Tz (detailed ) Tj 2.508333 0 Td 48.611111 Tz (description ) Tj 3.422222 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 51.851852 Tz (techniques ) Tj 3.325 0 Td 49.907407 Tz (applicable ) Tj 3.188889 0 Td 46.990741 Tz (to ) Tj 51.428571 0 0 51.428571 0 1043.598985 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 47.800926 Tz (creation ) Tj 2.586111 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 49.583333 Tz (protecting ) Tj 3.188889 0 Td 55.632716 Tz (groups ) Tj 2.255556 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 45.37037 Tz (their ) Tj 1.594444 0 Td 56.018519 Tz (removal ) Tj 2.625 0 Td 54.012346 Tz (can ) Tj 1.225 0 Td 59.953704 Tz (be ) Tj 51.428571 0 0 51.428571 0 1004.395604 Tm 6.261111 0 Td 57.037037 Tz (found ) Tj 2.119444 0 Td 43.75 Tz (in ) Tj 0.933333 0 Td 45.37037 Tz (T. ) Tj 0.991667 0 Td 63.194444 Tz (W. ) Tj 1.166667 0 Td 54.62963 Tz (Greene, ) Tj 2.683333 0 Td 50.378788 Tz (Protecting ) Tj 3.733333 0 Td 58.873457 Tz (Groups ) Tj 2.547222 0 Td 45.37037 Tz (in ) Tj 0.952778 0 Td 55.555556 Tz (Organic ) Tj 51.428571 0 0 51.428571 0 960.737643 Tm 6.261111 0 Td 53.619529 Tz (Chemistry', ) Tj 3.752778 0 Td 56.17284 Tz (3rd ) Tj 1.244444 0 Td 45.37037 Tz (edition, ) Tj 2.430556 0 Td 57.523148 Tz (John ) Tj 1.633333 0 Td 57.037037 Tz (Wiley ) Tj 1.944444 0 Td 60.493827 Tz (and ) Tj 1.322222 0 Td 53.148148 Tz (Sons, ) Tj 1.847222 0 Td 42.777778 Tz (Inc., ) Tj 1.575 0 Td 51.851852 Tz (1999. ) Tj 51.428571 0 0 51.428571 0 920.006935 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.497222 0 Td 52.5 Tz (metal ) Tj 1.925 0 Td 57.973251 Tz (complexes ) Tj 3.480556 0 Td 59.953704 Tz (of ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 50.925926 Tz (present ) Tj 2.488889 0 Td 50.411523 Tz (invention ) Tj 3.072222 0 Td 56.17284 Tz (can ) Tj 1.380556 0 Td 58.333333 Tz (be ) Tj 51.428571 0 0 51.428571 0 880.359703 Tm 6.261111 0 Td 52.121914 Tz (conveniently ) Tj 3.986111 0 Td 50.05144 Tz (prepared, ) Tj 2.975 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 58.333333 Tz (formed ) Tj 2.333333 0 Td 52.391975 Tz (during ) Tj 2.1 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 52.314815 Tz (process ) Tj 2.45 0 Td 55.092593 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 836.473171 Tm 6.261111 0 Td 48.611111 Tz (invention, ) Tj 3.091667 0 Td 51.851852 Tz (as ) Tj 0.816667 0 Td 48.611111 Tz (Solvates ) Tj 2.547222 0 Td 40.509259 Tz (\(e.g., ) Tj 1.633333 0 Td 47.962963 Tz (hydrates\). ) Tj 3.130556 0 Td 53.877315 Tz (Hydrates ) Tj 2.780556 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 797.031325 Tm 6.261111 0 Td 57.613169 Tz (complexes ) Tj 3.286111 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 50.411523 Tz (invention ) Tj 2.916667 0 Td 55.092593 Tz (can ) Tj 1.186111 0 Td 56.712963 Tz (be ) Tj 0.875 0 Td 51.851852 Tz (conveniently ) Tj 3.908333 0 Td 53.06713 Tz (prepared ) Tj 2.702778 0 Td 63.194444 Tz (by ) Tj 51.428571 0 0 51.428571 0 754.7162 Tm 6.261111 0 Td 45.751634 Tz (recrystallization ) Tj 4.958333 0 Td 58.333333 Tz (from ) Tj 1.691667 0 Td 56.712963 Tz (an ) Tj 0.972222 0 Td 52.716049 Tz (aqueous/organic ) Tj 5.036111 0 Td 50 Tz (solvent ) Tj 2.411111 0 Td 49.421296 Tz (mixture, ) Tj 51.428571 0 0 51.428571 0 713.348718 Tm 6.241667 0 Td 53.148148 Tz (using ) Tj 1.944444 0 Td 50.462963 Tz (organic ) Tj 2.45 0 Td 49.421296 Tz (solvents ) Tj 2.722222 0 Td 54.282407 Tz (such ) Tj 1.633333 0 Td 50.231481 Tz (as ) Tj 0.933333 0 Td 48.148148 Tz (dioxin, ) Tj 2.333333 0 Td 50.339506 Tz (tetrahydrofuran ) Tj 4.880556 0 Td 51.851852 Tz (or ) Tj 40 0 0 40 0 675 Tm 8.05 0 Td 68.055556 Tz (methanol. ) Tj 51.428571 0 0 51.428571 0 628.323259 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.380556 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 57.253086 Tz (complexes ) Tj 3.344444 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 44.560185 Tz (this ) Tj 1.322222 0 Td 50.05144 Tz (invention ) Tj 2.994444 0 Td 66.975309 Tz (may ) Tj 1.458333 0 Td 58.333333 Tz (be ) Tj 0.972222 0 Td 53.877315 Tz (modified ) Tj 51.428571 0 0 51.428571 0 587.489032 Tm 6.241667 0 Td 61.574074 Tz (by ) Tj 0.972222 0 Td 50.05144 Tz (attaching ) Tj 2.936111 0 Td 46.990741 Tz (to ) Tj 0.875 0 Td 49.537037 Tz (various ) Tj 2.372222 0 Td 49.907407 Tz (other ) Tj 1.730556 0 Td 49.537037 Tz (ligands ) Tj 2.372222 0 Td 48.611111 Tz (via ) Tj 1.108333 0 Td 58.333333 Tz (any ) Tj 1.341667 0 Td 60.277778 Tz (means ) Tj 2.1 0 Td 55.740741 Tz (delin ) Tj 51.428571 0 0 51.428571 0 545.72549 Tm 6.261111 0 Td 51.203704 Tz (eated ) Tj 1.75 0 Td 50.771605 Tz (herein ) Tj 2.061111 0 Td 48.611111 Tz (to ) Tj 0.816667 0 Td 57.407407 Tz (enhance ) Tj 2.644444 0 Td 45.37037 Tz (catalytic ) Tj 2.683333 0 Td 46.843434 Tz (properties. ) Tj 51.428571 0 0 51.428571 0 502.647668 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 57.253086 Tz (complexes ) Tj 3.325 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 50.411523 Tz (invention ) Tj 2.955556 0 Td 49.691358 Tz (are ) Tj 1.127778 0 Td 50.925926 Tz (defined ) Tj 2.352778 0 Td 51.311728 Tz (herein ) Tj 51.428571 0 0 51.428571 0 459.37028 Tm 6.241667 0 Td 61.574074 Tz (by ) Tj 0.991667 0 Td 44.722222 Tz (their ) Tj 1.497222 0 Td 55.092593 Tz (chemical ) Tj 2.858333 0 Td 46.666667 Tz (structures ) Tj 3.033333 0 Td 52.932099 Tz (and/or ) Tj 2.080556 0 Td 54.6875 Tz (chemical ) Tj 2.877778 0 Td 55.092593 Tz (names. ) Tj 2.236111 0 Td 64.166667 Tz (Where ) Tj 51.428571 0 0 51.428571 0 419.696041 Tm 6.261111 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 53.148148 Tz (metal ) Tj 1.788889 0 Td 60.185185 Tz (complex ) Tj 2.761111 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 47.800926 Tz (referred ) Tj 2.488889 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 58.333333 Tz (by ) Tj 0.933333 0 Td 53.472222 Tz (both ) Tj 1.497222 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 54.6875 Tz (chemical ) Tj 2.858333 0 Td 47.170782 Tz (structure ) Tj 48.571429 0 0 48.571429 0 378 Tm 6.629412 0 Td 61.764706 Tz (and ) Tj 1.276471 0 Td 61.764706 Tz (a ) Tj 0.535294 0 Td 57.47549 Tz (chemical ) Tj 3.005882 0 Td 60.392157 Tz (name, ) Tj 1.997059 0 Td 62.908497 Tz (and ) Tj 1.297059 0 Td 52.614379 Tz (the ) Tj 1.132353 0 Td 57.47549 Tz (chemical ) Tj 2.944118 0 Td 49.56427 Tz (structure ) Tj 2.882353 0 Td 61.764706 Tz (and ) Tj 1.276471 0 Td 71.372549 Tz (chemi ) Tj 48.571429 0 0 48.571429 0 337 Tm 6.629412 0 Td 49.183007 Tz (cal ) Tj 1.152941 0 Td 67.769608 Tz (name ) Tj 1.811765 0 Td 46.514161 Tz (conflict, ) Tj 2.717647 0 Td 52.614379 Tz (the ) Tj 1.132353 0 Td 57.47549 Tz (chemical ) Tj 3.005882 0 Td 49.945534 Tz (structure ) Tj 2.882353 0 Td 41.176471 Tz (is ) Tj 0.741176 0 Td 53.846154 Tz (determinative ) Tj 4.426471 0 Td 60.04902 Tz (of ) Tj 51.428571 0 0 51.428571 0 299.925714 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 59.62963 Tz (compound's ) Tj 3.85 0 Td 42.849794 Tz (identity. ) Tj 51.428571 0 0 51.428571 0 253.868571 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.477778 0 Td 45.694444 Tz (recitation ) Tj 3.130556 0 Td 56.712963 Tz (of ) Tj 0.952778 0 Td 55.092593 Tz (a ) Tj 0.7 0 Td 43.518519 Tz (listing ) Tj 2.197222 0 Td 56.712963 Tz (of ) Tj 0.952778 0 Td 54.6875 Tz (chemical ) Tj 2.994444 0 Td 54.552469 Tz (groups ) Tj 2.352778 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 60.493827 Tz (any ) Tj 40 0 0 40 0 218 Tm 8.05 0 Td 59.583333 Tz (definition ) Tj 4 0 Td 72.916667 Tz (of ) Tj 1.125 0 Td 70.833333 Tz (a ) Tj 0.8 0 Td 63.020833 Tz (variable ) Tj 3.4 0 Td 64.583333 Tz (herein ) Tj 2.75 0 Td 64.0625 Tz (includes ) Tj 3.5 0 Td 59.469697 Tz (definitions ) Tj 4.325 0 Td 72.916667 Tz (of ) Tj 1.15 0 Td 59.375 Tz (that ) Tj 51.428571 0 0 51.428571 0 171.292978 Tm 6.261111 0 Td 49.016204 Tz (variable ) Tj 2.488889 0 Td 50.231481 Tz (as ) Tj 0.777778 0 Td 59.41358 Tz (any ) Tj 1.244444 0 Td 47.530864 Tz (single ) Tj 1.866667 0 Td 56.388889 Tz (group ) Tj 1.866667 0 Td 51.851852 Tz (or ) Tj 0.777778 0 Td 54.503367 Tz (combination ) Tj 3.772222 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 43.75 Tz (listed ) Tj 1.730556 0 Td 50.925926 Tz (groups. ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.502778 0 Td 72.916667 Tz (12 ) Tj 40 0 0 40 0 2921 Tm 32.4 0 Td 81.944444 Tz (The ) Tj 1.975 0 Td 58.75 Tz (recitation ) Tj 4.075 0 Td 75 Tz (of ) Tj 1.3 0 Td 72.916667 Tz (an ) Tj 1.4 0 Td 78.75 Tz (embodiment ) Tj 5.25 0 Td 62.5 Tz (for ) Tj 1.625 0 Td 70.833333 Tz (a ) Tj 0.975 0 Td 62.5 Tz (variable ) Tj 3.5 0 Td 65.972222 Tz (herein ) Tj 51.428571 0 0 51.428571 0 2871.452711 Tm 25.2 0 Td 50.231481 Tz (includes ) Tj 2.683333 0 Td 46.180556 Tz (that ) Tj 1.361111 0 Td 60.925926 Tz (embodiment ) Tj 3.888889 0 Td 51.851852 Tz (as ) Tj 0.855556 0 Td 58.333333 Tz (any ) Tj 1.341667 0 Td 48.611111 Tz (single ) Tj 2.002778 0 Td 60.601852 Tz (embodiment ) Tj 3.908333 0 Td 51.851852 Tz (or ) Tj 0.875 0 Td 46.990741 Tz (in ) Tj 51.428571 0 0 51.428571 0 2827.921727 Tm 25.2 0 Td 54.79798 Tz (combination ) Tj 4.141667 0 Td 53.472222 Tz (with ) Tj 1.788889 0 Td 59.41358 Tz (any ) Tj 1.594444 0 Td 50.555556 Tz (other ) Tj 2.002778 0 Td 59.217172 Tz (embodiments ) Tj 4.452778 0 Td 51.851852 Tz (or ) Tj 1.088889 0 Td 49.826389 Tz (portions ) Tj 40 0 0 40 0 2790 Tm 32.375 0 Td 59.895833 Tz (thereof. ) Tj 40 0 0 40 0 2747 Tm 32.425 0 Td 66.666667 Tz (Processes ) Tj 3.925 0 Td 75 Tz (and ) Tj 1.675 0 Td 77.380952 Tz (Methods ) Tj 51.428571 0 0 51.428571 0 2699.086845 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 50.05144 Tz (invention ) Tj 2.897222 0 Td 48.611111 Tz (also ) Tj 1.341667 0 Td 51.851852 Tz (provides ) Tj 2.683333 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 43.569959 Tz (catalyst, ) Tj 2.566667 0 Td 58.333333 Tz (which ) Tj 1.944444 0 Td 54.372428 Tz (comprises ) Tj 3.111111 0 Td 58.333333 Tz (a ) Tj 51.428571 0 0 51.428571 0 2653.311512 Tm 25.2 0 Td 53.796296 Tz (metal ) Tj 1.886111 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 51.851852 Tz (the ) Tj 1.186111 0 Td 47.962963 Tz (invention. ) Tj 51.428571 0 0 51.428571 0 2612.163373 Tm 25.938889 0 Td 47.395833 Tz (Further, ) Tj 2.547222 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 50.411523 Tz (invention ) Tj 2.994444 0 Td 52.662037 Tz (provides ) Tj 2.819444 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 52.314815 Tz (process ) Tj 2.508333 0 Td 46.450617 Tz (for ) Tj 1.108333 0 Td 54.73251 Tz (producing ) Tj 51.428571 0 0 51.428571 0 2567.984106 Tm 25.180556 0 Td 57.928241 Tz (hydrogen ) Tj 3.072222 0 Td 59.953704 Tz (by ) Tj 1.05 0 Td 53.148148 Tz (using ) Tj 1.886111 0 Td 58.333333 Tz (a ) Tj 0.680556 0 Td 46.180556 Tz (catalyst ) Tj 2.527778 0 Td 56.712963 Tz (of ) Tj 0.894444 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 47.962963 Tz (invention. ) Tj 3.247222 0 Td 46.990741 Tz (In ) Tj 0.913889 0 Td 47.222222 Tz (certain ) Tj 51.428571 0 0 51.428571 0 2523.92176 Tm 25.2 0 Td 56.983025 Tz (embodiments, ) Tj 4.316667 0 Td 56.712963 Tz (hydrogen ) Tj 2.955556 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 56.30787 Tz (produced ) Tj 2.916667 0 Td 58.333333 Tz (from ) Tj 1.613889 0 Td 56.712963 Tz (an ) Tj 0.913889 0 Td 56.481481 Tz (aqueous ) Tj 2.586111 0 Td 60.763889 Tz (solu ) Tj 51.428571 0 0 51.428571 0 2482.434343 Tm 25.180556 0 Td 43.425926 Tz (tion. ) Tj 1.516667 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 52.314815 Tz (process ) Tj 2.430556 0 Td 54.012346 Tz (comprises ) Tj 3.15 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 46.990741 Tz (step ) Tj 1.361111 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 55.632716 Tz (adding ) Tj 2.197222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 46.180556 Tz (catalyst ) Tj 2.411111 0 Td 45.37037 Tz (to ) Tj 51.428571 0 0 51.428571 0 2434.764919 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 48.206019 Tz (solution ) Tj 2.586111 0 Td 51.203704 Tz (\(such ) Tj 1.788889 0 Td 44.290123 Tz (as, ) Tj 1.030556 0 Td 56.712963 Tz (an ) Tj 0.933333 0 Td 56.481481 Tz (aqueous ) Tj 2.644444 0 Td 45.37037 Tz (solution\). ) Tj 51.428571 0 0 51.428571 0 2392.974194 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.797222 0 Td 57.253086 Tz (one ) Tj 1.205556 0 Td 47.170782 Tz (instance, ) Tj 2.741667 0 Td 56.712963 Tz (an ) Tj 0.875 0 Td 45.640432 Tz (electrolysis ) Tj 3.480556 0 Td 48.611111 Tz (step ) Tj 1.361111 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 56.17284 Tz (performed ) Tj 3.188889 0 Td 46.018519 Tz (after ) Tj 1.536111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 2348.378921 Tm 25.2 0 Td 49.421296 Tz (addition ) Tj 2.586111 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 46.180556 Tz (catalyst ) Tj 2.411111 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 56.944444 Tz (aqueous ) Tj 2.625 0 Td 46.090535 Tz (solution. ) Tj 2.741667 0 Td 48.611111 Tz (In ) Tj 0.777778 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 47.685185 Tz (certain ) Tj 51.428571 0 0 51.428571 0 2303.308311 Tm 25.219444 0 Td 44.398148 Tz (situation, ) Tj 3.033333 0 Td 50.771605 Tz (the ) Tj 1.283333 0 Td 56.481481 Tz (aqueous ) Tj 2.8 0 Td 47.800926 Tz (solution ) Tj 2.702778 0 Td 45.37037 Tz (after ) Tj 1.691667 0 Td 50.771605 Tz (the ) Tj 1.263889 0 Td 49.826389 Tz (addition ) Tj 2.819444 0 Td 55.092593 Tz (of ) Tj 0.933333 0 Td 51.851852 Tz (the ) Tj 51.428571 0 0 51.428571 0 2260.91236 Tm 25.2 0 Td 46.585648 Tz (catalyst ) Tj 2.45 0 Td 52.932099 Tz (has ) Tj 1.225 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 76.157407 Tz (pH ) Tj 1.186111 0 Td 51.851852 Tz (value ) Tj 1.788889 0 Td 43.75 Tz (at ) Tj 0.758333 0 Td 55.092593 Tz (about ) Tj 1.886111 0 Td 42.12963 Tz (7. ) Tj 51.428571 0 0 51.428571 0 2216.148718 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.797222 0 Td 52.314815 Tz (another ) Tj 2.411111 0 Td 47.170782 Tz (instance, ) Tj 2.722222 0 Td 51.851852 Tz (the ) Tj 1.108333 0 Td 51.851852 Tz (process ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 50.05144 Tz (invention ) Tj 2.916667 0 Td 50.636574 Tz (includes ) Tj 51.428571 0 0 51.428571 0 2175.438964 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 50.231481 Tz (photolysis ) Tj 3.188889 0 Td 47.800926 Tz (step ) Tj 1.361111 0 Td 58.333333 Tz (on ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 56.018519 Tz (aqueous ) Tj 2.566667 0 Td 48.206019 Tz (solution ) Tj 2.469444 0 Td 46.018519 Tz (after ) Tj 1.516667 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 46.585648 Tz (catalyst ) Tj 2.391667 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 2129.622785 Tm 25.2 0 Td 52.391975 Tz (added. ) Tj 2.216667 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 57.253086 Tz (one ) Tj 1.302778 0 Td 55.092593 Tz (example, ) Tj 2.877778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 56.944444 Tz (aqueous ) Tj 2.644444 0 Td 48.611111 Tz (solution ) Tj 2.586111 0 Td 49.421296 Tz (also ) Tj 1.458333 0 Td 50.231481 Tz (contains ) Tj 51.428571 0 0 51.428571 0 2085.989011 Tm 25.2 0 Td 50.231481 Tz (ascorbic ) Tj 2.780556 0 Td 46.018519 Tz (acid. ) Tj 1.827778 0 Td 46.990741 Tz (In ) Tj 0.913889 0 Td 53.240741 Tz (another ) Tj 2.586111 0 Td 54.6875 Tz (example, ) Tj 3.033333 0 Td 48.611111 Tz (the ) Tj 1.244444 0 Td 74.537037 Tz (pH ) Tj 1.302778 0 Td 51.203704 Tz (value ) Tj 1.905556 0 Td 59.953704 Tz (of ) Tj 0.972222 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 2042.257534 Tm 25.2 0 Td 56.481481 Tz (aqueous ) Tj 2.683333 0 Td 47.800926 Tz (Solution ) Tj 2.605556 0 Td 37.268519 Tz (is ) Tj 0.738889 0 Td 51.311728 Tz (within ) Tj 2.138889 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 54.444444 Tz (range ) Tj 1.886111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 55.092593 Tz (about ) Tj 1.925 0 Td 58.333333 Tz (3 ) Tj 0.602778 0 Td 48.611111 Tz (to ) Tj 0.875 0 Td 42.12963 Tz (6. ) Tj 0.836111 0 Td 46.990741 Tz (In ) Tj 0.836111 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 2000.3125 Tm 25.219444 0 Td 45.775463 Tz (specific ) Tj 2.488889 0 Td 54.282407 Tz (example, ) Tj 2.897222 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 72.916667 Tz (pH ) Tj 1.186111 0 Td 51.203704 Tz (value ) Tj 1.827778 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 56.481481 Tz (aqueous ) Tj 2.663889 0 Td 48.611111 Tz (solution ) Tj 2.625 0 Td 40.509259 Tz (is ) Tj 40 0 0 40 0 1961 Tm 32.4 0 Td 70 Tz (about ) Tj 2.375 0 Td 56.25 Tz (4. ) Tj 51.428571 0 0 51.428571 0 1909.835669 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.758333 0 Td 58.333333 Tz (one ) Tj 1.205556 0 Td 58.038721 Tz (embodiment, ) Tj 3.966667 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 50.411523 Tz (invention ) Tj 2.897222 0 Td 44.907407 Tz (relates ) Tj 2.041667 0 Td 48.611111 Tz (to ) Tj 0.758333 0 Td 53.148148 Tz (using ) Tj 1.75 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 49.151235 Tz (cobalt ) Tj 52.857143 0 0 52.857143 0 1869.461343 Tm 24.518919 0 Td 52.342342 Tz (metal ) Tj 1.872973 0 Td 58.558559 Tz (complex ) Tj 2.781081 0 Td 49.81982 Tz (\(such ) Tj 1.816216 0 Td 42.042042 Tz (as, ) Tj 1.267568 0 Td 65.165165 Tz (Co\(DPA-Bpy\)\(OH\) ) Tj 6.12973 0 Td 57.387387 Tz (\(PF\), ) Tj 2.081081 0 Td 58.858859 Tz (and ) Tj 51.428571 0 0 51.428571 0 1828.80597 Tm 25.375 0 Td 69.771242 Tz (Co\(DPA-ABpy\)\(PF\)\) ) Tj 7.388889 0 Td 50.231481 Tz (as ) Tj 0.894444 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 46.990741 Tz (catalyst ) Tj 2.527778 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 56.712963 Tz (hydrogen ) Tj 3.033333 0 Td 66.975309 Tz (pro ) Tj 40 0 0 40 0 1786 Tm 32.4 0 Td 62.5 Tz (duction. ) Tj 51.428571 0 0 51.428571 0 1738.393316 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 50.411523 Tz (invention ) Tj 2.916667 0 Td 48.611111 Tz (also ) Tj 1.361111 0 Td 51.851852 Tz (provides ) Tj 2.663889 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 48.611111 Tz (nickel ) Tj 1.983333 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 59.259259 Tz (complex ) Tj 2.702778 0 Td 39.969136 Tz (\(e.g., ) Tj 51.428571 0 0 51.428571 0 1698.675393 Tm 25.413889 0 Td 69.513889 Tz (Ni\(DPA-ABpy\)\(OH\)\(BF\) ) Tj 9.313889 0 Td 50.231481 Tz (or ) Tj 1.788889 0 Td 65.679012 Tz (Ni\(DPA-Bpy\)\(HO\) ) Tj 52.857143 0 0 52.857143 0 1649.163987 Tm 24.537838 0 Td 70.630631 Tz (\(BF\)\) ) Tj 2.345946 0 Td 47.297297 Tz (as ) Tj 0.813514 0 Td 48.348348 Tz (the ) Tj 1.097297 0 Td 43.093093 Tz (catalyst. ) Tj 51.428571 0 0 51.428571 0 1604.769437 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.438889 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 59.259259 Tz (complex ) Tj 2.761111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.771605 Tz (invention ) Tj 2.994444 0 Td 56.17284 Tz (can ) Tj 1.263889 0 Td 59.953704 Tz (be ) Tj 0.952778 0 Td 52.256944 Tz (obtained ) Tj 2.780556 0 Td 59.953704 Tz (by ) Tj 51.428571 0 0 51.428571 0 1565.398046 Tm 25.2 0 Td 57.253086 Tz (mixing ) Tj 2.216667 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 50.771605 Tz (ligand ) Tj 2.002778 0 Td 58.333333 Tz (and ) Tj 1.205556 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 52.067901 Tz (metal-providing ) Tj 4.861111 0 Td 52.5 Tz (agent ) Tj 1.769444 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 53.877315 Tz (presence ) Tj 51.428571 0 0 51.428571 0 1517.890756 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 55.092593 Tz (an ) Tj 0.894444 0 Td 50.673401 Tz (appropriate ) Tj 3.597222 0 Td 48.206019 Tz (reaction ) Tj 2.586111 0 Td 46.585648 Tz (solvent. ) Tj 51.428571 0 0 51.428571 0 1474.921162 Tm 25.938889 0 Td 57.253086 Tz (For ) Tj 1.283333 0 Td 55.092593 Tz (example, ) Tj 2.955556 0 Td 51.851852 Tz (a ) Tj 0.641667 0 Td 53.148148 Tz (metal ) Tj 1.905556 0 Td 59.259259 Tz (complex ) Tj 2.8 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 50.411523 Tz (invention ) Tj 3.052778 0 Td 55.092593 Tz (can ) Tj 1.302778 0 Td 56.712963 Tz (be ) Tj 51.428571 0 0 51.428571 0 1433.233333 Tm 25.2 0 Td 53.06713 Tz (prepared ) Tj 2.761111 0 Td 61.574074 Tz (by ) Tj 0.991667 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 52.211934 Tz (following ) Tj 3.072222 0 Td 55.555556 Tz (method: ) Tj 51.428571 0 0 51.428571 0 1386.359946 Tm 25.977778 0 Td 45.37037 Tz (1\) ) Tj 0.758333 0 Td 56.17284 Tz (adding ) Tj 2.216667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 52.5 Tz (metal ) Tj 1.847222 0 Td 41.319444 Tz (salt ) Tj 1.225 0 Td 50.231481 Tz (or ) Tj 0.816667 0 Td 36.728395 Tz (its ) Tj 0.875 0 Td 52.777778 Tz (hydrate ) Tj 2.411111 0 Td 51.388889 Tz (thereof ) Tj 2.275 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 49.016204 Tz (solution ) Tj 51.428571 0 0 51.428571 0 1347.699647 Tm 25.2 0 Td 51.203704 Tz (containing ) Tj 3.227778 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 51.041667 Tz (pentadentate ) Tj 3.830556 0 Td 50.771605 Tz (ligand ) Tj 1.983333 0 Td 51.851852 Tz (\(Such ) Tj 1.691667 0 Td 45.37037 Tz (as, ) Tj 0.991667 0 Td 54.6875 Tz (N.N-Bis\(2-pyridi ) Tj 51.428571 0 0 51.428571 0 1304.692666 Tm 25.2 0 Td 52.5 Tz (nylmethyl\)-2,2'-Bipyridine-6-methanamine ) Tj 12.988889 0 Td 53.472222 Tz (or ) Tj 1.011111 0 Td 48.070988 Tz (6'\(\(bis\(pyri ) Tj 51.428571 0 0 51.428571 0 1261 Tm 25.2 0 Td 52.585604 Tz (din-2-ylmethyl\)amino\)methyl\)-N,N-dimethyl-2,2'-bipyri ) Tj 51.428571 0 0 51.428571 0 1215.865966 Tm 25.2 0 Td 50.605413 Tz (din-6-amine\), ) Tj 6.611111 0 Td 51.666667 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6- ) Tj 51.428571 0 0 51.428571 0 1173.533414 Tm 25.219444 0 Td 51.169591 Tz (\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 12.152778 0 Td 56.712963 Tz (\(DIQ-Bpy\), ) Tj 3.908333 0 Td 50.231481 Tz (or ) Tj 1.069444 0 Td 55.092593 Tz (a ) Tj 48.571429 0 0 48.571429 0 1126 Tm 26.682353 0 Td 51.470588 Tz (derivative ) Tj 3.335294 0 Td 53.431373 Tz (thereof ) Tj 2.408824 0 Td 48.039216 Tz (in ) Tj 0.823529 0 Td 58.333333 Tz (a ) Tj 0.576471 0 Td 51.470588 Tz (reaction ) Tj 2.738235 0 Td 51.960784 Tz (solvent ) Tj 2.429412 0 Td 48.039216 Tz (to ) Tj 0.844118 0 Td 52.614379 Tz (obtain ) Tj 2.120588 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 53.186275 Tz (mixture; ) Tj 40 0 0 40 0 1091 Tm 32.4 0 Td 76.388889 Tz (and ) Tj 51.428571 0 0 51.428571 0 1044.381264 Tm 25.919444 0 Td 51.851852 Tz (2\) ) Tj 0.875 0 Td 48.251029 Tz (refluxing ) Tj 2.858333 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 53.703704 Tz (mixture ) Tj 2.488889 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 48.611111 Tz (step ) Tj 1.497222 0 Td 37.808642 Tz (1\). ) Tj 51.428571 0 0 51.428571 0 1001.606602 Tm 25.938889 0 Td 59.143519 Tz (Examples ) Tj 3.286111 0 Td 59.953704 Tz (of ) Tj 1.05 0 Td 47.395833 Tz (suitable ) Tj 2.722222 0 Td 48.206019 Tz (reaction ) Tj 2.8 0 Td 50 Tz (solvent ) Tj 2.527778 0 Td 50.925926 Tz (include ) Tj 2.566667 0 Td 48.611111 Tz (water, ) Tj 48.571429 0 0 48.571429 0 960 Tm 26.682353 0 Td 46.719457 Tz (acetonitrile, ) Tj 3.829412 0 Td 49.754902 Tz (acetic ) Tj 1.976471 0 Td 50.098039 Tz (acid, ) Tj 1.688235 0 Td 52.042484 Tz (oxalic ) Tj 2.079412 0 Td 48.72549 Tz (acid, ) Tj 1.667647 0 Td 68.137255 Tz (ammonia ) Tj 3.067647 0 Td 51.470588 Tz (water, ) Tj 2.058824 0 Td 70.686275 Tz (metha ) Tj 51.428571 0 0 51.428571 0 922.190985 Tm 25.2 0 Td 46.180556 Tz (nol, ) Tj 1.283333 0 Td 48.611111 Tz (ethanol, ) Tj 2.566667 0 Td 50.378788 Tz (n-propanol, ) Tj 3.558333 0 Td 50.411523 Tz (isopropyl ) Tj 2.936111 0 Td 48.206019 Tz (alcohol, ) Tj 2.527778 0 Td 58.831909 Tz (2-methoxyetha ) Tj 51.428571 0 0 51.428571 0 881.054309 Tm 25.2 0 Td 46.180556 Tz (nol, ) Tj 1.341667 0 Td 48.287037 Tz (1-butanol, ) Tj 3.15 0 Td 49.74537 Tz (1,1-dimethylethanol, ) Tj 6.144444 0 Td 51.851852 Tz (ethylene ) Tj 2.625 0 Td 47.222222 Tz (glycol, ) Tj 2.177778 0 Td 48.148148 Tz (diethyl ) Tj 51.428571 0 0 51.428571 0 837.711425 Tm 25.2 0 Td 44.290123 Tz (ether, ) Tj 1.886111 0 Td 52.175926 Tz (1.2-dimethoxyethane, ) Tj 6.475 0 Td 52.441077 Tz (methylethyl ) Tj 3.636111 0 Td 45.37037 Tz (ether, ) Tj 1.886111 0 Td 49.421296 Tz (1,4-dioxane, ) Tj 51.428571 0 0 51.428571 0 797.388817 Tm 25.180556 0 Td 49.21875 Tz (tetrahydrofuran, ) Tj 5.327778 0 Td 53.472222 Tz (benzene, ) Tj 3.169444 0 Td 48.206019 Tz (toluene, ) Tj 2.936111 0 Td 49.537037 Tz (Xylene, ) Tj 2.761111 0 Td 49.494949 Tz (mesitylene, ) Tj 48.571429 0 0 48.571429 0 752 Tm 26.682353 0 Td 54.411765 Tz (durene, ) Tj 2.491176 0 Td 50.183824 Tz (decalin, ) Tj 2.655882 0 Td 55.545343 Tz (dichloromethane, ) Tj 5.558824 0 Td 55.213904 Tz (chloroform, ) Tj 3.870588 0 Td 57.189542 Tz (carbon ) Tj 2.264706 0 Td 54.901961 Tz (tetra ) Tj 48.571429 0 0 48.571429 0 711 Tm 26.682353 0 Td 50.326797 Tz (chloride, ) Tj 2.861765 0 Td 55.882353 Tz (chlorobenzene, ) Tj 4.941176 0 Td 53.529412 Tz (1,2-dichlorobenzene, ) Tj 6.567647 0 Td 62.388592 Tz (N,N'-dimeth ) Tj 51.428571 0 0 51.428571 0 673.440678 Tm 25.180556 0 Td 54.822531 Tz (ylformamide, ) Tj 4.413889 0 Td 53.596866 Tz (N,N'-dimethyl ) Tj 4.647222 0 Td 52.175926 Tz (acetamide, ) Tj 3.616667 0 Td 57.175926 Tz (N-methyl-2-pyr ) Tj 51.428571 0 0 51.428571 0 629.104972 Tm 25.2 0 Td 47.890947 Tz (rolidone, ) Tj 3.713889 0 Td 50.591564 Tz (dimethylsulfoxide, ) Tj 6.591667 0 Td 49.826389 Tz (acetone, ) Tj 3.5 0 Td 46.616809 Tz (benzonitrile, ) Tj 51.428571 0 0 51.428571 0 587.719557 Tm 25.180556 0 Td 48.148148 Tz (triethylamine, ) Tj 4.316667 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 47.530864 Tz (pyridine. ) Tj 2.819444 0 Td 84.259259 Tz (A ) Tj 0.7 0 Td 47.800926 Tz (reaction ) Tj 2.566667 0 Td 50.462963 Tz (solvent ) Tj 2.352778 0 Td 51.851852 Tz (obtained ) Tj 2.702778 0 Td 61.574074 Tz (by ) Tj 51.428571 0 0 51.428571 0 543.669565 Tm 25.2 0 Td 57.253086 Tz (mixing ) Tj 2.216667 0 Td 59.41358 Tz (two ) Tj 1.263889 0 Td 50.231481 Tz (or ) Tj 0.777778 0 Td 60.763889 Tz (more ) Tj 1.594444 0 Td 52.5 Tz (kinds ) Tj 1.730556 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 60.763889 Tz (them ) Tj 1.672222 0 Td 66.975309 Tz (may ) Tj 1.361111 0 Td 58.333333 Tz (be ) Tj 0.836111 0 Td 55.902778 Tz (used ) Tj 1.497222 0 Td 58.333333 Tz (and ) Tj 1.186111 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 50.462963 Tz (solvent ) Tj 51.428571 0 0 51.428571 0 505.187105 Tm 25.180556 0 Td 59.62963 Tz (which ) Tj 2.022222 0 Td 55.092593 Tz (can ) Tj 1.263889 0 Td 49.016204 Tz (dissolve ) Tj 2.586111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 50.231481 Tz (ligand ) Tj 2.022222 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 51.635802 Tz (metal-providing ) Tj 4.861111 0 Td 53.148148 Tz (agent ) Tj 1.808333 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 467 Tm 25.2 0 Td 46.990741 Tz (preferred. ) Tj 48.571429 0 0 48.571429 0 420 Tm 27.464706 0 Td 51.470588 Tz (In ) Tj 1.008824 0 Td 49.509804 Tz (certain ) Tj 2.470588 0 Td 60.04902 Tz (embodiments, ) Tj 4.694118 0 Td 53.75817 Tz (the ) Tj 1.338235 0 Td 51.041667 Tz (reaction ) Tj 2.841176 0 Td 53.431373 Tz (solvent ) Tj 2.594118 0 Td 42.892157 Tz (is ) Tj 0.905882 0 Td 50.898693 Tz (water, ) Tj 48.571429 0 0 48.571429 0 378 Tm 26.682353 0 Td 46.719457 Tz (acetonitrile, ) Tj 3.911765 0 Td 56.617647 Tz (or ) Tj 0.885294 0 Td 61.764706 Tz (a ) Tj 0.658824 0 Td 56.372549 Tz (mixture ) Tj 2.614706 0 Td 48.897059 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 338.40404 Tm 25.938889 0 Td 52.572016 Tz (Reactions ) Tj 3.013889 0 Td 57.253086 Tz (can ) Tj 1.186111 0 Td 56.712963 Tz (be ) Tj 0.816667 0 Td 56.532922 Tz (performed ) Tj 3.227778 0 Td 45.37037 Tz (at ) Tj 0.680556 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 53.030303 Tz (temperature ) Tj 3.636111 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 53.796296 Tz (about ) Tj 1.769444 0 Td 62.654321 Tz (-10 ) Tj 51.428571 0 0 51.428571 0 294.511111 Tm 25.180556 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 56.712963 Tz (200 ) Tj 1.613889 0 Td 48.611111 Tz (C., ) Tj 1.127778 0 Td 46.450617 Tz (for ) Tj 1.069444 0 Td 55.092593 Tz (example, ) Tj 2.897222 0 Td 58.333333 Tz (0 ) Tj 0.602778 0 Td 45.37037 Tz (to ) Tj 0.836111 0 Td 55.092593 Tz (150 ) Tj 1.575 0 Td 46.450617 Tz (C., ) Tj 1.069444 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 61.574074 Tz (0 ) Tj 0.602778 0 Td 45.37037 Tz (to ) Tj 0.875 0 Td 53.472222 Tz (100 ) Tj 1.536111 0 Td 55.092593 Tz (C. ) Tj 0.855556 0 Td 64.814815 Tz (The ) Tj 51.428571 0 0 51.428571 0 253.520548 Tm 25.2 0 Td 48.611111 Tz (reaction ) Tj 2.508333 0 Td 55.092593 Tz (can ) Tj 1.166667 0 Td 56.712963 Tz (be ) Tj 0.836111 0 Td 56.17284 Tz (performed ) Tj 3.208333 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 55.092593 Tz (time ) Tj 1.458333 0 Td 52.391975 Tz (period ) Tj 2.061111 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 54.444444 Tz (about ) Tj 1.847222 0 Td 32.407407 Tz (1 ) Tj 0.466667 0 Td 56.17284 Tz (minute ) Tj 48.571429 0 0 48.571429 0 212 Tm 26.661765 0 Td 49.754902 Tz (to ) Tj 0.947059 0 Td 34.313725 Tz (1 ) Tj 0.576471 0 Td 59.705882 Tz (week, ) Tj 2.038235 0 Td 58.333333 Tz (Such ) Tj 1.626471 0 Td 48.039216 Tz (as, ) Tj 1.111765 0 Td 61.764706 Tz (5 ) Tj 0.638235 0 Td 57.352941 Tz (minutes ) Tj 2.655882 0 Td 49.754902 Tz (to ) Tj 0.864706 0 Td 65.196078 Tz (24 ) Tj 1.008824 0 Td 52.614379 Tz (hours, ) Tj 2.182353 0 Td 53.186275 Tz (or ) Tj 0.864706 0 Td 57.647059 Tz (about ) Tj 2.017647 0 Td 37.745098 Tz (1 ) Tj 0.555882 0 Td 60.906863 Tz (hour ) Tj 51.428571 0 0 51.428571 0 169.800253 Tm 25.180556 0 Td 45.37037 Tz (to ) Tj 0.875 0 Td 51.851852 Tz (12 ) Tj 0.836111 0 Td 49.691358 Tz (hours. ) Tj 2.002778 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 47.800926 Tz (reaction ) Tj 2.527778 0 Td 52.441077 Tz (temperature ) Tj 3.655556 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 47.800926 Tz (reaction ) Tj 2.547222 0 Td 53.472222 Tz (time ) Tj ET Q endstream endobj 274 0 obj << /Length 1 >> stream q endstream endobj 275 0 obj << /Length 49515 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.151351 0 Td 72.522523 Tz (13 ) Tj 51.428571 0 0 51.428571 0 2917.957055 Tm 6.261111 0 Td 55.092593 Tz (can ) Tj 1.186111 0 Td 49.421296 Tz (also ) Tj 1.380556 0 Td 58.333333 Tz (be ) Tj 0.894444 0 Td 49.608262 Tz (appropriately ) Tj 4.083333 0 Td 54.012346 Tz (optimized ) Tj 3.111111 0 Td 56.17284 Tz (depending ) Tj 3.227778 0 Td 56.712963 Tz (on ) Tj 0.913889 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 52.5 Tz (kinds ) Tj 51.428571 0 0 51.428571 0 2876.606383 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 1.011111 0 Td 50.771605 Tz (the ) Tj 1.322222 0 Td 47.222222 Tz (ligand, ) Tj 2.430556 0 Td 48.611111 Tz (the ) Tj 1.341667 0 Td 51.851852 Tz (metal-providing ) Tj 5.055556 0 Td 49.151235 Tz (agent, ) Tj 2.177778 0 Td 60.493827 Tz (and ) Tj 1.497222 0 Td 54.6875 Tz (chemical ) Tj 51.428571 0 0 51.428571 0 2832.511392 Tm 6.261111 0 Td 50.231481 Tz (reagents ) Tj 2.683333 0 Td 55.092593 Tz (used ) Tj 1.575 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 46.450617 Tz (reaction. ) Tj 51.428571 0 0 51.428571 0 2791.033792 Tm 7.019444 0 Td 52.572016 Tz (Reactions ) Tj 2.994444 0 Td 48.611111 Tz (for ) Tj 1.011111 0 Td 51.851852 Tz (preparing ) Tj 2.936111 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 53.148148 Tz (metal ) Tj 1.769444 0 Td 57.253086 Tz (complexes ) Tj 3.266667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 61.574074 Tz (inven ) Tj 51.428571 0 0 51.428571 0 2749.095238 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.477778 0 Td 68.055556 Tz (may ) Tj 1.536111 0 Td 54.012346 Tz (use ) Tj 1.283333 0 Td 49.259259 Tz (acids ) Tj 1.788889 0 Td 52.391975 Tz (and/or ) Tj 2.158333 0 Td 52.5 Tz (bases ) Tj 1.866667 0 Td 46.990741 Tz (to ) Tj 0.894444 0 Td 42.453704 Tz (facilitate ) Tj 2.838889 0 Td 37.808642 Tz (its ) Tj 0.991667 0 Td 48.611111 Tz (progress. ) Tj 40 0 0 40 0 2713 Tm 8.05 0 Td 73.333333 Tz (Acids ) Tj 2.475 0 Td 75 Tz (and ) Tj 1.625 0 Td 66.666667 Tz (bases ) Tj 2.325 0 Td 62.5 Tz (useful ) Tj 2.55 0 Td 58.333333 Tz (in ) Tj 0.975 0 Td 65.277778 Tz (the ) Tj 1.475 0 Td 75 Tz (methods ) Tj 3.425 0 Td 64.583333 Tz (herein ) Tj 2.6 0 Td 65.277778 Tz (are ) Tj 1.45 0 Td 83.333333 Tz (known ) Tj 2.85 0 Td 62.5 Tz (in ) Tj 51.428571 0 0 51.428571 0 2664.561769 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 38.078704 Tz (art. ) Tj 1.205556 0 Td 55.740741 Tz (Acids ) Tj 1.944444 0 Td 51.388889 Tz (include ) Tj 2.411111 0 Td 58.333333 Tz (any ) Tj 1.322222 0 Td 48.070988 Tz (acidic ) Tj 2.041667 0 Td 51.203704 Tz (chemicals, ) Tj 3.363889 0 Td 58.333333 Tz (which ) Tj 2.061111 0 Td 54.012346 Tz (can ) Tj 1.244444 0 Td 59.953704 Tz (be ) Tj 51.428571 0 0 51.428571 0 2626.08867 Tm 6.261111 0 Td 50.411523 Tz (inorganic ) Tj 3.013889 0 Td 40.509259 Tz (\(e.g., ) Tj 1.730556 0 Td 50.231481 Tz (ascorbic ) Tj 2.683333 0 Td 46.666667 Tz (acid, ) Tj 1.652778 0 Td 49.85755 Tz (hydrochloric, ) Tj 4.180556 0 Td 44.290123 Tz (Sulfuric, ) Tj 2.683333 0 Td 42.12963 Tz (nitric ) Tj 51.428571 0 0 51.428571 0 2584.688504 Tm 6.261111 0 Td 46.450617 Tz (acids, ) Tj 1.963889 0 Td 60.763889 Tz (aluminum ) Tj 3.208333 0 Td 45.640432 Tz (trichloride\) ) Tj 3.597222 0 Td 50.231481 Tz (or ) Tj 0.855556 0 Td 51.388889 Tz (organic ) Tj 2.469444 0 Td 40.509259 Tz (\(e.g., ) Tj 1.730556 0 Td 60.601852 Tz (camphorsul ) Tj 51.428571 0 0 51.428571 0 2543.168153 Tm 6.261111 0 Td 49.259259 Tz (fonic ) Tj 1.866667 0 Td 46.018519 Tz (acid, ) Tj 1.730556 0 Td 49.945534 Tz (p-toluenesulfonic ) Tj 5.463889 0 Td 46.666667 Tz (acid, ) Tj 1.769444 0 Td 46.450617 Tz (acetic ) Tj 2.061111 0 Td 46.018519 Tz (acid, ) Tj 1.730556 0 Td 52.932099 Tz (ytterbium ) Tj 51.428571 0 0 51.428571 0 2498.374831 Tm 6.241667 0 Td 40.329218 Tz (triflate\) ) Tj 2.508333 0 Td 46.990741 Tz (in ) Tj 0.933333 0 Td 46.759259 Tz (nature. ) Tj 2.313889 0 Td 55.740741 Tz (Acids ) Tj 2.022222 0 Td 49.691358 Tz (are ) Tj 1.263889 0 Td 48.611111 Tz (useful ) Tj 2.119444 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 46.990741 Tz (either ) Tj 2.002778 0 Td 45.730453 Tz (catalytic ) Tj 2.819444 0 Td 53.472222 Tz (or ) Tj 40 0 0 40 0 2464 Tm 8.075 0 Td 63.392857 Tz (Stoichiometric ) Tj 5.825 0 Td 75 Tz (amounts ) Tj 3.675 0 Td 58.333333 Tz (to ) Tj 1.225 0 Td 54.583333 Tz (facilitate ) Tj 3.75 0 Td 65.277778 Tz (the ) Tj 1.675 0 Td 59.583333 Tz (reactions. ) Tj 4.15 0 Td 70.833333 Tz (Bases ) Tj 51.428571 0 0 51.428571 0 2416.748718 Tm 6.261111 0 Td 46.666667 Tz (refer ) Tj 1.613889 0 Td 46.990741 Tz (to ) Tj 0.816667 0 Td 57.253086 Tz (any ) Tj 1.302778 0 Td 49.259259 Tz (basic ) Tj 1.730556 0 Td 51.527778 Tz (chemicals, ) Tj 3.344444 0 Td 58.333333 Tz (which ) Tj 2.041667 0 Td 54.012346 Tz (can ) Tj 1.225 0 Td 58.333333 Tz (be ) Tj 0.933333 0 Td 50.411523 Tz (inorganic ) Tj 2.975 0 Td 40.509259 Tz (\(e.g., ) Tj 51.428571 0 0 51.428571 0 2377.864078 Tm 6.280556 0 Td 58.333333 Tz (Sodium ) Tj 2.333333 0 Td 49.421296 Tz (bicarbonate, ) Tj 3.811111 0 Td 54.372428 Tz (potassium ) Tj 3.169444 0 Td 53.148148 Tz (hydroxide\) ) Tj 3.441667 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 51.388889 Tz (organic ) Tj 2.391667 0 Td 40.509259 Tz (\(e.g., ) Tj 51.428571 0 0 51.428571 0 2334.438424 Tm 6.241667 0 Td 48.611111 Tz (triethylamine, ) Tj 4.258333 0 Td 50.05144 Tz (pyridine\) ) Tj 2.916667 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 45.833333 Tz (nature. ) Tj 2.216667 0 Td 55.092593 Tz (Bases ) Tj 1.808333 0 Td 50.771605 Tz (are ) Tj 1.108333 0 Td 49.151235 Tz (useful ) Tj 2.002778 0 Td 42.12963 Tz (in ) Tj 0.719444 0 Td 47.530864 Tz (either ) Tj 51.428571 0 0 51.428571 0 2291.298969 Tm 6.261111 0 Td 45.37037 Tz (catalytic ) Tj 2.8 0 Td 53.472222 Tz (or ) Tj 0.952778 0 Td 49.305556 Tz (Stoichiometric ) Tj 4.472222 0 Td 58.333333 Tz (amounts ) Tj 2.780556 0 Td 46.990741 Tz (to ) Tj 0.933333 0 Td 42.12963 Tz (facilitate ) Tj 2.858333 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 59.143519 Tz (reac ) Tj 40 0 0 40 0 2256 Tm 8.025 0 Td 56.944444 Tz (tions. ) Tj 51.428571 0 0 51.428571 0 2212.561798 Tm 7 0 Td 48.361823 Tz (Additionally, ) Tj 4.025 0 Td 49.537037 Tz (various ) Tj 2.275 0 Td 49.789562 Tz (preparation ) Tj 3.5 0 Td 47.314815 Tz (steps ) Tj 1.633333 0 Td 68.055556 Tz (may ) Tj 1.380556 0 Td 59.953704 Tz (be ) Tj 0.875 0 Td 56.893004 Tz (performed ) Tj 51.428571 0 0 51.428571 0 2167.085603 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 56.712963 Tz (an ) Tj 0.913889 0 Td 46.8107 Tz (alternate ) Tj 2.8 0 Td 55.092593 Tz (sequence ) Tj 2.897222 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 52.5 Tz (order ) Tj 1.788889 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 52.662037 Tz (give ) Tj 1.497222 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50 Tz (desired ) Tj 2.372222 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2126.576923 Tm 6.261111 0 Td 54.444444 Tz (complexes. ) Tj 3.538889 0 Td 46.990741 Tz (In ) Tj 0.777778 0 Td 47.530864 Tz (addition, ) Tj 2.761111 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 46.8107 Tz (solvents, ) Tj 2.722222 0 Td 50.854701 Tz (temperatures, ) Tj 4.180556 0 Td 49.421296 Tz (reaction ) Tj 51.428571 0 0 51.428571 0 2083.346939 Tm 6.261111 0 Td 47.962963 Tz (durations, ) Tj 3.188889 0 Td 41.319444 Tz (etc. ) Tj 1.322222 0 Td 49.907407 Tz (delineated ) Tj 3.247222 0 Td 51.311728 Tz (herein ) Tj 2.1 0 Td 51.851852 Tz (are ) Tj 1.225 0 Td 47.530864 Tz (for ) Tj 1.127778 0 Td 53.472222 Tz (purposes ) Tj 2.877778 0 Td 56.712963 Tz (of ) Tj 0.875 0 Td 49.907407 Tz (illus ) Tj 51.428571 0 0 51.428571 0 2043.325953 Tm 6.241667 0 Td 45.37037 Tz (tration ) Tj 2.080556 0 Td 52.662037 Tz (only ) Tj 1.438889 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 57.253086 Tz (one ) Tj 1.186111 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 51.446759 Tz (ordinary ) Tj 2.644444 0 Td 40.833333 Tz (skill ) Tj 1.380556 0 Td 46.990741 Tz (in ) Tj 0.719444 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 43.209877 Tz (art ) Tj 0.913889 0 Td 46.990741 Tz (will ) Tj 1.283333 0 Td 52.572016 Tz (recognize ) Tj 51.428571 0 0 51.428571 0 2000.277487 Tm 6.241667 0 Td 46.990741 Tz (that ) Tj 1.458333 0 Td 47.530864 Tz (variation ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 48.611111 Tz (reaction ) Tj 2.702778 0 Td 49.907407 Tz (conditions ) Tj 3.344444 0 Td 55.092593 Tz (can ) Tj 1.322222 0 Td 56.481481 Tz (produce ) Tj 2.702778 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1960.942308 Tm 6.261111 0 Td 50 Tz (desired ) Tj 2.313889 0 Td 53.148148 Tz (metal ) Tj 1.769444 0 Td 57.613169 Tz (complexes ) Tj 3.305556 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 50.925926 Tz (present ) Tj 2.333333 0 Td 47.962963 Tz (invention. ) Tj 3.130556 0 Td 50.411523 Tz (Synthetic ) Tj 51.428571 0 0 51.428571 0 1918.650943 Tm 6.261111 0 Td 52.932099 Tz (chemistry ) Tj 3.052778 0 Td 50.771605 Tz (transformations ) Tj 4.763889 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 49.583333 Tz (protecting ) Tj 3.15 0 Td 56.388889 Tz (group ) Tj 1.925 0 Td 61.574074 Tz (methodolo ) Tj 51.428571 0 0 51.428571 0 1879.881499 Tm 6.261111 0 Td 48.611111 Tz (gies ) Tj 1.380556 0 Td 47.727273 Tz (\(protection ) Tj 3.363889 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 49.608262 Tz (deprotection\) ) Tj 4.083333 0 Td 48.611111 Tz (useful ) Tj 1.944444 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 50.501543 Tz (synthesizing ) Tj 3.830556 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1833.58 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.866667 0 Td 56.893004 Tz (complexes ) Tj 3.305556 0 Td 51.851852 Tz (described ) Tj 3.013889 0 Td 50.231481 Tz (herein ) Tj 2.022222 0 Td 50.771605 Tz (are ) Tj 1.127778 0 Td 65.462963 Tz (known ) Tj 2.197222 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 45.37037 Tz (art ) Tj 0.991667 0 Td 61.574074 Tz (and ) Tj 51.428571 0 0 51.428571 0 1792.380353 Tm 6.261111 0 Td 48.206019 Tz (include, ) Tj 2.527778 0 Td 49.691358 Tz (for ) Tj 1.05 0 Td 55.497685 Tz (example, ) Tj 2.858333 0 Td 51.851852 Tz (those ) Tj 1.788889 0 Td 54.282407 Tz (Such ) Tj 1.516667 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 51.49177 Tz (described ) Tj 2.994444 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 50.231481 Tz (R. ) Tj 0.875 0 Td 51.851852 Tz (Larock, ) Tj 51.428571 0 0 51.428571 0 1752.36342 Tm 6.261111 0 Td 58.582621 Tz (Comprehensive ) Tj 4.841667 0 Td 55.092593 Tz (Organic ) Tj 2.547222 0 Td 51.851852 Tz (Transformations, ) Tj 5.25 0 Td 84.259259 Tz (VCH ) Tj 1.827778 0 Td 49.907407 Tz (Publishers ) Tj 51.428571 0 0 51.428571 0 1709.112245 Tm 6.280556 0 Td 50.462963 Tz (\(1989\); ) Tj 2.294444 0 Td 46.990741 Tz (T. ) Tj 0.797222 0 Td 64.814815 Tz (W. ) Tj 0.972222 0 Td 58.873457 Tz (Greene ) Tj 2.294444 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 37.268519 Tz (P. ) Tj 0.7 0 Td 56.712963 Tz (G. ) Tj 0.913889 0 Td 66.435185 Tz (M. ) Tj 1.030556 0 Td 54.444444 Tz (Wuts, ) Tj 1.886111 0 Td 48.935185 Tz (Protective ) Tj 3.169444 0 Td 58.873457 Tz (Groups ) Tj 51.428571 0 0 51.428571 0 1669.596977 Tm 6.280556 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 56.481481 Tz (Organic ) Tj 2.566667 0 Td 47.314815 Tz (Synthesis, ) Tj 3.091667 0 Td 49.691358 Tz (2d. ) Tj 1.147222 0 Td 46.990741 Tz (Ed., ) Tj 1.341667 0 Td 56.712963 Tz (John ) Tj 1.575 0 Td 57.685185 Tz (Wiley ) Tj 1.925 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 58.333333 Tz (Sons ) Tj 1.613889 0 Td 50.462963 Tz (\(1991\); ) Tj 52.857143 0 0 52.857143 0 1624.403141 Tm 6.110811 0 Td 47.297297 Tz (L. ) Tj 0.889189 0 Td 47.822823 Tz (Fieser ) Tj 1.948649 0 Td 57.807808 Tz (and ) Tj 1.286486 0 Td 64.63964 Tz (M. ) Tj 1.116216 0 Td 43.243243 Tz (Fieser, ) Tj 2.118919 0 Td 49.399399 Tz (Fieser ) Tj 2.062162 0 Td 59.90991 Tz (and ) Tj 1.324324 0 Td 46.903153 Tz (Fieser's ) Tj 2.591892 0 Td 52.815315 Tz (Reagents ) Tj 2.781081 0 Td 49.399399 Tz (for ) Tj 51.428571 0 0 51.428571 0 1585.824234 Tm 6.280556 0 Td 56.944444 Tz (Organic ) Tj 2.722222 0 Td 47.962963 Tz (Synthesis, ) Tj 3.227778 0 Td 57.523148 Tz (John ) Tj 1.75 0 Td 57.037037 Tz (Wiley ) Tj 2.041667 0 Td 60.493827 Tz (and ) Tj 1.419444 0 Td 59.143519 Tz (Sons ) Tj 1.769444 0 Td 50.462963 Tz (\(1994\); ) Tj 2.488889 0 Td 58.333333 Tz (and ) Tj 1.438889 0 Td 46.990741 Tz (L. ) Tj 51.428571 0 0 51.428571 0 1546.606516 Tm 6.280556 0 Td 49.331276 Tz (Paquette, ) Tj 2.955556 0 Td 43.75 Tz (ed., ) Tj 1.380556 0 Td 54.012346 Tz (Encyclopedia ) Tj 4.2 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 53.472222 Tz (Reagents ) Tj 2.858333 0 Td 50.771605 Tz (for ) Tj 1.186111 0 Td 56.944444 Tz (Organic ) Tj 2.644444 0 Td 72.376543 Tz (Syn ) Tj 51.428571 0 0 51.428571 0 1501.466019 Tm 6.261111 0 Td 43.055556 Tz (thesis, ) Tj 2.002778 0 Td 56.712963 Tz (John ) Tj 1.555556 0 Td 57.037037 Tz (Wiley ) Tj 1.886111 0 Td 59.41358 Tz (and ) Tj 1.244444 0 Td 57.523148 Tz (Sons ) Tj 1.594444 0 Td 49.074074 Tz (\(1995\), ) Tj 2.236111 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 53.796296 Tz (subsequent ) Tj 3.363889 0 Td 48.206019 Tz (editions ) Tj 40 0 0 40 0 1465 Tm 8.025 0 Td 59.895833 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 1419.469677 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.302778 0 Td 53.472222 Tz (prepared ) Tj 2.780556 0 Td 53.148148 Tz (metal ) Tj 1.808333 0 Td 57.253086 Tz (complexes ) Tj 3.325 0 Td 54.012346 Tz (can ) Tj 1.166667 0 Td 58.333333 Tz (be ) Tj 0.894444 0 Td 51.131687 Tz (separated ) Tj 2.975 0 Td 56.712963 Tz (from ) Tj 1.594444 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1375.515892 Tm 6.261111 0 Td 48.611111 Tz (reaction ) Tj 2.586111 0 Td 52.777778 Tz (mixture ) Tj 2.391667 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 47.685185 Tz (further ) Tj 2.177778 0 Td 47.395833 Tz (purified ) Tj 2.430556 0 Td 61.574074 Tz (by ) Tj 0.933333 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 58.873457 Tz (method ) Tj 2.333333 0 Td 52.211934 Tz (described ) Tj 51.428571 0 0 51.428571 0 1335.066849 Tm 6.241667 0 Td 50.771605 Tz (herein ) Tj 2.294444 0 Td 52.932099 Tz (and/or ) Tj 2.313889 0 Td 61.574074 Tz (by ) Tj 1.263889 0 Td 54.282407 Tz (methods, ) Tj 3.091667 0 Td 54.282407 Tz (such ) Tj 1.769444 0 Td 44.290123 Tz (as, ) Tj 1.263889 0 Td 58.333333 Tz (a ) Tj 0.797222 0 Td 46.323529 Tz (recrystallization ) Tj 51.428571 0 0 51.428571 0 1294.673077 Tm 6.261111 0 Td 56.018519 Tz (method, ) Tj 2.527778 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 49.331276 Tz (redeposit ) Tj 2.858333 0 Td 55.092593 Tz (method, ) Tj 2.508333 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 58.333333 Tz (a ) Tj 0.505556 0 Td 56.712963 Tz (chromatography ) Tj 4.977778 0 Td 55.092593 Tz (method. ) Tj 51.428571 0 0 51.428571 0 1251.316644 Tm 6.280556 0 Td 46.990741 Tz (Further, ) Tj 2.625 0 Td 59.41358 Tz (two ) Tj 1.419444 0 Td 53.472222 Tz (or ) Tj 0.972222 0 Td 62.384259 Tz (more ) Tj 1.827778 0 Td 59.953704 Tz (of ) Tj 0.972222 0 Td 48.611111 Tz (the ) Tj 1.225 0 Td 49.259259 Tz (separation ) Tj 3.344444 0 Td 57.87037 Tz (methods ) Tj 2.819444 0 Td 66.975309 Tz (may ) Tj 1.536111 0 Td 59.953704 Tz (be ) Tj 51.428571 0 0 51.428571 0 1211.794466 Tm 6.261111 0 Td 59.953704 Tz (employed ) Tj 3.247222 0 Td 43.75 Tz (in ) Tj 0.875 0 Td 52.932099 Tz (combination. ) Tj 4.141667 0 Td 68.055556 Tz (As ) Tj 1.147222 0 Td 55.092593 Tz (can ) Tj 1.341667 0 Td 59.953704 Tz (be ) Tj 1.030556 0 Td 51.262626 Tz (appreciated ) Tj 3.694444 0 Td 61.574074 Tz (by ) Tj 1.108333 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1168.548503 Tm 6.280556 0 Td 45.833333 Tz (skilled ) Tj 2.119444 0 Td 43.75 Tz (artisan, ) Tj 2.294444 0 Td 48.611111 Tz (further ) Tj 2.216667 0 Td 57.407407 Tz (methods ) Tj 2.625 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 50.501543 Tz (synthesizing ) Tj 3.791667 0 Td 52.932099 Tz (and/or ) Tj 2.061111 0 Td 64.00463 Tz (sepa ) Tj 51.428571 0 0 51.428571 0 1126.540816 Tm 6.261111 0 Td 47.530864 Tz (rating ) Tj 1.963889 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 57.973251 Tz (complexes ) Tj 3.383333 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 55.497685 Tz (formulae ) Tj 2.897222 0 Td 50.771605 Tz (herein ) Tj 2.1 0 Td 46.180556 Tz (will ) Tj 1.380556 0 Td 58.333333 Tz (be ) Tj 51.428571 0 0 51.428571 0 1084.795053 Tm 6.261111 0 Td 51.388889 Tz (evident ) Tj 2.411111 0 Td 45.37037 Tz (to ) Tj 0.797222 0 Td 51.203704 Tz (those ) Tj 1.769444 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 51.446759 Tz (ordinary ) Tj 2.741667 0 Td 41.481481 Tz (skill ) Tj 1.497222 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 38.888889 Tz (art. ) Tj 51.428571 0 0 51.428571 0 1047.590038 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 56.30787 Tz (produced ) Tj 2.975 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 65.895062 Tz (may ) Tj 1.419444 0 Td 47.138047 Tz (precipitate ) Tj 3.344444 0 Td 56.17284 Tz (depending ) Tj 51.428571 0 0 51.428571 0 1001.84456 Tm 6.261111 0 Td 61.574074 Tz (on ) Tj 1.030556 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 54.282407 Tz (kind ) Tj 1.575 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 48.206019 Tz (reaction ) Tj 2.625 0 Td 46.990741 Tz (solvent; ) Tj 2.586111 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 48.070988 Tz (precipitated ) Tj 3.772222 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 962.247874 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.683333 0 Td 55.092593 Tz (can ) Tj 1.147222 0 Td 58.333333 Tz (be ) Tj 0.855556 0 Td 47.800926 Tz (isolated ) Tj 2.430556 0 Td 58.333333 Tz (and ) Tj 1.186111 0 Td 47.800926 Tz (purified ) Tj 2.430556 0 Td 61.574074 Tz (by ) Tj 0.933333 0 Td 49.583333 Tz (separating ) Tj 3.130556 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 52.5 Tz (metal ) Tj 51.428571 0 0 51.428571 0 921.912281 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.741667 0 Td 58.333333 Tz (by ) Tj 0.952778 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 46.450617 Tz (solid-liquid ) Tj 3.558333 0 Td 49.907407 Tz (separation ) Tj 3.266667 0 Td 59.953704 Tz (method ) Tj 2.391667 0 Td 54.282407 Tz (such ) Tj 1.536111 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 44.290123 Tz (filtra ) Tj 51.428571 0 0 51.428571 0 880.757412 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.516667 0 Td 60.493827 Tz (and ) Tj 1.477778 0 Td 49.907407 Tz (Subjecting ) Tj 3.363889 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 50.771605 Tz (separated ) Tj 3.091667 0 Td 53.240741 Tz (product ) Tj 2.625 0 Td 46.990741 Tz (to ) Tj 0.952778 0 Td 58.333333 Tz (a ) Tj 0.758333 0 Td 57.407407 Tz (washing ) Tj 51.428571 0 0 51.428571 0 839.666667 Tm 6.261111 0 Td 50.771605 Tz (operation ) Tj 2.994444 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 52.391975 Tz (drying ) Tj 2.138889 0 Td 50.411523 Tz (operation ) Tj 2.955556 0 Td 51.851852 Tz (as ) Tj 0.894444 0 Td 47.530864 Tz (required. ) Tj 51.428571 0 0 51.428571 0 795.840849 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.438889 0 Td 50.411523 Tz (invention ) Tj 3.072222 0 Td 47.222222 Tz (further ) Tj 2.236111 0 Td 52.256944 Tz (provides ) Tj 2.838889 0 Td 52.391975 Tz (design ) Tj 2.197222 0 Td 59.41358 Tz (and ) Tj 1.380556 0 Td 48.971193 Tz (synthesis ) Tj 2.936111 0 Td 59.953704 Tz (of ) Tj 51.428571 0 0 51.428571 0 752.915601 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.886111 0 Td 56.893004 Tz (complexes ) Tj 3.305556 0 Td 46.990741 Tz (that ) Tj 1.341667 0 Td 50.771605 Tz (are ) Tj 1.166667 0 Td 48.611111 Tz (useful ) Tj 1.983333 0 Td 51.851852 Tz (as ) Tj 0.894444 0 Td 45.730453 Tz (catalysts ) Tj 2.722222 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 55.092593 Tz (redox ) Tj 1.925 0 Td 59.143519 Tz (reac ) Tj 40 0 0 40 0 717 Tm 8.025 0 Td 56.944444 Tz (tions. ) Tj 51.428571 0 0 51.428571 0 669.690799 Tm 6.280556 0 Td 53.240741 Tz (Density ) Tj 2.527778 0 Td 50.87963 Tz (Functional ) Tj 3.286111 0 Td 58.333333 Tz (Theory ) Tj 2.352778 0 Td 61.574074 Tz (\(DFT\) ) Tj 2.080556 0 Td 50.771605 Tz (Calculations ) Tj 40 0 0 40 0 634 Tm 9 0 Td 64.393939 Tz (Theoretical ) Tj 4.475 0 Td 62.152778 Tz (calculations ) Tj 4.775 0 Td 75 Tz (were ) Tj 2.025 0 Td 62.5 Tz (carried ) Tj 2.9 0 Td 65.277778 Tz (out ) Tj 1.45 0 Td 67.708333 Tz (with ) Tj 1.9 0 Td 63.888889 Tz (the ) Tj 1.35 0 Td 87.5 Tz (Gauss ) Tj 51.428571 0 0 51.428571 0 585.243995 Tm 6.261111 0 Td 48.611111 Tz (ian ) Tj 1.108333 0 Td 59.953704 Tz (09 ) Tj 0.913889 0 Td 52.662037 Tz (Software ) Tj 2.722222 0 Td 56.944444 Tz (package ) Tj 2.586111 0 Td 58.333333 Tz (\(M. ) Tj 1.244444 0 Td 38.888889 Tz (J. ) Tj 0.738889 0 Td 49.151235 Tz (Frisch ) Tj 1.963889 0 Td 46.990741 Tz (et ) Tj 0.719444 0 Td 38.078704 Tz (al., ) Tj 1.108333 0 Td 52.932099 Tz (Gaussian, ) Tj 3.091667 0 Td 41.481481 Tz (Inc., ) Tj 51.428571 0 0 51.428571 0 545.975031 Tm 6.261111 0 Td 51.041667 Tz (Wallingford, ) Tj 3.947222 0 Td 54.552469 Tz (Conn., ) Tj 2.275 0 Td 51.311728 Tz (2009\). ) Tj 2.197222 0 Td 52.777778 Tz (Density ) Tj 2.547222 0 Td 48.611111 Tz (functional ) Tj 3.208333 0 Td 51.311728 Tz (theory ) Tj 2.177778 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 502.498008 Tm 6.241667 0 Td 55.902778 Tz (used ) Tj 1.769444 0 Td 52.662037 Tz (with ) Tj 1.691667 0 Td 72.376543 Tz (PBE ) Tj 1.711111 0 Td 57.118056 Tz (exchange ) Tj 3.130556 0 Td 58.333333 Tz (and ) Tj 1.438889 0 Td 47.727273 Tz (correlation ) Tj 3.577778 0 Td 48.316498 Tz (functionals ) Tj 3.597222 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 463.958435 Tm 6.261111 0 Td 51.58179 Tz (conjunctions ) Tj 3.966667 0 Td 51.851852 Tz (with ) Tj 1.497222 0 Td 48.611111 Tz (default ) Tj 2.236111 0 Td 56.17284 Tz (pruned ) Tj 2.236111 0 Td 52.932099 Tz (course ) Tj 2.1 0 Td 48.611111 Tz (grids ) Tj 1.711111 0 Td 47.530864 Tz (for ) Tj 1.05 0 Td 49.331276 Tz (gradients ) Tj 51.428571 0 0 51.428571 0 419.764861 Tm 6.261111 0 Td 58.333333 Tz (and ) Tj 1.341667 0 Td 52.662037 Tz (Hessians ) Tj 2.838889 0 Td 46.180556 Tz (\(35, ) Tj 1.458333 0 Td 51.851852 Tz (110\) ) Tj 1.75 0 Td 49.074074 Tz (neither ) Tj 2.294444 0 Td 49.421296 Tz (grid ) Tj 1.458333 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 57.253086 Tz (pruned ) Tj 2.333333 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 51.851852 Tz (cobalt, ) Tj 51.428571 0 0 51.428571 0 379.440415 Tm 6.261111 0 Td 58.333333 Tz (and ) Tj 1.4 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 48.148148 Tz (default ) Tj 2.391667 0 Td 71.296296 Tz (SCF ) Tj 1.633333 0 Td 55.681818 Tz (convergence ) Tj 4.025 0 Td 45.37037 Tz (criterion ) Tj 2.838889 0 Td 47.530864 Tz (for ) Tj 1.166667 0 Td 57.928241 Tz (geometry ) Tj 57.142857 0 0 57.142857 0 338.2 Tm 5.635 0 Td 45.769231 Tz (optimizations ) Tj 3.7975 0 Td 67.8125 Tz (\(10\) ) Tj 1.855 0 Td 44.722222 Tz (\(R. ) Tj 1.0675 0 Td 49.583333 Tz (G. ) Tj 0.8575 0 Td 45.9375 Tz (Parr ) Tj 1.295 0 Td 40.833333 Tz (et ) Tj 0.7 0 Td 33.541667 Tz (al., ) Tj 1.085 0 Td 46.666667 Tz (Density ) Tj 2.2225 0 Td 47.833333 Tz (Functional ) Tj 51.428571 0 0 51.428571 0 295.57072 Tm 6.3 0 Td 55.632716 Tz (Theory ) Tj 2.294444 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 60.925926 Tz (Atoms ) Tj 2.1 0 Td 63.734568 Tz (and ) Tj 1.380556 0 Td 52.5 Tz (Molecules, ) Tj 3.422222 0 Td 59.41358 Tz (Oxford ) Tj 2.391667 0 Td 50.555556 Tz (University ) Tj 3.363889 0 Td 45.910494 Tz (Press, ) Tj 51.428571 0 0 51.428571 0 251.851752 Tm 6.241667 0 Td 76.697531 Tz (New ) Tj 1.594444 0 Td 53.148148 Tz (York, ) Tj 1.886111 0 Td 52.5 Tz (1989; ) Tj 1.827778 0 Td 37.268519 Tz (J. ) Tj 0.7 0 Td 38.888889 Tz (P. ) Tj 0.738889 0 Td 59.953704 Tz (Perdew ) Tj 2.411111 0 Td 45.37037 Tz (et ) Tj 0.738889 0 Td 36.458333 Tz (al., ) Tj 1.147222 0 Td 51.203704 Tz (Phys. ) Tj 1.847222 0 Td 46.990741 Tz (Rev. ) Tj 1.477778 0 Td 39.537037 Tz (Lett. ) Tj 1.555556 0 Td 51.203704 Tz (1996, ) Tj 51.428571 0 0 51.428571 0 210.793893 Tm 6.261111 0 Td 56.588319 Tz (77.3865-3868; ) Tj 4.588889 0 Td 59.41358 Tz (and ) Tj 1.205556 0 Td 37.268519 Tz (J. ) Tj 0.661111 0 Td 38.888889 Tz (P. ) Tj 0.680556 0 Td 59.41358 Tz (Perdew ) Tj 2.333333 0 Td 42.12963 Tz (et ) Tj 0.661111 0 Td 36.458333 Tz (al., ) Tj 1.108333 0 Td 50.555556 Tz (Phys. ) Tj 1.769444 0 Td 46.180556 Tz (Rev. ) Tj 1.4 0 Td 40.185185 Tz (Lett. ) Tj 1.497222 0 Td 51.203704 Tz (1997, ) Tj 51.428571 0 0 51.428571 0 168 Tm 6.261111 0 Td 50.771605 Tz (78, ) Tj 1.186111 0 Td 50.231481 Tz (1396\). ) Tj 2.041667 0 Td 70.216049 Tz (Two ) Tj 1.477778 0 Td 49.259259 Tz (basis ) Tj 1.711111 0 Td 45.37037 Tz (set ) Tj 1.011111 0 Td 54.552469 Tz (combinations ) Tj 4.180556 0 Td 58.333333 Tz (were ) Tj 1.613889 0 Td 45.37037 Tz (utilized ) Tj 2.411111 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 43.75 Tz (this ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.502778 0 Td 74.537037 Tz (14 ) Tj 51.428571 0 0 51.428571 0 2914.497436 Tm 25.219444 0 Td 45.910494 Tz (study. ) Tj 1.925 0 Td 55.092593 Tz (For ) Tj 1.205556 0 Td 56.712963 Tz (BS1, ) Tj 1.575 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 47.962963 Tz (basis ) Tj 1.672222 0 Td 44.290123 Tz (set ) Tj 0.991667 0 Td 45.37037 Tz (utilized ) Tj 2.372222 0 Td 47.530864 Tz (for ) Tj 1.011111 0 Td 50.231481 Tz (cobalt ) Tj 2.002778 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 65.895062 Tz (Hay ) Tj 51.428571 0 0 51.428571 0 2871.313131 Tm 25.2 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 63.194444 Tz (Wadt ) Tj 1.711111 0 Td 49.259259 Tz (basis ) Tj 1.711111 0 Td 45.37037 Tz (set ) Tj 1.069444 0 Td 56.712963 Tz (\(BS\) ) Tj 1.594444 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 46.450617 Tz (effective ) Tj 2.702778 0 Td 53.472222 Tz (core ) Tj 1.516667 0 Td 46.8107 Tz (potential ) Tj 2.780556 0 Td 60.277778 Tz (\(ECP\) ) Tj 51.428571 0 0 51.428571 0 2827.338481 Tm 25.2 0 Td 54.79798 Tz (combination ) Tj 3.986111 0 Td 62.294239 Tz (\(LanL2DZ\) ) Tj 3.694444 0 Td 48.611111 Tz (as ) Tj 0.952778 0 Td 53.472222 Tz (modified ) Tj 2.858333 0 Td 61.574074 Tz (by ) Tj 1.069444 0 Td 59.62963 Tz (Couty ) Tj 2.080556 0 Td 59.41358 Tz (and ) Tj 1.419444 0 Td 46.018519 Tz (Hall, ) Tj 51.428571 0 0 51.428571 0 2783.800995 Tm 25.180556 0 Td 60.277778 Tz (where ) Tj 2.002778 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 59.41358 Tz (two ) Tj 1.283333 0 Td 54.012346 Tz (outermost ) Tj 3.111111 0 Td 58.333333 Tz (p ) Tj 0.563889 0 Td 49.691358 Tz (functions ) Tj 2.897222 0 Td 57.523148 Tz (have ) Tj 1.575 0 Td 56.712963 Tz (been ) Tj 1.613889 0 Td 50.636574 Tz (replaced ) Tj 2.605556 0 Td 61.574074 Tz (by ) Tj 51.428571 0 0 51.428571 0 2741.717185 Tm 25.2 0 Td 51.851852 Tz (a ) Tj 0.661111 0 Td 50.231481 Tz (\(41\) ) Tj 1.516667 0 Td 42.12963 Tz (split ) Tj 1.555556 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 54.012346 Tz (optimized ) Tj 3.227778 0 Td 49.691358 Tz (cobalt ) Tj 2.1 0 Td 58.333333 Tz (4p ) Tj 1.05 0 Td 47.890947 Tz (function; ) Tj 2.916667 0 Td 59.41358 Tz (and ) Tj 1.380556 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 2695.62484 Tm 25.219444 0 Td 51.851852 Tz (6-31 ) Tj 1.322222 0 Td 62.384259 Tz (G\(d\) ) Tj 1.672222 0 Td 48.611111 Tz (basis ) Tj 1.672222 0 Td 44.560185 Tz (sets ) Tj 1.263889 0 Td 59.143519 Tz (were ) Tj 1.613889 0 Td 55.902778 Tz (used ) Tj 1.536111 0 Td 47.530864 Tz (for ) Tj 1.011111 0 Td 41.049383 Tz (all ) Tj 0.933333 0 Td 50.555556 Tz (other ) Tj 1.691667 0 Td 57.037037 Tz (atoms ) Tj 1.944444 0 Td 38.888889 Tz (\(P. ) Tj 0.913889 0 Td 37.268519 Tz (J. ) Tj 0.680556 0 Td 65.895062 Tz (Hay ) Tj 51.428571 0 0 51.428571 0 2652.776623 Tm 25.2 0 Td 43.75 Tz (et ) Tj 0.719444 0 Td 35.648148 Tz (al., ) Tj 1.069444 0 Td 38.888889 Tz (J. ) Tj 0.738889 0 Td 60.277778 Tz (Chem. ) Tj 2.080556 0 Td 50.555556 Tz (Phys. ) Tj 1.847222 0 Td 51.203704 Tz (1985, ) Tj 1.75 0 Td 56.565657 Tz (82,299-310; ) Tj 3.966667 0 Td 66.435185 Tz (M. ) Tj 0.972222 0 Td 60.277778 Tz (Couty ) Tj 1.983333 0 Td 46.990741 Tz (et ) Tj 0.719444 0 Td 37.268519 Tz (al., ) Tj 1.088889 0 Td 38.888889 Tz (J. ) Tj 51.428571 0 0 51.428571 0 2611.298153 Tm 25.219444 0 Td 56.944444 Tz (Comput. ) Tj 2.722222 0 Td 60.277778 Tz (Chem. ) Tj 2.138889 0 Td 51.851852 Tz (1996, ) Tj 1.847222 0 Td 47.530864 Tz (17, ) Tj 1.166667 0 Td 54.12037 Tz (1359-1370; ) Tj 3.5 0 Td 64.814815 Tz (W. ) Tj 1.011111 0 Td 37.268519 Tz (J. ) Tj 0.738889 0 Td 57.685185 Tz (Hehre ) Tj 1.944444 0 Td 45.37037 Tz (et ) Tj 0.738889 0 Td 37.268519 Tz (al., ) Tj 1.088889 0 Td 40.509259 Tz (J. ) Tj 51.428571 0 0 51.428571 0 2568.820779 Tm 25.219444 0 Td 59.62963 Tz (Chem. ) Tj 2.061111 0 Td 51.203704 Tz (Phys. ) Tj 1.847222 0 Td 51.851852 Tz (1972, ) Tj 1.769444 0 Td 48.611111 Tz (56, ) Tj 1.05 0 Td 55.740741 Tz (2257; ) Tj 1.847222 0 Td 93.981481 Tz (& ) Tj 0.797222 0 Td 38.888889 Tz (P. ) Tj 0.680556 0 Td 55.092593 Tz (C. ) Tj 0.894444 0 Td 52.932099 Tz (Hariharan ) Tj 3.033333 0 Td 45.37037 Tz (et ) Tj 0.7 0 Td 39.969136 Tz (al. ) Tj 0.972222 0 Td 48.070988 Tz (Theor: ) Tj 51.428571 0 0 51.428571 0 2527 Tm 25.219444 0 Td 55.740741 Tz (Chim. ) Tj 1.944444 0 Td 55.902778 Tz (Acta ) Tj 1.652778 0 Td 52.5 Tz (1973, ) Tj 1.827778 0 Td 49.691358 Tz (28, ) Tj 1.147222 0 Td 52.211934 Tz (213-222\). ) Tj 48.571429 0 0 48.571429 0 2487 Tm 27.444118 0 Td 61.764706 Tz (For ) Tj 1.297059 0 Td 62.622549 Tz (BS2, ) Tj 1.708824 0 Td 52.614379 Tz (the ) Tj 1.111765 0 Td 43.464052 Tz (all ) Tj 0.988235 0 Td 51.470588 Tz (electron ) Tj 2.738235 0 Td 63.671024 Tz (6-311+G** ) Tj 3.685294 0 Td 50.784314 Tz (basis ) Tj 1.729412 0 Td 48.039216 Tz (sets ) Tj 1.358824 0 Td 62.622549 Tz (were ) Tj 1.688235 0 Td 60.04902 Tz (used ) Tj 51.428571 0 0 51.428571 0 2443.812834 Tm 25.2 0 Td 49.691358 Tz (for ) Tj 1.069444 0 Td 41.049383 Tz (all ) Tj 0.972222 0 Td 57.685185 Tz (atoms ) Tj 2.002778 0 Td 48.611111 Tz (\(R. ) Tj 1.147222 0 Td 55.092593 Tz (Krishnan ) Tj 2.897222 0 Td 43.75 Tz (et ) Tj 0.738889 0 Td 37.268519 Tz (al., ) Tj 1.088889 0 Td 42.12963 Tz (J. ) Tj 0.816667 0 Td 60.277778 Tz (Chem. ) Tj 2.158333 0 Td 49.259259 Tz (Phys. ) Tj 1.866667 0 Td 51.851852 Tz (1980, ) Tj 1.788889 0 Td 49.691358 Tz (72, ) Tj 51.428571 0 0 51.428571 0 2404.944083 Tm 25.219444 0 Td 54.282407 Tz (650-654; ) Tj 2.858333 0 Td 56.712963 Tz (K. ) Tj 0.952778 0 Td 55.362654 Tz (Raghavachari ) Tj 4.219444 0 Td 45.37037 Tz (et ) Tj 0.777778 0 Td 37.268519 Tz (al., ) Tj 1.088889 0 Td 42.12963 Tz (J. ) Tj 0.816667 0 Td 60.277778 Tz (Chem. ) Tj 2.138889 0 Td 50.555556 Tz (Phys. ) Tj 1.886111 0 Td 50.555556 Tz (1989, ) Tj 1.788889 0 Td 49.691358 Tz (91, ) Tj 51.428571 0 0 51.428571 0 2361.477707 Tm 25.258333 0 Td 54.12037 Tz (1062-1065; ) Tj 3.519444 0 Td 38.888889 Tz (P. ) Tj 0.680556 0 Td 40.509259 Tz (J. ) Tj 0.719444 0 Td 55.092593 Tz (Hay, ) Tj 1.516667 0 Td 38.888889 Tz (J. ) Tj 0.777778 0 Td 58.981481 Tz (Chem. ) Tj 2.1 0 Td 49.907407 Tz (Phys. ) Tj 1.827778 0 Td 52.5 Tz (1977, ) Tj 1.808333 0 Td 56.837607 Tz (66,4377-4384; ) Tj 51.428571 0 0 51.428571 0 2319.77193 Tm 25.2 0 Td 58.333333 Tz (A. ) Tj 0.855556 0 Td 37.268519 Tz (J. ) Tj 0.680556 0 Td 53.472222 Tz (H. ) Tj 0.816667 0 Td 51.851852 Tz (Wachters, ) Tj 2.955556 0 Td 40.509259 Tz (J. ) Tj 0.7 0 Td 60.925926 Tz (Chem. ) Tj 2.061111 0 Td 49.907407 Tz (Phys. ) Tj 1.769444 0 Td 51.851852 Tz (1970, ) Tj 1.730556 0 Td 49.691358 Tz (52, ) Tj 1.108333 0 Td 53.030303 Tz (1033-1036\). ) Tj 3.616667 0 Td 64.814815 Tz (The ) Tj 51.428571 0 0 51.428571 0 2281.957055 Tm 25.2 0 Td 49.537037 Tz (density ) Tj 2.313889 0 Td 41.666667 Tz (fitting ) Tj 1.925 0 Td 54.594017 Tz (approximation ) Tj 4.511111 0 Td 47.530864 Tz (for ) Tj 1.030556 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 41.203704 Tz (fitting ) Tj 1.925 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 63.888889 Tz (Coulomb ) Tj 51.428571 0 0 51.428571 0 2238.653165 Tm 25.2 0 Td 47.170782 Tz (potential ) Tj 2.8 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 55.902778 Tz (used ) Tj 1.575 0 Td 48.611111 Tz (for ) Tj 1.088889 0 Td 39.969136 Tz (all ) Tj 1.011111 0 Td 72.376543 Tz (PBE ) Tj 1.555556 0 Td 46.866097 Tz (calculations; ) Tj 3.927778 0 Td 47.170782 Tz (auxiliary ) Tj 2.858333 0 Td 70.216049 Tz (den ) Tj 51.428571 0 0 51.428571 0 2198.834532 Tm 25.219444 0 Td 41.859568 Tz (sity-fitting ) Tj 3.208333 0 Td 48.611111 Tz (basis ) Tj 1.672222 0 Td 49.691358 Tz (functions ) Tj 2.897222 0 Td 59.143519 Tz (were ) Tj 1.613889 0 Td 52.572016 Tz (generated ) Tj 3.033333 0 Td 50.605413 Tz (automatically ) Tj 4.2 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 2155.635359 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 48.251029 Tz (specified ) Tj 2.858333 0 Td 87.5 Tz (AO ) Tj 1.361111 0 Td 47.962963 Tz (basis ) Tj 1.769444 0 Td 44.290123 Tz (set ) Tj 1.127778 0 Td 48.611111 Tz (\(B. ) Tj 1.244444 0 Td 29.166667 Tz (I. ) Tj 0.7 0 Td 54.62963 Tz (Dunlap, ) Tj 2.586111 0 Td 38.888889 Tz (J. ) Tj 0.875 0 Td 59.62963 Tz (Chem. ) Tj 2.197222 0 Td 49.907407 Tz (Phys. ) Tj 51.428571 0 0 51.428571 0 2112.194937 Tm 25.258333 0 Td 51.851852 Tz (1983, ) Tj 1.808333 0 Td 50.771605 Tz (78, ) Tj 1.147222 0 Td 55.740741 Tz (3140-3142; ) Tj 3.636111 0 Td 51.851852 Tz (B. ) Tj 0.894444 0 Td 30.787037 Tz (I. ) Tj 0.641667 0 Td 54.62963 Tz (Dunlap, ) Tj 2.527778 0 Td 61.574074 Tz (J ) Tj 0.583333 0 Td 63.734568 Tz (Mol ) Tj 1.4 0 Td 56.481481 Tz (Struc-Theochem ) Tj 51.428571 0 0 51.428571 0 2070.975968 Tm 25.2 0 Td 54.444444 Tz (2000, ) Tj 1.847222 0 Td 51.851852 Tz (529, ) Tj 1.497222 0 Td 52.391975 Tz (37-40; ) Tj 2.158333 0 Td 50.231481 Tz (B. ) Tj 0.855556 0 Td 34.027778 Tz (I. ) Tj 0.661111 0 Td 58.333333 Tz (Dunlap ) Tj 2.333333 0 Td 42.12963 Tz (et ) Tj 0.738889 0 Td 36.458333 Tz (al., ) Tj 1.069444 0 Td 40.509259 Tz (J. ) Tj 0.797222 0 Td 59.62963 Tz (Chem. ) Tj 2.1 0 Td 49.907407 Tz (Phys. ) Tj 1.847222 0 Td 51.203704 Tz (1979, ) Tj 51.428571 0 0 51.428571 0 2029.932468 Tm 25.2 0 Td 48.611111 Tz (71, ) Tj 1.088889 0 Td 55.740741 Tz (3396-3402; ) Tj 3.558333 0 Td 53.472222 Tz (B. ) Tj 0.875 0 Td 29.166667 Tz (I. ) Tj 0.602778 0 Td 58.333333 Tz (Dunlap ) Tj 2.294444 0 Td 42.12963 Tz (et ) Tj 0.7 0 Td 37.268519 Tz (al., ) Tj 1.05 0 Td 40.509259 Tz (J. ) Tj 0.738889 0 Td 60.277778 Tz (Chem. ) Tj 2.080556 0 Td 50.555556 Tz (Phys. ) Tj 1.808333 0 Td 51.851852 Tz (1979, ) Tj 1.75 0 Td 49.691358 Tz (71, ) Tj 51.428571 0 0 51.428571 0 1989.594628 Tm 25.2 0 Td 53.914141 Tz (4993-4999\). ) Tj 3.752778 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 53.703704 Tz (Hessian ) Tj 2.508333 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 60.358796 Tz (computed ) Tj 3.111111 0 Td 58.333333 Tz (on ) Tj 0.933333 0 Td 53.292181 Tz (gas-phase ) Tj 3.072222 0 Td 57.523148 Tz (opti ) Tj 51.428571 0 0 51.428571 0 1945.623616 Tm 25.2 0 Td 59.62963 Tz (mized ) Tj 2.022222 0 Td 53.472222 Tz (geometries ) Tj 3.461111 0 Td 59.41358 Tz (and ) Tj 1.341667 0 Td 51.041667 Tz (standard ) Tj 2.741667 0 Td 41.245791 Tz (statistical ) Tj 3.033333 0 Td 54.12037 Tz (mechanical ) Tj 3.538889 0 Td 55.092593 Tz (rela ) Tj 51.428571 0 0 51.428571 0 1905.453739 Tm 25.180556 0 Td 48.971193 Tz (tionships ) Tj 2.897222 0 Td 58.333333 Tz (were ) Tj 1.613889 0 Td 55.902778 Tz (used ) Tj 1.575 0 Td 45.37037 Tz (to ) Tj 0.797222 0 Td 54.012346 Tz (determine ) Tj 3.15 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 57.253086 Tz (change ) Tj 2.275 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 58.333333 Tz (Gibbs ) Tj 2.041667 0 Td 51.851852 Tz (Free ) Tj 58.571429 0 0 58.571429 0 1860.220149 Tm 22.126829 0 Td 47.899729 Tz (energy ) Tj 1.895122 0 Td 42.682927 Tz (in ) Tj 0.682927 0 Td 43.631436 Tz (the ) Tj 0.939024 0 Td 47.425474 Tz (gas ) Tj 1.041463 0 Td 44.579946 Tz (phase, ) Tj 1.792683 0 Td 92.95393 Tz (AG. ) Tj 1.860976 0 Td 55.01355 Tz (The ) Tj 1.178049 0 Td 42.999097 Tz (solvation ) Tj 2.492683 0 Td 41.971545 Tz (free ) Tj 1.178049 0 Td 41.734417 Tz (energies, ) Tj 50 0 0 50 0 1821.561848 Tm 25.92 0 Td 81.666667 Tz (AG ) Tj 2.52 0 Td 61.666667 Tz (were ) Tj 1.9 0 Td 50.666667 Tz (calculated ) Tj 3.44 0 Td 54.666667 Tz (using ) Tj 2.06 0 Td 51.111111 Tz (the ) Tj 1.32 0 Td 90 Tz (SMD ) Tj 2.08 0 Td 61.666667 Tz (method ) Tj 2.64 0 Td 52.222222 Tz (\(A. ) Tj 1.4 0 Td 48.333333 Tz (V. ) Tj 25.714286 0 0 25.714286 0 1819 Tm 52.305556 0 Td 108.024691 Tz (so: ) Tj 51.428571 0 0 51.428571 0 1778.822134 Tm 25.2 0 Td 57.928241 Tz (Marenich ) Tj 3.052778 0 Td 45.37037 Tz (et ) Tj 0.758333 0 Td 37.268519 Tz (al., ) Tj 1.147222 0 Td 38.888889 Tz (J. ) Tj 0.816667 0 Td 50.555556 Tz (Phys. ) Tj 1.866667 0 Td 60.277778 Tz (Chem. ) Tj 2.138889 0 Td 71.296296 Tz (B ) Tj 0.680556 0 Td 53.796296 Tz (2009, ) Tj 1.963889 0 Td 48.611111 Tz (113, ) Tj 1.477778 0 Td 53.619529 Tz (6378-6396\). ) Tj 51.428571 0 0 51.428571 0 1738.04305 Tm 25.2 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 86.419753 Tz (SMD ) Tj 1.75 0 Td 48.611111 Tz (solvation ) Tj 2.858333 0 Td 58.981481 Tz (model ) Tj 1.944444 0 Td 62.654321 Tz (was ) Tj 1.322222 0 Td 55.092593 Tz (used ) Tj 1.497222 0 Td 53.472222 Tz (with ) Tj 1.458333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 48.148148 Tz (default ) Tj 2.177778 0 Td 68.703704 Tz (param ) Tj 40 0 0 40 0 1703 Tm 32.4 0 Td 58.333333 Tz (eters ) Tj 2.05 0 Td 62.916667 Tz (consistent ) Tj 4.075 0 Td 68.75 Tz (with ) Tj 2 0 Td 70 Tz (water ) Tj 2.375 0 Td 75 Tz (and ) Tj 1.625 0 Td 59.027778 Tz (acetonitrile ) Tj 4.55 0 Td 64.583333 Tz (as ) Tj 1.1 0 Td 63.888889 Tz (the ) Tj 1.475 0 Td 59.895833 Tz (solvent. ) Tj 51.428571 0 0 51.428571 0 1656.454318 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 47.800926 Tz (reaction ) Tj 2.488889 0 Td 47.800926 Tz (free ) Tj 1.302778 0 Td 54.552469 Tz (energy ) Tj 2.158333 0 Td 55.555556 Tz (changes ) Tj 2.527778 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.231481 Tz (possible ) Tj 2.605556 0 Td 59.305556 Tz (mechanisms ) Tj 51.428571 0 0 51.428571 0 1613.194514 Tm 25.2 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 54.444444 Tz (water ) Tj 1.788889 0 Td 59.143519 Tz (were ) Tj 1.594444 0 Td 49.259259 Tz (calculated ) Tj 3.130556 0 Td 53.472222 Tz (with ) Tj 1.477778 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 46.990741 Tz (free ) Tj 1.302778 0 Td 54.552469 Tz (energy ) Tj 2.158333 0 Td 55.092593 Tz (changes ) Tj 2.547222 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 1571.514007 Tm 25.2 0 Td 52.932099 Tz (gas ) Tj 1.127778 0 Td 55.092593 Tz (phase ) Tj 1.808333 0 Td 58.333333 Tz (and ) Tj 1.186111 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 48.971193 Tz (Solvation ) Tj 2.819444 0 Td 47.800926 Tz (free ) Tj 1.283333 0 Td 50.231481 Tz (energies ) Tj 2.586111 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 47.530864 Tz (reactants ) Tj 2.722222 0 Td 59.41358 Tz (and ) Tj 51.428571 0 0 51.428571 0 1532.225847 Tm 25.2 0 Td 51.851852 Tz (products ) Tj 2.741667 0 Td 43.75 Tz (in ) Tj 0.758333 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 58.009259 Tz (Born-Haber ) Tj 3.636111 0 Td 52.5 Tz (cycle ) Tj 1.769444 0 Td 51.041667 Tz (\(Eq. ) Tj 1.516667 0 Td 38.888889 Tz (1\). ) Tj 0.913889 0 Td 64.814815 Tz (The ) Tj 1.322222 0 Td 60.358796 Tz (computed ) Tj 3.130556 0 Td 46.990741 Tz (free ) Tj 51.428571 0 0 51.428571 0 1487.030928 Tm 25.2 0 Td 54.012346 Tz (energy ) Tj 2.197222 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 46.450617 Tz (solution, ) Tj 2.741667 0 Td 82.098765 Tz (AG, ) Tj 1.925 0 Td 54.444444 Tz (...", ) Tj 1.886111 0 Td 40.509259 Tz (is ) Tj 0.738889 0 Td 49.259259 Tz (calculated ) Tj 3.188889 0 Td 57.523148 Tz (from ) Tj 1.672222 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 46.180556 Tz (free ) Tj 25.714286 0 0 25.714286 0 1486 Tm 63.933333 0 Td 87.5 Tz (so ) Tj 1.594444 0 Td 68.055556 Tz (in ) Tj 51.428571 0 0 51.428571 0 1450.198263 Tm 25.2 0 Td 54.012346 Tz (energy ) Tj 2.430556 0 Td 57.253086 Tz (change ) Tj 2.508333 0 Td 45.37037 Tz (in ) Tj 0.991667 0 Td 50.771605 Tz (the ) Tj 1.341667 0 Td 55.092593 Tz (gas ) Tj 1.438889 0 Td 55.092593 Tz (phase ) Tj 2.138889 0 Td 56.712963 Tz (of ) Tj 1.030556 0 Td 50.771605 Tz (the ) Tj 1.361111 0 Td 55.092593 Tz (redox ) Tj 2.119444 0 Td 49.537037 Tz (couple, ) Tj 25.714286 0 0 25.714286 0 1427 Tm 53.977778 0 Td 68.055556 Tz (readix ) Tj 58.571429 0 0 58.571429 0 1400.396927 Tm 22.126829 0 Td 116.666667 Tz (AG", ) Tj 3.107317 0 Td 42.682927 Tz (the ) Tj 1.058537 0 Td 43.315266 Tz (solvation ) Tj 2.629268 0 Td 40.54878 Tz (free ) Tj 1.263415 0 Td 47.899729 Tz (energy ) Tj 1.980488 0 Td 50.745257 Tz (change ) Tj 2.1 0 Td 50.813008 Tz (between ) Tj 2.42439 0 Td 42.682927 Tz (the ) Tj 51.428571 0 0 51.428571 0 1362.256975 Tm 25.2 0 Td 52.256944 Tz (oxidized ) Tj 3.461111 0 Td 104.166667 Tz (AG'\(ox\) ) Tj 5.347222 0 Td 61.574074 Tz (and ) Tj 1.866667 0 Td 48.611111 Tz (the ) Tj 1.633333 0 Td 54.62963 Tz (reduced ) Tj 3.072222 0 Td 49.537037 Tz (species ) Tj 51.428571 0 0 51.428571 0 1321.24173 Tm 25.413889 0 Td 157.716049 Tz (AG' ) Tj 3.344444 0 Td 50.771605 Tz (\(red\), ) Tj 2.002778 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 62.114198 Tz (number ) Tj 2.411111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 49.421296 Tz (protons, ) Tj 2.586111 0 Td 43.75 Tz (lost ) Tj 1.244444 0 Td 57.523148 Tz (from ) Tj 1.613889 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1279.931398 Tm 25.2 0 Td 59.259259 Tz (complex ) Tj 2.741667 0 Td 46.990741 Tz (to ) Tj 0.816667 0 Td 48.611111 Tz (Solution ) Tj 2.605556 0 Td 45.37037 Tz (\(n\) ) Tj 1.069444 0 Td 44.560185 Tz (\(Eq. ) Tj 1.341667 0 Td 38.888889 Tz (1\). ) Tj 1.011111 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 51.203704 Tz (order ) Tj 1.769444 0 Td 48.611111 Tz (to ) Tj 0.816667 0 Td 54.166667 Tz (account ) Tj 2.488889 0 Td 49.691358 Tz (for ) Tj 1.088889 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 1239.066158 Tm 25.2 0 Td 46.990741 Tz (loss ) Tj 1.380556 0 Td 55.092593 Tz (of ) Tj 0.797222 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 51.851852 Tz (proton ) Tj 2.119444 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 50 Tz (solvent ) Tj 2.333333 0 Td 54.444444 Tz (water ) Tj 1.827778 0 Td 51.851852 Tz (or ) Tj 0.816667 0 Td 43.874644 Tz (acetonitrile, ) Tj 3.675 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 57.79321 Tz (experi ) Tj 61.428571 0 0 61.428571 0 1190.072993 Tm 21.097674 0 Td 45.671835 Tz (mental ) Tj 1.823256 0 Td 44.496124 Tz (value ) Tj 1.497674 0 Td 39.793282 Tz (for ) Tj 0.846512 0 Td 41.602067 Tz (the ) Tj 0.911628 0 Td 41.300603 Tz (solvation ) Tj 2.393023 0 Td 47.48062 Tz (of ) Tj 0.651163 0 Td 46.124031 Tz (a ) Tj 0.439535 0 Td 44.315245 Tz (proton ) Tj 1.790698 0 Td 71.085271 Tz (\(AG,"\(H\)=- ) Tj 52.857143 0 0 52.857143 0 1153 Tm 24.518919 0 Td 52.972973 Tz (265.9 ) Tj 1.854054 0 Td 51.238739 Tz (kcal/mol ) Tj 2.724324 0 Td 56.756757 Tz (and ) Tj 1.286486 0 Td 74.099099 Tz (AG ) Tj 4.502703 0 Td 55.323505 Tz (\(H"\)=-260.2 ) Tj 3.897297 0 Td 49.74975 Tz (kcal/mol\) ) Tj 58.571429 0 0 58.571429 0 1111.201624 Tm 22.126829 0 Td 51.219512 Tz (and ) Tj 1.143902 0 Td 43.631436 Tz (the ) Tj 0.990244 0 Td 46.793135 Tz (gas-phase ) Tj 2.731707 0 Td 51.219512 Tz (Gibbs ) Tj 1.741463 0 Td 41.971545 Tz (free ) Tj 1.229268 0 Td 46.476965 Tz (energy ) Tj 1.929268 0 Td 49.796748 Tz (of ) Tj 0.734146 0 Td 48.373984 Tz (a ) Tj 0.512195 0 Td 46.95122 Tz (proton ) Tj 2.031707 0 Td 88.211382 Tz (AG. ) Tj 58.571429 0 0 58.571429 0 1071.058824 Tm 22.143902 0 Td 48.943089 Tz (\(H"\)=-6.28 ) Tj 3.243902 0 Td 44.105691 Tz (kcal ) Tj 1.34878 0 Td 61.178862 Tz (mol" ) Tj 1.997561 0 Td 52.642276 Tz (were ) Tj 1.553659 0 Td 48.373984 Tz (used ) Tj 1.434146 0 Td 43.631436 Tz (\(C. ) Tj 1.07561 0 Td 34.146341 Tz (P. ) Tj 0.717073 0 Td 47.804878 Tz (Kelly ) Tj 1.690244 0 Td 38.414634 Tz (et ) Tj 0.734146 0 Td 32.723577 Tz (al., ) Tj 1.041463 0 Td 35.569106 Tz (J. ) Tj 51.428571 0 0 51.428571 0 1031.414141 Tm 25.2 0 Td 51.203704 Tz (Phys. ) Tj 1.769444 0 Td 60.277778 Tz (Chem. ) Tj 2.022222 0 Td 71.296296 Tz (B ) Tj 0.563889 0 Td 53.796296 Tz (2006, ) Tj 1.847222 0 Td 54.282407 Tz (111,408-422: ) Tj 4.083333 0 Td 55.092593 Tz (C. ) Tj 0.816667 0 Td 38.888889 Tz (P. ) Tj 0.661111 0 Td 53.148148 Tz (Kelly ) Tj 1.75 0 Td 42.12963 Tz (et ) Tj 0.641667 0 Td 37.268519 Tz (al., ) Tj 1.030556 0 Td 38.888889 Tz (J. ) Tj 0.7 0 Td 50.555556 Tz (Phys. ) Tj 48.571429 0 0 48.571429 0 989 Tm 26.702941 0 Td 63.823529 Tz (Chem. ) Tj 2.285294 0 Td 72.058824 Tz (B ) Tj 0.7 0 Td 58.333333 Tz (2006, ) Tj 2.1 0 Td 52.328431 Tz (110, ) Tj 1.605882 0 Td 58.619281 Tz (16066-16081; ) Tj 4.55 0 Td 61.764706 Tz (and ) Tj 1.358824 0 Td 60.04902 Tz (A. ) Tj 1.008824 0 Td 67.254902 Tz (Moser ) Tj 2.264706 0 Td 46.323529 Tz (et ) Tj 0.844118 0 Td 37.745098 Tz (al., ) Tj 1.173529 0 Td 42.892157 Tz (J. ) Tj 51.428571 0 0 51.428571 0 947.153153 Tm 25.2 0 Td 51.851852 Tz (Phys. ) Tj 1.866667 0 Td 59.62963 Tz (Chem. ) Tj 2.119444 0 Td 71.296296 Tz (B ) Tj 0.661111 0 Td 54.444444 Tz (2010, ) Tj 1.944444 0 Td 48.611111 Tz (114, ) Tj 1.458333 0 Td 54.095442 Tz (13911-13921\). ) Tj 52.857143 0 0 52.857143 0 861 Tm 26.145946 0 Td 90.09009 Tz (AGP=AG, ) Tj 4.256757 0 Td 50.45045 Tz (redoxicone+AGP\(red\)- ) Tj 42.857143 0 0 42.857143 0 828.685185 Tm 33.6 0 Td 60.925926 Tz (AG. ) Tj 2.286667 0 Td 67.307692 Tz ("P\(ox\)-n/AG.,\(H\)+AG.P\(H'\) ) Tj 13.976667 0 Td 42.777778 Tz (Eq. ) Tj 1.026667 0 Td 38.888889 Tz (1 ) Tj 40 0 0 40 0 779 Tm 32.4 0 Td 83.333333 Tz (AG. ) Tj 2.3 0 Td 65.625 Tz (...' ) Tj 2.15 0 Td 58.333333 Tz (in ) Tj 0.925 0 Td 58.680556 Tz (acetonitrile ) Tj 4.4 0 Td 65.277778 Tz (are ) Tj 1.375 0 Td 70.833333 Tz (used ) Tj 1.925 0 Td 58.333333 Tz (to ) Tj 0.925 0 Td 69.444444 Tz (determine ) Tj 3.95 0 Td 63.888889 Tz (the ) Tj 1.35 0 Td 66.145833 Tz (standard ) Tj 25.714286 0 0 25.714286 0 771 Tm 52.305556 0 Td 84.259259 Tz (so ) Tj 1.438889 0 Td 61.574074 Tz (in ) Tj 58.571429 0 0 58.571429 0 730.807747 Tm 22.126829 0 Td 51.219512 Tz (one ) Tj 1.212195 0 Td 42.682927 Tz (electron ) Tj 2.356098 0 Td 47.804878 Tz (redox ) Tj 1.741463 0 Td 39.837398 Tz (potential, ) Tj 2.697561 0 Td 64.02439 Tz (E. ) Tj 1.792683 0 Td 68.292683 Tz ('", ) Tj 1.553659 0 Td 51.788618 Tz (where ) Tj 1.860976 0 Td 56.910569 Tz (F ) Tj 0.631707 0 Td 34.146341 Tz (is ) Tj 0.7 0 Td 44.579946 Tz (the ) Tj 58.571429 0 0 58.571429 0 691.110599 Tm 22.126829 0 Td 49.186992 Tz (Faraday ) Tj 2.236585 0 Td 42.682927 Tz (constant, ) Tj 2.526829 0 Td 47.804878 Tz (23.06 ) Tj 1.621951 0 Td 44.817073 Tz (kcal ) Tj 1.280488 0 Td 68.292683 Tz (mol'V' ) Tj 2.714634 0 Td 49.322493 Tz (\(Eq2\). ) Tj 47.142857 0 0 47.142857 0 564 Tm 32.433333 0 Td 94.276094 Tz (AGE ) Tj 31.428571 0 0 31.428571 0 530 Tm 49.127273 0 Td 53.030303 Tz (1 ) Tj 0.540909 0 Td 114.015152 Tz (XF ) Tj 40 0 0 40 0 573.085106 Tm 53.35 0 Td 66.666667 Tz (Eq ) Tj 1.1 0 Td 62.5 Tz (2 ) Tj 31.428571 0 0 31.428571 0 564 Tm 45.118182 0 Td 54.090909 Tz (.comp ) Tj 22.857143 0 0 22.857143 0 543 Tm 61.64375 0 Td 69.270833 Tz (so ) Tj 1.05 0 Td 54.6875 Tz (in ) Tj 51.428571 0 0 51.428571 0 419.785997 Tm 25.2 0 Td 50.231481 Tz (Calculations ) Tj 4.044444 0 Td 58.333333 Tz (on ) Tj 1.127778 0 Td 55.740741 Tz (Metal ) Tj 2.061111 0 Td 60.853909 Tz (Complexes ) Tj 3.675 0 Td 59.953704 Tz (of ) Tj 1.05 0 Td 48.611111 Tz (the ) Tj 1.283333 0 Td 51.131687 Tz (Invention ) Tj 3.15 0 Td 60.493827 Tz (and ) Tj 40 0 0 40 0 384 Tm 32.425 0 Td 64.583333 Tz (Possible ) Tj 3.4 0 Td 78.75 Tz (Mechanisms ) Tj 51.428571 0 0 51.428571 0 338.14 Tm 25.919444 0 Td 63.194444 Tz (To ) Tj 0.913889 0 Td 53.240741 Tz (provide ) Tj 2.372222 0 Td 47.222222 Tz (insight ) Tj 2.119444 0 Td 46.990741 Tz (into ) Tj 1.283333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 60.493827 Tz (mechanism ) Tj 3.441667 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 52.391975 Tz (proton ) Tj 2.080556 0 Td 50.771605 Tz (reduction ) Tj 51.428571 0 0 51.428571 0 297.320592 Tm 25.180556 0 Td 61.574074 Tz (by ) Tj 0.933333 0 Td 60.185185 Tz (complex ) Tj 2.761111 0 Td 40.509259 Tz (2. ) Tj 0.758333 0 Td 73.45679 Tz (DFT ) Tj 1.516667 0 Td 48.341049 Tz (calculations ) Tj 3.713889 0 Td 58.333333 Tz (were ) Tj 1.613889 0 Td 56.532922 Tz (performed ) Tj 3.227778 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 52.314815 Tz (explore ) Tj 51.428571 0 0 51.428571 0 252.276705 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.225 0 Td 50.231481 Tz (possible ) Tj 2.761111 0 Td 47.800926 Tz (reaction ) Tj 2.663889 0 Td 48.611111 Tz (intermediates, ) Tj 4.413889 0 Td 59.41358 Tz (and ) Tj 1.4 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 48.206019 Tz (reaction ) Tj 2.683333 0 Td 46.990741 Tz (free ) Tj 51.428571 0 0 51.428571 0 215.796526 Tm 25.2 0 Td 54.012346 Tz (energy ) Tj 2.236111 0 Td 55.555556 Tz (changes ) Tj 2.625 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 50.231481 Tz (possible ) Tj 2.663889 0 Td 57.523148 Tz (pathways ) Tj 3.033333 0 Td 48.611111 Tz (for ) Tj 1.108333 0 Td 52.932099 Tz (proton ) Tj 2.216667 0 Td 50.771605 Tz (reduction ) Tj 51.428571 0 0 51.428571 0 168 Tm 25.219444 0 Td 48.611111 Tz (\(see ) Tj 1.361111 0 Td 54.444444 Tz (Table ) Tj 1.925 0 Td 40.509259 Tz (1, ) Tj 0.758333 0 Td 60.648148 Tz (Schemes ) Tj 2.780556 0 Td 84.259259 Tz (A ) Tj 0.7 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 68.055556 Tz (B ) Tj 0.661111 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 54.282407 Tz (FIG. ) Tj 1.594444 0 Td 46.180556 Tz (14\). ) Tj ET Q endstream endobj 276 0 obj << /Length 1 >> stream q endstream endobj 277 0 obj << /Length 12077 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.151351 0 Td 74.099099 Tz (15 ) Tj 18.445946 0 Td 72.522523 Tz (16 ) Tj 51.428571 0 0 51.428571 0 2917.295165 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.302778 0 Td 59.953704 Tz (computed ) Tj 3.072222 0 Td 50.411523 Tz (reduction ) Tj 2.916667 0 Td 47.314815 Tz (potentials ) Tj 3.052778 0 Td 55.092593 Tz (of ) Tj 0.797222 0 Td 59.259259 Tz (complex ) Tj 2.663889 0 Td 58.333333 Tz (2 ) Tj 0.544444 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 55.092593 Tz (water ) Tj 40 0 0 40 0 2882 Tm 8.05 0 Td 63.888889 Tz (are ) Tj 1.475 0 Td 80 Tz (shown ) Tj 2.75 0 Td 58.333333 Tz (in ) Tj 1 0 Td 69.166667 Tz (Table ) Tj 2.475 0 Td 47.916667 Tz (1. ) Tj 38.571429 0 0 38.571429 0 2794 Tm 18.07037 0 Td 101.111111 Tz (TABLE ) Tj 3.448148 0 Td 25.925926 Tz (1. ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 40 0 0 40 0 2726.002762 Tm 9.125 0 Td 54.513889 Tz (Experimental ) Tj 4.15 0 Td 58.333333 Tz (and ) Tj 1.325 0 Td 58.854167 Tz (computed ) Tj 3.1 0 Td 55 Tz (redox ) Tj 1.875 0 Td 47.083333 Tz (potentials ) Tj 3.075 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 59.52381 Tz (complex ) Tj 2.75 0 Td 54.166667 Tz (2 ) Tj 0.575 0 Td 43.75 Tz (in ) Tj 0.8 0 Td 49.305556 Tz (water, ) Tj 40 0 0 40 0 2688 Tm 16.975 0 Td 75 Tz (EL, ) Tj 1.575 0 Td 83.333333 Tz (V ) Tj 0.775 0 Td 54.166667 Tz (vs ) Tj 0.875 0 Td 76.388889 Tz (SHE ) Tj 32.857143 0 0 32.857143 0 2628 Tm 17.834783 0 Td 67.210145 Tz (Exp. ) Tj 7.63913 0 Td 77.777778 Tz (BS1 ) Tj 7.547826 0 Td 79.468599 Tz (BS2 ) Tj 31.785714 0 0 31.785714 0 2567 Tm 11.640449 0 Td 70.786517 Tz (CoIIII ) Tj 7.110112 0 Td 64.23221 Tz (O.15 ) Tj 7.770787 0 Td 65.543071 Tz (O.09 ) Tj 7.770787 0 Td 66.853933 Tz (O.08 ) Tj 31.428571 0 0 31.428571 0 2535.227273 Tm 12.027273 0 Td 65.757576 Tz (Colli ) Tj 6.427273 0 Td 70 Tz (-O.90 ) Tj 7.859091 0 Td 70 Tz (-1.07 ) Tj 7.859091 0 Td 68.939394 Tz (-O.71 ) Tj 5.440909 0 Td 71.590909 Tz (10 ) Tj 51.428571 0 0 51.428571 0 2428.380435 Tm 7 0 Td 56.018519 Tz (Without ) Tj 2.625 0 Td 54.62963 Tz (wishing ) Tj 2.566667 0 Td 46.990741 Tz (to ) Tj 0.836111 0 Td 58.333333 Tz (be ) Tj 0.952778 0 Td 60.925926 Tz (bound ) Tj 2.1 0 Td 59.953704 Tz (by ) Tj 0.972222 0 Td 59.41358 Tz (any ) Tj 1.361111 0 Td 46.759259 Tz (theory, ) Tj 2.275 0 Td 63.734568 Tz (Scheme ) Tj 2.527778 0 Td 87.5 Tz (A ) Tj 51.428571 0 0 51.428571 0 2388.58209 Tm 6.261111 0 Td 49.421296 Tz (presents ) Tj 2.702778 0 Td 49.826389 Tz (possible ) Tj 2.722222 0 Td 59.305556 Tz (mechanisms ) Tj 3.888889 0 Td 58.333333 Tz (of ) Tj 0.991667 0 Td 77.777778 Tz (H ) Tj 1.05 0 Td 51.203704 Tz (evolution/production ) Tj 51.428571 0 0 51.428571 0 2345.841808 Tm 6.261111 0 Td 51.131687 Tz (catalyzed ) Tj 2.975 0 Td 61.574074 Tz (by ) Tj 1.011111 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 49.691358 Tz (cobalt ) Tj 2.002778 0 Td 57.613169 Tz (complexes ) Tj 3.363889 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 48.287037 Tz (invention. ) Tj 40 0 0 40 0 2240.872562 Tm 12.35 0 Td 63.194444 Tz (Scheme ) Tj 2.475 0 Td 54.166667 Tz (A. ) Tj 0.9 0 Td 50 Tz (Possible ) Tj 2.575 0 Td 53.030303 Tz (mechanistic ) Tj 3.675 0 Td 57.291667 Tz (pathways ) Tj 2.975 0 Td 56.25 Tz (of ) Tj 0.825 0 Td 83.333333 Tz (H ) Tj 0.925 0 Td 50.462963 Tz (evolution ) Tj 2.925 0 Td 60.416667 Tz (by ) Tj 0.925 0 Td 60.119048 Tz (complex ) Tj 2.725 0 Td 41.666667 Tz (2. ) Tj 32.857143 0 0 32.857143 0 2163.666667 Tm 16.221739 0 Td 278.985507 Tz ( ) Tj 8.369565 0 Td 55.797101 Tz (e ) Tj 47.619048 0 0 47.619048 0 2125.33526 Tm 8.127 0 Td 53.9 Tz (\(CoI2 ) Tj 5.691 0 Td 55.125 Tz (Colt ) Tj 5.985 0 Td 57.75 Tz (Co ) Tj 124.285714 0 0 124.285714 0 1997 Tm 5.366667 0 Td 33.524904 Tz (II" ) Tj 2.534483 0 Td 45.59387 Tz (" ) Tj 27.142857 0 0 27.142857 0 1953 Tm 30.136842 0 Td 73.684211 Tz (e ) Tj 14.257895 0 Td 73.684211 Tz (e ) Tj 40.714286 0 0 40.714286 0 1921.417778 Tm 15.178947 0 Td 60.721248 Tz (Colil- ) Tj 2.308772 0 Td 72.319688 Tz (H2+ ) Tj 1.964912 0 Td 117.348928 Tz (-e- ) Tj 2.97193 0 Td 66.315789 Tz (Coll- ) Tj 2.112281 0 Td 79.824561 Tz (H' ) Tj 9.505263 0 Td 104.385965 Tz (CJ-H ) Tj 93.142857 0 0 93.142857 0 1809.82058 Tm 3.886503 0 Td 33.103272 Tz (Cott-H2+ ) Tj 3.671779 0 Td 41.155419 Tz (r ) Tj 2.909509 0 Td 67.99591 Tz (" ) Tj 1.868098 0 Td 47.239264 Tz (Co-H" ) Tj 3.199387 0 Td 67.99591 Tz (" ) Tj 48.571429 0 0 48.571429 0 1687 Tm 6.629412 0 Td 65.196078 Tz (2CoI2 ) Tj 2.758824 0 Td 54.901961 Tz (+ ) Tj 0.864706 0 Td 48.039216 Tz (H. ) Tj 1.976471 0 Td 60.392157 Tz (Coil' ) Tj 2.491176 0 Td 54.901961 Tz (+ ) Tj 0.844118 0 Td 36.029412 Tz (H. ) Tj 1.935294 0 Td 61.764706 Tz (CoI2 ) Tj 2.388235 0 Td 54.901961 Tz (+ ) Tj 0.905882 0 Td 49.754902 Tz (H, ) Tj 1.852941 0 Td 73.77451 Tz (2Co+ ) Tj 2.347059 0 Td 58.333333 Tz (+ ) Tj 0.947059 0 Td 49.754902 Tz (H. ) Tj 1.955882 0 Td 43.921569 Tz (Coil' ) Tj 1.955882 0 Td 51.470588 Tz (+ ) Tj 0.864706 0 Td 48.039216 Tz (H. ) Tj 32.857143 0 0 32.857143 0 1638 Tm 12.752174 0 Td 65.942029 Tz (6 ) Tj 14.973913 0 Td 45.652174 Tz (1 ) Tj 0.63913 0 Td 96.376812 Tz (& ) Tj 0.882609 0 Td 71.014493 Tz (2 ) Tj 6.086957 0 Td 65.942029 Tz (7 ) Tj 0.7 0 Td 96.376812 Tz (& ) Tj 0.882609 0 Td 71.014493 Tz (8 ) Tj 5.782609 0 Td 65.942029 Tz (3 ) Tj 0.669565 0 Td 101.449275 Tz (& ) Tj 0.913043 0 Td 76.086957 Tz (4 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 51.428571 0 0 51.428571 0 1248.512064 Tm 7.019444 0 Td 46.990741 Tz (In ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 58.981481 Tz (above ) Tj 2.061111 0 Td 56.018519 Tz (Scheme, ) Tj 2.644444 0 Td 57.118056 Tz (pathways ) Tj 3.111111 0 Td 50.771605 Tz (1-5 ) Tj 1.244444 0 Td 61.574074 Tz (show ) Tj 1.847222 0 Td 57.449495 Tz (mononuclear ) Tj 51.428571 0 0 51.428571 0 1209.399015 Tm 6.261111 0 Td 48.611111 Tz (reactions ) Tj 2.819444 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 57.523148 Tz (pathways ) Tj 3.013889 0 Td 51.851852 Tz (6-8 ) Tj 1.147222 0 Td 62.384259 Tz (show ) Tj 1.769444 0 Td 50.411523 Tz (dinuclear ) Tj 2.916667 0 Td 48.251029 Tz (reactions ) Tj 2.838889 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1168 Tm 6.280556 0 Td 56.712963 Tz (He ) Tj 0.972222 0 Td 48.611111 Tz (evolution. ) Tj 51.428571 0 0 51.428571 0 1131.163849 Tm 7.019444 0 Td 54.282407 Tz (FIG. ) Tj 1.594444 0 Td 55.092593 Tz (15 ) Tj 0.894444 0 Td 53.20216 Tz (demonstrates ) Tj 4.063889 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 44.965278 Tz (relative ) Tj 2.352778 0 Td 55.092593 Tz (energy ) Tj 2.216667 0 Td 57.253086 Tz (change ) Tj 2.255556 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 55.902778 Tz (each ) Tj 51.428571 0 0 51.428571 0 1086.904762 Tm 6.280556 0 Td 47.800926 Tz (step ) Tj 1.341667 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 57.118056 Tz (pathways ) Tj 2.975 0 Td 43.209877 Tz (listed ) Tj 1.730556 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 63.734568 Tz (Scheme ) Tj 2.430556 0 Td 56.712963 Tz (A. ) Tj 0.913889 0 Td 53.292181 Tz (Dinuclear ) Tj 3.052778 0 Td 59.41358 Tz (mecha- ) Tj 2.527778 0 Td 48.611111 Tz (45 ) Tj 51.428571 0 0 51.428571 0 1044.314578 Tm 6.261111 0 Td 57.037037 Tz (nisms ) Tj 1.944444 0 Td 49.691358 Tz (are ) Tj 1.108333 0 Td 48.611111 Tz (plotted ) Tj 2.313889 0 Td 52.662037 Tz (with ) Tj 1.536111 0 Td 55.092593 Tz (2 ) Tj 0.602778 0 Td 57.037037 Tz (moles ) Tj 1.983333 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 48.206019 Tz (reaction ) Tj 2.586111 0 Td 46.585648 Tz (species. ) Tj 2.527778 0 Td 56.17284 Tz (Except ) Tj 51.428571 0 0 51.428571 0 1002.788462 Tm 6.261111 0 Td 58.333333 Tz (pathway ) Tj 2.663889 0 Td 43.75 Tz (5, ) Tj 0.680556 0 Td 41.049383 Tz (all ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 52.146465 Tz (mechanistic ) Tj 3.616667 0 Td 57.118056 Tz (pathways ) Tj 2.936111 0 Td 49.691358 Tz (are ) Tj 1.05 0 Td 62.384259 Tz (thermodynami ) Tj 51.428571 0 0 51.428571 0 954.731893 Tm 6.261111 0 Td 46.666667 Tz (cally ) Tj 1.788889 0 Td 49.016204 Tz (favored. ) Tj 2.722222 0 Td 50.87963 Tz (Therefore, ) Tj 3.422222 0 Td 47.685185 Tz (further ) Tj 2.313889 0 Td 47.222222 Tz (kinetic ) Tj 2.333333 0 Td 59.41358 Tz (and ) Tj 1.438889 0 Td 52.146465 Tz (mechanistic ) Tj 51.428571 0 0 51.428571 0 911.475325 Tm 6.280556 0 Td 47.685185 Tz (studies ) Tj 2.333333 0 Td 51.851852 Tz (are ) Tj 1.283333 0 Td 56.712963 Tz (needed ) Tj 2.372222 0 Td 46.990741 Tz (to ) Tj 0.933333 0 Td 44.871795 Tz (differentiate ) Tj 3.869444 0 Td 48.611111 Tz (the ) Tj 1.263889 0 Td 47.800926 Tz (reaction ) Tj 2.625 0 Td 57.523148 Tz (pathways ) Tj 38 0 0 38 0 875.797251 Tm 8.473684 0 Td 59.210526 Tz (listed ) Tj 2.473684 0 Td 61.403509 Tz (in ) Tj 1.078947 0 Td 86.988304 Tz (Scheme ) Tj 3.421053 0 Td 74.561404 Tz (A. ) Tj 17.263158 0 Td 63.596491 Tz (50 ) Tj 51.428571 0 0 51.428571 0 826.161549 Tm 7.019444 0 Td 52.662037 Tz (Free ) Tj 1.516667 0 Td 55.092593 Tz (energy ) Tj 2.275 0 Td 55.092593 Tz (changes ) Tj 2.625 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 52.146465 Tz (mechanistic ) Tj 3.713889 0 Td 48.611111 Tz (steps ) Tj 1.75 0 Td 59.143519 Tz (were ) Tj 1.672222 0 Td 60.493827 Tz (cal ) Tj 51.428571 0 0 51.428571 0 786.256842 Tm 6.261111 0 Td 50 Tz (culated ) Tj 2.333333 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 54.282407 Tz (provided ) Tj 2.858333 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 64.814815 Tz (Scheme ) Tj 2.605556 0 Td 48.611111 Tz (B: ) Tj 40 0 0 40 0 615.864648 Tm 15.35 0 Td 63.194444 Tz (Scheme ) Tj 2.475 0 Td 52.083333 Tz (B. ) Tj 0.875 0 Td 49.583333 Tz (Postulated ) Tj 3.175 0 Td 50.320513 Tz (intermediates ) Tj 4.125 0 Td 50 Tz (\(with ) Tj 1.725 0 Td 59.375 Tz (computed ) Tj 3.075 0 Td 45.3125 Tz (relative ) Tj 2.35 0 Td 47.916667 Tz (free ) Tj 1.325 0 Td 49.074074 Tz (energies\) ) Tj 2.875 0 Td 48.611111 Tz (for ) Tj 1.1 0 Td 54.166667 Tz (H2 ) Tj 0.925 0 Td 50 Tz (evolution ) Tj 2.9 0 Td 60.416667 Tz (by ) Tj 0.95 0 Td 59.52381 Tz (complex ) Tj 2.675 0 Td 41.666667 Tz (2. ) Tj 31.428571 0 0 31.428571 0 549 Tm 12.727273 0 Td 63.636364 Tz (Path ) Tj 1.877273 0 Td 50.378788 Tz (1: ) Tj 47.142857 0 0 47.142857 0 480 Tm 8.442424 0 Td 49.494949 Tz (Col ) Tj 2.142424 0 Td 60.10101 Tz (+ ) Tj 1.421212 0 Td 49.494949 Tz (2e ) Tj 1.760606 0 Td 60.10101 Tz (+ ) Tj 1.4 0 Td 63.636364 Tz (2H ) Tj 2.015152 0 Td 152.020202 Tz (-- ) Tj 2.842424 0 Td 49.494949 Tz (Col ) Tj 2.163636 0 Td 60.10101 Tz (+ ) Tj 1.421212 0 Td 36.531987 Tz (H2. ) Tj 32.142857 0 0 32.142857 0 415 Tm 18.666667 0 Td 62.222222 Tz (e ) Tj 10.017778 0 Td 103.703704 Tz (H ) Tj 13.16 0 Td 62.222222 Tz (e ) Tj 12.475556 0 Td 103.703704 Tz (H ) Tj 48.163265 0 0 48.163265 0 384 Tm 8.305085 0 Td 51.330038 Tz (\(CoI2" ) Tj 7.495339 0 Td 76.129944 Tz (Cot ) Tj 6.540254 0 Td 45.677966 Tz (\(CoII ) Tj 2.22161 0 Td 46.716102 Tz (H]2+ ) Tj 6.602542 0 Td 83.050847 Tz (|Co- ) Tj 2.076271 0 Td 49.599812 Tz (H]" ) Tj 6.913983 0 Td 49.02307 Tz (Coll?" ) Tj 32.619048 0 0 32.619048 0 362.504717 Tm 16.616058 0 Td 77.210057 Tz (BS1-79.81 ) Tj 10.270073 0 Td 70.255474 Tz (BS1: ) Tj 1.962044 0 Td 61.313869 Tz (-6.76 ) Tj 10.515328 0 Td 74.087591 Tz (BS1: ) Tj 2.054015 0 Td 62.16545 Tz (-75.73 ) Tj 11.925547 0 Td 71.532847 Tz (-H2 ) Tj 34.642857 0 0 34.642857 0 330.411765 Tm 11.690722 0 Td 76.013746 Tz (BS1:0 ) Tj 3.954639 0 Td 67.353952 Tz (BS2: ) Tj 1.818557 0 Td 58.533792 Tz (-84.51 ) Tj 7.793814 0 Td 68.556701 Tz (BS2: ) Tj 1.934021 0 Td 56.769759 Tz (-5.27 ) Tj 9.929897 0 Td 67.353952 Tz (BS2: ) Tj 1.847423 0 Td 60.137457 Tz (-75.88 ) Tj 16.049485 0 Td 67.353952 Tz (BS1:-185.4 ) Tj 31.428571 0 0 31.428571 0 303.77439 Tm 12.95 0 Td 72.916667 Tz (BS2: ) Tj 2.036364 0 Td 68.939394 Tz (O ) Tj 38.881818 0 Td 72.916667 Tz (BS1: ) Tj 2.004545 0 Td 66.287879 Tz (-23.09 ) Tj 4.772727 0 Td 72.916667 Tz (BS2: ) Tj 2.036364 0 Td 66.287879 Tz (-186.6 ) Tj 31.428571 0 0 31.428571 0 274 Tm 53.868182 0 Td 72.916667 Tz (BS2: ) Tj 2.004545 0 Td 66.287879 Tz (-20.99 ) Tj ET Q endstream endobj 278 0 obj << /Length 1 >> stream q endstream endobj 279 0 obj << /Length 39400 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.151351 0 Td 74.099099 Tz (19 ) Tj 51.428571 0 0 51.428571 0 2913.753978 Tm 6.261111 0 Td 58.333333 Tz (Pure ) Tj 1.536111 0 Td 49.907407 Tz (Appl. ) Tj 1.75 0 Td 60.277778 Tz (Chem. ) Tj 2.1 0 Td 51.851852 Tz (1986, ) Tj 1.75 0 Td 54.012346 Tz (58,955-966\). ) Tj 4.044444 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 47.727273 Tz (differences ) Tj 3.363889 0 Td 45.37037 Tz (in ) Tj 0.719444 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 2875.095368 Tm 6.261111 0 Td 51.311728 Tz (values ) Tj 2.119444 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 55.092593 Tz (redox ) Tj 1.886111 0 Td 46.990741 Tz (potentials ) Tj 3.052778 0 Td 50.771605 Tz (are ) Tj 1.186111 0 Td 45.046296 Tz (relatively ) Tj 2.936111 0 Td 48.251029 Tz (accurate. ) Tj 51.428571 0 0 51.428571 0 2833.185751 Tm 7.019444 0 Td 50 Tz (Results ) Tj 2.294444 0 Td 58.333333 Tz (from ) Tj 1.613889 0 Td 75.617284 Tz (DFT ) Tj 1.536111 0 Td 54.282407 Tz (computations ) Tj 4.122222 0 Td 51.851852 Tz (suggest ) Tj 2.372222 0 Td 44.560185 Tz (that ) Tj 1.244444 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 62.114198 Tz (number ) Tj 2.372222 0 Td 59.953704 Tz (of ) Tj 51.428571 0 0 51.428571 0 2792.679245 Tm 6.261111 0 Td 48.611111 Tz (reaction ) Tj 2.488889 0 Td 57.523148 Tz (pathways ) Tj 2.916667 0 Td 51.851852 Tz (are ) Tj 1.069444 0 Td 55.473856 Tz (thermodynamically ) Tj 5.872222 0 Td 50.411523 Tz (favorable ) Tj 2.916667 0 Td 47.530864 Tz (for ) Tj 0.972222 0 Td 68.055556 Tz (pro ) Tj 51.428571 0 0 51.428571 0 2748.883688 Tm 6.241667 0 Td 50.771605 Tz (ton ) Tj 1.341667 0 Td 50.05144 Tz (reduction ) Tj 3.072222 0 Td 61.574074 Tz (by ) Tj 1.127778 0 Td 59.259259 Tz (complex ) Tj 2.877778 0 Td 42.12963 Tz (2. ) Tj 0.894444 0 Td 55.902778 Tz (Such ) Tj 1.672222 0 Td 51.851852 Tz (as ) Tj 0.972222 0 Td 50.771605 Tz (the ) Tj 1.302778 0 Td 57.253086 Tz (one ) Tj 1.4 0 Td 62.87037 Tz (shown ) Tj 2.275 0 Td 46.990741 Tz (in ) Tj 58.571429 0 0 58.571429 0 2707.535714 Tm 5.514634 0 Td 56.436314 Tz (Scheme ) Tj 2.236585 0 Td 54.065041 Tz (2 ) Tj 0.546341 0 Td 52.357724 Tz (where ) Tj 1.809756 0 Td 42.682927 Tz (the ) Tj 0.990244 0 Td 46.747967 Tz (binding ) Tj 2.185366 0 Td 52.642276 Tz (of ) Tj 0.768293 0 Td 46.476965 Tz (proton ) Tj 1.912195 0 Td 39.837398 Tz (to ) Tj 0.717073 0 Td 42.682927 Tz (the ) Tj 0.990244 0 Td 48.373984 Tz (Co' ) Tj 1.178049 0 Td 49.796748 Tz (form ) Tj 1.434146 0 Td 52.642276 Tz (of ) Tj 57.142857 0 0 57.142857 0 2667.411168 Tm 5.635 0 Td 53.333333 Tz (complex ) Tj 2.4325 0 Td 52.5 Tz (2 ) Tj 0.4725 0 Td 44.236111 Tz (yields ) Tj 1.75 0 Td 46.666667 Tz (the ) Tj 0.98 0 Td 69.027778 Tz (Co' ) Tj 1.9425 0 Td 75.833333 Tz (H ) Tj 0.63 0 Td 42.65625 Tz (species. ) Tj 2.2575 0 Td 45.833333 Tz (Further ) Tj 2.065 0 Td 46.018519 Tz (reduction ) Tj 2.625 0 Td 53.958333 Tz (of ) Tj 58.571429 0 0 58.571429 0 2625.083004 Tm 5.497561 0 Td 68.292683 Tz (Co' ) Tj 1.878049 0 Td 76.829268 Tz (H ) Tj 0.631707 0 Td 38.414634 Tz (to ) Tj 0.597561 0 Td 60.704607 Tz (Co' ) Tj 1.741463 0 Td 76.829268 Tz (H ) Tj 0.597561 0 Td 43.902439 Tz (species ) Tj 2.014634 0 Td 46.95122 Tz (followed ) Tj 2.407317 0 Td 52.642276 Tz (by ) Tj 0.768293 0 Td 46.747967 Tz (binding ) Tj 2.082927 0 Td 51.219512 Tz (of ) Tj 0.7 0 Td 46.341463 Tz (another ) Tj 52.857143 0 0 52.857143 0 2581.391916 Tm 6.072973 0 Td 52.027027 Tz (proton ) Tj 2.1 0 Td 44.144144 Tz (results ) Tj 2.062162 0 Td 45.720721 Tz (in ) Tj 0.851351 0 Td 45.720721 Tz (H. ) Tj 0.945946 0 Td 49.74975 Tz (evolution ) Tj 2.913514 0 Td 59.009009 Tz (\(Scheme ) Tj 2.667568 0 Td 43.093093 Tz (2\). ) Tj 38.571429 0 0 38.571429 0 2463.938744 Tm 10.525926 0 Td 65.534979 Tz (Scheme ) Tj 2.566667 0 Td 43.209877 Tz (2. ) Tj 0.803704 0 Td 57.79321 Tz (Proposed ) Tj 2.955556 0 Td 62.894376 Tz (mechanism ) Tj 3.62963 0 Td 50.411523 Tz (for ) Tj 1.062963 0 Td 51.851852 Tz (the ) Tj 1.088889 0 Td 54.73251 Tz (proton ) Tj 2.203704 0 Td 51.851852 Tz (reduction ) Tj 3.059259 0 Td 60.493827 Tz (by ) Tj 0.907407 0 Td 45.37037 Tz (2. ) Tj 37.142857 0 0 37.142857 0 2395 Tm 16.692308 0 Td 89.74359 Tz (H ) Tj 14.107692 0 Td 89.74359 Tz (H ) Tj 42.857143 0 0 42.857143 0 2369.631161 Tm 7.536667 0 Td 64.166667 Tz (Co ) Tj 1.96 0 Td 112.777778 Tz (--- ) Tj 2.776667 0 Td 64.166667 Tz (Co ) Tj 1.75 0 Td 167.222222 Tz (-> ) Tj 2.823333 0 Td 107.916667 Tz (Co-H ) Tj 3.336667 0 Td 108.888889 Tz (--> ) Tj 2.776667 0 Td 105.972222 Tz (Co-H ) Tj 3.29 0 Td 167.222222 Tz (-> ) Tj 48.571429 0 0 48.571429 0 2320 Tm 21.720588 0 Td 46.895425 Tz (Col ) Tj 1.729412 0 Td 54.901961 Tz (+ ) Tj 0.967647 0 Td 41.176471 Tz (H. ) Tj 51.428571 0 0 51.428571 0 2202.185751 Tm 7.019444 0 Td 50 Tz (Results ) Tj 2.294444 0 Td 58.333333 Tz (from ) Tj 1.613889 0 Td 75.617284 Tz (DFT ) Tj 1.536111 0 Td 54.282407 Tz (computations ) Tj 4.122222 0 Td 51.851852 Tz (suggest ) Tj 2.372222 0 Td 44.560185 Tz (that ) Tj 1.244444 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 62.114198 Tz (number ) Tj 2.372222 0 Td 59.953704 Tz (of ) Tj 51.428571 0 0 51.428571 0 2162.309227 Tm 6.261111 0 Td 48.611111 Tz (reaction ) Tj 2.722222 0 Td 57.118056 Tz (pathways ) Tj 3.111111 0 Td 49.691358 Tz (are ) Tj 1.263889 0 Td 55.473856 Tz (thermodynamically ) Tj 6.047222 0 Td 51.851852 Tz (favourable ) Tj 3.5 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 2118.81225 Tm 6.261111 0 Td 52.391975 Tz (proton ) Tj 2.197222 0 Td 50.05144 Tz (reduction ) Tj 2.975 0 Td 61.574074 Tz (by ) Tj 1.011111 0 Td 59.722222 Tz (complex ) Tj 2.8 0 Td 40.509259 Tz (2. ) Tj 0.816667 0 Td 54.282407 Tz (Such ) Tj 1.575 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 57.253086 Tz (one ) Tj 1.322222 0 Td 62.222222 Tz (shown ) Tj 2.158333 0 Td 46.990741 Tz (in ) Tj 58.571429 0 0 58.571429 0 2076.535714 Tm 5.514634 0 Td 56.436314 Tz (Scheme ) Tj 2.236585 0 Td 54.065041 Tz (2 ) Tj 0.546341 0 Td 52.357724 Tz (where ) Tj 1.809756 0 Td 42.682927 Tz (the ) Tj 0.990244 0 Td 46.747967 Tz (binding ) Tj 2.185366 0 Td 52.642276 Tz (of ) Tj 0.768293 0 Td 46.476965 Tz (proton ) Tj 1.912195 0 Td 39.837398 Tz (to ) Tj 0.717073 0 Td 42.682927 Tz (the ) Tj 0.990244 0 Td 48.373984 Tz (Co' ) Tj 1.178049 0 Td 49.796748 Tz (form ) Tj 1.434146 0 Td 52.642276 Tz (of ) Tj 57.142857 0 0 57.142857 0 2036.411168 Tm 5.635 0 Td 53.333333 Tz (complex ) Tj 2.4325 0 Td 52.5 Tz (2 ) Tj 0.4725 0 Td 44.236111 Tz (yields ) Tj 1.75 0 Td 46.666667 Tz (the ) Tj 0.98 0 Td 69.027778 Tz (Co' ) Tj 1.9425 0 Td 75.833333 Tz (H ) Tj 0.63 0 Td 42.65625 Tz (species. ) Tj 2.2575 0 Td 45.833333 Tz (Further ) Tj 2.065 0 Td 46.018519 Tz (reduction ) Tj 2.625 0 Td 53.958333 Tz (of ) Tj 58.571429 0 0 58.571429 0 1994.083004 Tm 5.497561 0 Td 68.292683 Tz (Co' ) Tj 1.878049 0 Td 76.829268 Tz (H ) Tj 0.631707 0 Td 38.414634 Tz (to ) Tj 0.597561 0 Td 60.704607 Tz (Co' ) Tj 1.741463 0 Td 76.829268 Tz (H ) Tj 0.597561 0 Td 43.902439 Tz (species ) Tj 2.014634 0 Td 46.95122 Tz (followed ) Tj 2.407317 0 Td 52.642276 Tz (by ) Tj 0.768293 0 Td 46.747967 Tz (binding ) Tj 2.082927 0 Td 51.219512 Tz (of ) Tj 0.7 0 Td 46.341463 Tz (another ) Tj 52.857143 0 0 52.857143 0 1950.391916 Tm 6.072973 0 Td 52.027027 Tz (proton ) Tj 2.1 0 Td 44.144144 Tz (results ) Tj 2.062162 0 Td 45.720721 Tz (in ) Tj 0.851351 0 Td 45.720721 Tz (H. ) Tj 0.945946 0 Td 49.74975 Tz (evolution ) Tj 2.913514 0 Td 59.009009 Tz (\(Scheme ) Tj 2.667568 0 Td 43.093093 Tz (2\). ) Tj 38.571429 0 0 38.571429 0 1879 Tm 10.992593 0 Td 95.349794 Tz (EXEMPLIFICATION ) Tj 8.944444 0 Td 99.382716 Tz (OF ) Tj 1.503704 0 Td 106.584362 Tz (THE ) Tj 2.281481 0 Td 98.422497 Tz (INVENTION ) Tj 51.428571 0 0 51.428571 0 1793.029207 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.438889 0 Td 52.211934 Tz (following ) Tj 3.111111 0 Td 57.118056 Tz (examples ) Tj 3.072222 0 Td 49.691358 Tz (are ) Tj 1.166667 0 Td 54.012346 Tz (put ) Tj 1.263889 0 Td 46.666667 Tz (forth ) Tj 1.730556 0 Td 51.851852 Tz (so ) Tj 0.933333 0 Td 50.231481 Tz (as ) Tj 0.933333 0 Td 45.37037 Tz (to ) Tj 0.836111 0 Td 53.703704 Tz (provide ) Tj 51.428571 0 0 51.428571 0 1748.673392 Tm 6.241667 0 Td 51.851852 Tz (those ) Tj 1.769444 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 51.041667 Tz (ordinary ) Tj 2.702778 0 Td 40.833333 Tz (skill ) Tj 1.458333 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 43.209877 Tz (art ) Tj 0.972222 0 Td 53.472222 Tz (with ) Tj 1.516667 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 56.30787 Tz (complete ) Tj 2.897222 0 Td 49.259259 Tz (disclosure ) Tj 51.428571 0 0 51.428571 0 1707.176614 Tm 6.261111 0 Td 58.333333 Tz (and ) Tj 1.205556 0 Td 48.905724 Tz (description ) Tj 3.383333 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 68.055556 Tz (how ) Tj 1.4 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 65.625 Tz (make ) Tj 1.711111 0 Td 58.333333 Tz (and ) Tj 1.205556 0 Td 54.012346 Tz (use ) Tj 1.088889 0 Td 51.851852 Tz (the ) Tj 1.108333 0 Td 52.5 Tz (metal ) Tj 1.730556 0 Td 57.613169 Tz (complexes ) Tj 51.428571 0 0 51.428571 0 1664.656516 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 48.287037 Tz (invention. ) Tj 3.072222 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 59.953704 Tz (method ) Tj 2.333333 0 Td 48.611111 Tz (for ) Tj 0.991667 0 Td 50.084175 Tz (preparation ) Tj 3.5 0 Td 55.092593 Tz (can ) Tj 1.205556 0 Td 50.462963 Tz (include ) Tj 2.294444 0 Td 49.691358 Tz (the ) Tj 52.857143 0 0 52.857143 0 1621.284974 Tm 6.072973 0 Td 53.603604 Tz (use ) Tj 1.286486 0 Td 55.18018 Tz (of ) Tj 0.908108 0 Td 55.705706 Tz (one ) Tj 1.305405 0 Td 52.027027 Tz (or ) Tj 0.927027 0 Td 59.90991 Tz (more ) Tj 1.759459 0 Td 47.072072 Tz (intermediates, ) Tj 4.275676 0 Td 52.815315 Tz (chemical ) Tj 2.856757 0 Td 48.873874 Tz (reagents ) Tj 2.648649 0 Td 59.90991 Tz (and ) Tj 51.428571 0 0 51.428571 0 1581.09375 Tm 6.280556 0 Td 48.251029 Tz (synthetic ) Tj 2.858333 0 Td 49.151235 Tz (routes ) Tj 2.002778 0 Td 50.231481 Tz (as ) Tj 0.855556 0 Td 49.907407 Tz (delineated ) Tj 3.227778 0 Td 47.222222 Tz (herein. ) Tj 40 0 0 40 0 1508 Tm 11.225 0 Td 39.583333 Tz (I. ) Tj 0.8 0 Td 70.833333 Tz (General ) Tj 3.325 0 Td 68.333333 Tz (Procedures ) Tj 4.4 0 Td 77.777778 Tz (and ) Tj 1.75 0 Td 65.555556 Tz (Instrumentation ) Tj 51.428571 0 0 51.428571 0 1420.003871 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.341667 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 57.973251 Tz (complexes ) Tj 3.325 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 50.411523 Tz (invention ) Tj 2.936111 0 Td 55.092593 Tz (can ) Tj 1.186111 0 Td 59.953704 Tz (be ) Tj 0.913889 0 Td 52.662037 Tz (prepared ) Tj 2.722222 0 Td 55.092593 Tz (or ) Tj 51.428571 0 0 51.428571 0 1376.843185 Tm 6.241667 0 Td 56.712963 Tz (used ) Tj 1.497222 0 Td 63.194444 Tz (by ) Tj 0.933333 0 Td 58.333333 Tz (methods ) Tj 2.605556 0 Td 51.49177 Tz (described ) Tj 2.955556 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 42.939815 Tz (this ) Tj 1.205556 0 Td 46.585648 Tz (section, ) Tj 2.391667 0 Td 50.771605 Tz (the ) Tj 1.030556 0 Td 54.73251 Tz (examples, ) Tj 3.091667 0 Td 61.574074 Tz (and ) Tj 40 0 0 40 0 1341 Tm 8.025 0 Td 65.277778 Tz (the ) Tj 1.475 0 Td 70.3125 Tz (chemical ) Tj 3.725 0 Td 53.787879 Tz (literature. ) Tj 51.428571 0 0 51.428571 0 1295.247956 Tm 6.338889 0 Td 37.268519 Tz (1. ) Tj 0.719444 0 Td 50.411523 Tz (Materials ) Tj 2.975 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 53.652263 Tz (Syntheses ) Tj 51.428571 0 0 51.428571 0 1253.609632 Tm 7 0 Td 49.691358 Tz (All ) Tj 1.127778 0 Td 53.619529 Tz (experiments ) Tj 3.752778 0 Td 59.143519 Tz (were ) Tj 1.613889 0 Td 55.452675 Tz (conducted ) Tj 3.227778 0 Td 55.092593 Tz (under ) Tj 1.827778 0 Td 56.712963 Tz (an ) Tj 0.875 0 Td 64.814815 Tz (Ar ) Tj 0.933333 0 Td 56.388889 Tz (atmosphere ) Tj 51.428571 0 0 51.428571 0 1211.816901 Tm 6.241667 0 Td 50.771605 Tz (unless ) Tj 2.197222 0 Td 48.070988 Tz (noted. ) Tj 2.061111 0 Td 49.691358 Tz (All ) Tj 1.225 0 Td 53.652263 Tz (chemicals ) Tj 3.208333 0 Td 59.41358 Tz (and ) Tj 1.4 0 Td 49.421296 Tz (reagents ) Tj 2.722222 0 Td 59.143519 Tz (were ) Tj 1.730556 0 Td 55.092593 Tz (purchased ) Tj 51.428571 0 0 51.428571 0 1169.8 Tm 6.261111 0 Td 58.333333 Tz (from ) Tj 1.788889 0 Td 55.34188 Tz (Sigma-Aldrich ) Tj 4.705556 0 Td 50.231481 Tz (unless ) Tj 2.236111 0 Td 48.070988 Tz (noted. ) Tj 2.119444 0 Td 53.877315 Tz (Ascorbic ) Tj 2.955556 0 Td 46.666667 Tz (acid, ) Tj 1.827778 0 Td 71.296296 Tz (Hg ) Tj 1.244444 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 1128.253254 Tm 6.261111 0 Td 47.638889 Tz (electronic ) Tj 3.072222 0 Td 57.685185 Tz (\(99.9998%\) ) Tj 3.636111 0 Td 53.472222 Tz (or ) Tj 0.797222 0 Td 49.583333 Tz (puratronic ) Tj 3.169444 0 Td 49.691358 Tz (\(or ) Tj 1.05 0 Td 59.806397 Tz (99.999995%\) ) Tj 4.102778 0 Td 55.092593 Tz (grade ) Tj 51.428571 0 0 51.428571 0 1085.617021 Tm 6.241667 0 Td 59.953704 Tz (were ) Tj 1.788889 0 Td 54.73251 Tz (purchased ) Tj 3.325 0 Td 57.523148 Tz (from ) Tj 1.730556 0 Td 52.662037 Tz (Alfa ) Tj 1.613889 0 Td 49.691358 Tz (Aesar. ) Tj 2.177778 0 Td 57.685185 Tz (Water ) Tj 2.061111 0 Td 49.907407 Tz (\(18.2 ) Tj 1.847222 0 Td 60.763889 Tz (MS2\) ) Tj 1.827778 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 1048.930233 Tm 6.261111 0 Td 47.395833 Tz (purified ) Tj 2.45 0 Td 53.148148 Tz (using ) Tj 1.75 0 Td 53.240741 Tz (Milli-Q ) Tj 2.411111 0 Td 51.851852 Tz (system. ) Tj 2.411111 0 Td 52.091907 Tz (N.N-Bis\(2-pyridinylmethyl\)- ) Tj 51.428571 0 0 51.428571 0 1008.483871 Tm 6.261111 0 Td 52.075351 Tz (2,2'-bipyridine-6-methanamine ) Tj 9.255556 0 Td 61.213992 Tz (\(DPA-Bpy\) ) Tj 3.5 0 Td 60.493827 Tz (was ) Tj 1.322222 0 Td 51.851852 Tz (synthesized ) Tj 51.428571 0 0 51.428571 0 961.463158 Tm 6.261111 0 Td 53.292181 Tz (according ) Tj 3.188889 0 Td 45.37037 Tz (to ) Tj 0.875 0 Td 43.75 Tz (literature ) Tj 2.955556 0 Td 60.493827 Tz (method ) Tj 2.488889 0 Td 47.530864 Tz (\(B. ) Tj 1.244444 0 Td 61.111111 Tz (Radaram ) Tj 2.877778 0 Td 46.990741 Tz (et ) Tj 0.855556 0 Td 37.268519 Tz (al., ) Tj 1.244444 0 Td 46.450617 Tz (Inorg. ) Tj 51.428571 0 0 51.428571 0 918 Tm 6.280556 0 Td 60.277778 Tz (Chem. ) Tj 2.119444 0 Td 52.5 Tz (2011, ) Tj 1.827778 0 Td 49.691358 Tz (50, ) Tj 1.205556 0 Td 54.344729 Tz (10564-10571\). ) Tj 40 0 0 40 0 884 Tm 8.05 0 Td 56.25 Tz (2. ) Tj 1.075 0 Td 65.555556 Tz (Instrumentation ) Tj 51.428571 0 0 51.428571 0 838.029369 Tm 7.019444 0 Td 56.712963 Tz (UV-vis ) Tj 2.625 0 Td 50.87963 Tz (absorption ) Tj 3.655556 0 Td 48.611111 Tz (spectra ) Tj 2.625 0 Td 58.333333 Tz (were ) Tj 1.983333 0 Td 57.928241 Tz (measured ) Tj 3.363889 0 Td 52.5 Tz (using ) Tj 2.119444 0 Td 58.333333 Tz (a ) Tj 51.428571 0 0 51.428571 0 796.740514 Tm 6.280556 0 Td 65.219907 Tz (HP-8452A ) Tj 3.363889 0 Td 53.148148 Tz (diode ) Tj 1.827778 0 Td 49.907407 Tz (array ) Tj 1.769444 0 Td 49.85755 Tz (spectrometer. ) Tj 4.180556 0 Td 64.274691 Tz (ESI-MS ) Tj 2.586111 0 Td 48.611111 Tz (spectra ) Tj 2.313889 0 Td 59.143519 Tz (were ) Tj 51.428571 0 0 51.428571 0 753.342385 Tm 6.261111 0 Td 52.256944 Tz (obtained ) Tj 2.663889 0 Td 58.333333 Tz (from ) Tj 1.555556 0 Td 56.944444 Tz (ThermoElectron ) Tj 4.997222 0 Td 78.858025 Tz (LCQ ) Tj 1.536111 0 Td 58.333333 Tz (Advantage ) Tj 3.325 0 Td 46.450617 Tz (liquid ) Tj 1.847222 0 Td 64.00463 Tz (chro ) Tj 52.857143 0 0 52.857143 0 712.797872 Tm 6.091892 0 Td 55.705706 Tz (matograph ) Tj 3.405405 0 Td 57.545045 Tz (mass ) Tj 1.740541 0 Td 48.024948 Tz (spectrometer. ) Tj 4.105405 0 Td 62.012012 Tz (The ) Tj 1.456757 0 Td 50.800801 Tz (formation ) Tj 3.121622 0 Td 56.756757 Tz (of ) Tj 0.983784 0 Td 78.828829 Tz (H ) Tj 1.097297 0 Td 59.90991 Tz (was ) Tj 51.428571 0 0 51.428571 0 670.868318 Tm 6.261111 0 Td 54.768519 Tz (determined ) Tj 3.577778 0 Td 61.574074 Tz (by ) Tj 1.069444 0 Td 56.712963 Tz (an ) Tj 1.030556 0 Td 77.777778 Tz (HP ) Tj 1.225 0 Td 60.763889 Tz (5890 ) Tj 1.75 0 Td 45.910494 Tz (series ) Tj 2.022222 0 Td 37.268519 Tz (II ) Tj 0.777778 0 Td 61.574074 Tz (Gas ) Tj 1.438889 0 Td 59.081197 Tz (Chromatograph ) Tj 58.571429 0 0 58.571429 0 627 Tm 5.480488 0 Td 47.662602 Tz (with ) Tj 1.382927 0 Td 51.219512 Tz (a ) Tj 0.495122 0 Td 73.03523 Tz (TCD ) Tj 1.553659 0 Td 43.394309 Tz (detector ) Tj 2.304878 0 Td 47.804878 Tz (\(Molecular ) Tj 3.056098 0 Td 44.390244 Tz (sieve ) Tj 1.587805 0 Td 51.219512 Tz (5 ) Tj 0.546341 0 Td 73.98374 Tz (A ) Tj 0.682927 0 Td 47.662602 Tz (column\). ) Tj 2.560976 0 Td 65.447154 Tz (Pho ) Tj 51.428571 0 0 51.428571 0 587.410256 Tm 6.241667 0 Td 45.664983 Tz (tocatalytic ) Tj 3.325 0 Td 48.251029 Tz (reactions ) Tj 2.897222 0 Td 59.143519 Tz (were ) Tj 1.691667 0 Td 47.685185 Tz (carried ) Tj 2.275 0 Td 51.851852 Tz (out ) Tj 1.225 0 Td 51.851852 Tz (using ) Tj 1.827778 0 Td 55.092593 Tz (an ) Tj 0.991667 0 Td 75.617284 Tz (LED ) Tj 1.652778 0 Td 53.796296 Tz (\(Cree ) Tj 51.428571 0 0 51.428571 0 545.736059 Tm 6.261111 0 Td 61.574074 Tz (3-Up ) Tj 1.672222 0 Td 62.222222 Tz (XP-E\) ) Tj 2.061111 0 Td 59.953704 Tz (lamp ) Tj 1.613889 0 Td 46.990741 Tz (at ) Tj 0.738889 0 Td 60.493827 Tz (450 ) Tj 1.302778 0 Td 59.41358 Tz (nm. ) Tj 1.302778 0 Td 54.012346 Tz (Elemental ) Tj 3.111111 0 Td 51.041667 Tz (analyses ) Tj 2.663889 0 Td 58.333333 Tz (were ) Tj 1.594444 0 Td 59.143519 Tz (done ) Tj 51.428571 0 0 51.428571 0 503.473411 Tm 6.241667 0 Td 61.574074 Tz (by ) Tj 1.030556 0 Td 48.206019 Tz (Atlantic ) Tj 2.625 0 Td 52.211934 Tz (Microlab, ) Tj 3.169444 0 Td 44.560185 Tz (Inc, ) Tj 1.322222 0 Td 48.206019 Tz (Atlanta, ) Tj 2.605556 0 Td 56.17284 Tz (Ga. ) Tj 1.380556 0 Td 71.296296 Tz (EPR ) Tj 1.594444 0 Td 48.148148 Tz (spectra ) Tj 2.352778 0 Td 59.143519 Tz (were ) Tj 51.428571 0 0 51.428571 0 463.369483 Tm 6.261111 0 Td 53.06713 Tz (recorded ) Tj 2.897222 0 Td 58.333333 Tz (on ) Tj 1.05 0 Td 55.092593 Tz (a ) Tj 0.680556 0 Td 53.148148 Tz (Varian-122 ) Tj 3.558333 0 Td 59.953704 Tz (X-band ) Tj 2.508333 0 Td 52.662037 Tz (spectrometer ) Tj 4.102778 0 Td 56.30787 Tz (equipped ) Tj 51.428571 0 0 51.428571 0 422.153439 Tm 6.241667 0 Td 54.282407 Tz (with ) Tj 1.691667 0 Td 58.333333 Tz (an ) Tj 1.069444 0 Td 55.092593 Tz (Air ) Tj 1.4 0 Td 52.256944 Tz (Products ) Tj 2.936111 0 Td 49.016204 Tz (Helitran ) Tj 2.761111 0 Td 48.206019 Tz (cryostat ) Tj 2.702778 0 Td 58.333333 Tz (and ) Tj 1.458333 0 Td 52.73569 Tz (temperature ) Tj 51.428571 0 0 51.428571 0 378.9877 Tm 6.261111 0 Td 47.638889 Tz (controller ) Tj 3.091667 0 Td 45.37037 Tz (at ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 42.534722 Tz (Illinois ) Tj 2.352778 0 Td 50.231481 Tz (Electron ) Tj 2.702778 0 Td 54.552469 Tz (Paramagnetic ) Tj 4.238889 0 Td 57.973251 Tz (Resonance ) Tj 51.428571 0 0 51.428571 0 338.00319 Tm 6.280556 0 Td 55.092593 Tz (Research ) Tj 2.897222 0 Td 54.552469 Tz (Center ) Tj 2.177778 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 50.87963 Tz (University ) Tj 3.305556 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 40.329218 Tz (Illinois. ) Tj 51.428571 0 0 51.428571 0 296.533666 Tm 7 0 Td 52.391975 Tz (Cyclic ) Tj 2.138889 0 Td 53.20216 Tz (voltammetric ) Tj 4.102778 0 Td 56.983025 Tz (measurements ) Tj 4.336111 0 Td 59.143519 Tz (were ) Tj 1.594444 0 Td 56.532922 Tz (performed ) Tj 3.266667 0 Td 54.282407 Tz (with ) Tj 51.428571 0 0 51.428571 0 253.741294 Tm 6.261111 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 84.259259 Tz (CH ) Tj 1.263889 0 Td 51.262626 Tz (Instruments ) Tj 3.597222 0 Td 47.260802 Tz (potentiostat ) Tj 3.616667 0 Td 58.873457 Tz (\(Model ) Tj 2.352778 0 Td 54.282407 Tz (660\) ) Tj 1.536111 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 45.37037 Tz (0.1 ) Tj 1.088889 0 Td 90.092593 Tz (MTBAP ) Tj 51.428571 0 0 51.428571 0 213.11421 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 45.640432 Tz (acetonitrile ) Tj 3.597222 0 Td 53.472222 Tz (or ) Tj 0.991667 0 Td 47.530864 Tz (1.0 ) Tj 1.147222 0 Td 106.944444 Tz (M ) Tj 0.952778 0 Td 74.537037 Tz (pH ) Tj 1.225 0 Td 51.851852 Tz (7.0 ) Tj 1.244444 0 Td 58.333333 Tz (sodium ) Tj 2.411111 0 Td 55.092593 Tz (phosphate ) Tj 3.286111 0 Td 49.151235 Tz (buffer ) Tj 51.428571 0 0 51.428571 0 173.168878 Tm 6.241667 0 Td 53.148148 Tz (using ) Tj 1.769444 0 Td 50.231481 Tz (glassy ) Tj 2.041667 0 Td 54.012346 Tz (carbon ) Tj 2.138889 0 Td 57.87037 Tz (working ) Tj 2.605556 0 Td 47.314815 Tz (electrode, ) Tj 3.033333 0 Td 53.472222 Tz (platinum ) Tj 2.761111 0 Td 54.282407 Tz (wire ) Tj 1.497222 0 Td 68.055556 Tz (coun ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 77.252252 Tz (20 ) Tj 51.428571 0 0 51.428571 0 2914.315469 Tm 25.180556 0 Td 45.37037 Tz (ter ) Tj 1.030556 0 Td 46.990741 Tz (electrode, ) Tj 3.111111 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 62.5 Tz (Ag/AgCl ) Tj 2.916667 0 Td 49.691358 Tz (reference ) Tj 2.936111 0 Td 46.990741 Tz (electrode. ) Tj 3.072222 0 Td 52.5 Tz (Controlled ) Tj 51.428571 0 0 51.428571 0 2877.787916 Tm 25.2 0 Td 47.170782 Tz (potential ) Tj 2.741667 0 Td 45.910494 Tz (electrolysis ) Tj 3.519444 0 Td 62.654321 Tz (was ) Tj 1.302778 0 Td 55.812757 Tz (conducted ) Tj 3.227778 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 48.611111 Tz (1.0 ) Tj 1.069444 0 Td 103.703704 Tz (M ) Tj 0.836111 0 Td 58.873457 Tz (sodium ) Tj 2.333333 0 Td 67.24537 Tz (phos ) Tj 51.428571 0 0 51.428571 0 2839.42439 Tm 25.2 0 Td 52.5 Tz (phate ) Tj 1.711111 0 Td 49.151235 Tz (buffer ) Tj 1.866667 0 Td 46.990741 Tz (at ) Tj 0.7 0 Td 72.916667 Tz (pH ) Tj 1.05 0 Td 55.092593 Tz (7 ) Tj 0.505556 0 Td 45.37037 Tz (in ) Tj 0.680556 0 Td 56.712963 Tz (an ) Tj 0.913889 0 Td 54.552469 Tz (H-type ) Tj 2.1 0 Td 47.530864 Tz (gas-tight ) Tj 2.702778 0 Td 51.851852 Tz (dual ) Tj 1.419444 0 Td 58.038721 Tz (compartment ) Tj 57.142857 0 0 57.142857 0 2796.954198 Tm 22.68 0 Td 36.75 Tz (cell. ) Tj 1.225 0 Td 78.75 Tz (A ) Tj 0.595 0 Td 51.25 Tz (mercury ) Tj 2.2925 0 Td 50.3125 Tz (pool ) Tj 1.365 0 Td 46.666667 Tz (with ) Tj 1.2775 0 Td 49.583333 Tz (a ) Tj 0.4725 0 Td 44.583333 Tz (surface ) Tj 1.995 0 Td 45.9375 Tz (area ) Tj 1.26 0 Td 52.5 Tz (of ) Tj 0.7 0 Td 44.722222 Tz (4.9 ) Tj 0.9625 0 Td 65.625 Tz (cm ) Tj 1.2075 0 Td 55.416667 Tz (was ) Tj 1.1725 0 Td 50.3125 Tz (used ) Tj 51.428571 0 0 51.428571 0 2758.791614 Tm 25.2 0 Td 50.231481 Tz (as ) Tj 0.913889 0 Td 57.87037 Tz (working ) Tj 2.722222 0 Td 47.638889 Tz (electrode, ) Tj 3.169444 0 Td 54.73251 Tz (connected ) Tj 3.266667 0 Td 53.240741 Tz (through ) Tj 2.566667 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 53.877315 Tz (platinum ) Tj 2.916667 0 Td 54.282407 Tz (wire ) Tj 51.428571 0 0 51.428571 0 2720.61708 Tm 25.2 0 Td 52.932099 Tz (placed ) Tj 2.255556 0 Td 46.990741 Tz (at ) Tj 0.933333 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 56.712963 Tz (bottom ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.972222 0 Td 50.771605 Tz (the ) Tj 1.322222 0 Td 56.481481 Tz (mercury ) Tj 2.741667 0 Td 49.259259 Tz (pool. ) Tj 1.847222 0 Td 72.916667 Tz (An ) Tj 1.263889 0 Td 56.944444 Tz (aqueous ) Tj 51.428571 0 0 51.428571 0 2678.298289 Tm 25.2 0 Td 63.425926 Tz (Ag/AgCl ) Tj 2.916667 0 Td 49.691358 Tz (reference ) Tj 2.858333 0 Td 50.05144 Tz (electrode ) Tj 2.936111 0 Td 57.79321 Tz (\(BASi\) ) Tj 2.294444 0 Td 61.574074 Tz (was ) Tj 1.341667 0 Td 52.932099 Tz (placed ) Tj 2.119444 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 52.777778 Tz (electro ) Tj 51.428571 0 0 51.428571 0 2641.723716 Tm 25.2 0 Td 45.37037 Tz (lyte ) Tj 1.263889 0 Td 48.611111 Tz (Solution ) Tj 2.508333 0 Td 58.333333 Tz (above ) Tj 1.925 0 Td 56.944444 Tz (mercury ) Tj 2.566667 0 Td 48.611111 Tz (pool. ) Tj 1.633333 0 Td 87.5 Tz (A ) Tj 0.641667 0 Td 53.472222 Tz (platinum ) Tj 2.741667 0 Td 52.391975 Tz (gauze, ) Tj 2.080556 0 Td 54.282407 Tz (used ) Tj 1.497222 0 Td 50.231481 Tz (as ) Tj 51.428571 0 0 51.428571 0 2601.377551 Tm 25.2 0 Td 47.530864 Tz (auxiliary ) Tj 2.877778 0 Td 47.638889 Tz (electrode, ) Tj 3.208333 0 Td 61.574074 Tz (was ) Tj 1.4 0 Td 53.472222 Tz (placed ) Tj 2.255556 0 Td 45.37037 Tz (in ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 49.907407 Tz (other ) Tj 1.788889 0 Td 58.333333 Tz (compartment ) Tj 51.428571 0 0 51.428571 0 2560.547771 Tm 25.2 0 Td 45.010288 Tz (partition ) Tj 2.741667 0 Td 57.523148 Tz (from ) Tj 1.691667 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 48.206019 Tz (solution ) Tj 2.586111 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 57.87037 Tz (working ) Tj 2.683333 0 Td 46.990741 Tz (electrode. ) Tj 3.169444 0 Td 58.333333 Tz (Both ) Tj 51.428571 0 0 51.428571 0 2522.773537 Tm 25.180556 0 Td 58.333333 Tz (working ) Tj 2.780556 0 Td 60.493827 Tz (and ) Tj 1.438889 0 Td 47.530864 Tz (auxiliary ) Tj 2.955556 0 Td 56.983025 Tz (compartments ) Tj 4.491667 0 Td 52.211934 Tz (contained ) Tj 3.169444 0 Td 52.662037 Tz (22.5 ) Tj 1.652778 0 Td 82.638889 Tz (mL ) Tj 51.428571 0 0 51.428571 0 2483.933833 Tm 25.2 0 Td 46.548822 Tz (electrolyte ) Tj 3.383333 0 Td 46.342593 Tz (Solutions, ) Tj 3.111111 0 Td 58.981481 Tz (which ) Tj 2.080556 0 Td 59.143519 Tz (were ) Tj 1.730556 0 Td 52.824074 Tz (thoroughly ) Tj 3.5 0 Td 54.6875 Tz (degassed ) Tj 2.916667 0 Td 61.574074 Tz (by ) Tj 51.428571 0 0 51.428571 0 2443.140647 Tm 25.2 0 Td 53.703704 Tz (purging ) Tj 2.683333 0 Td 52.662037 Tz (with ) Tj 1.652778 0 Td 66.435185 Tz (Ar ) Tj 1.186111 0 Td 48.611111 Tz (for ) Tj 1.225 0 Td 63.194444 Tz (30 ) Tj 1.205556 0 Td 59.41358 Tz (min ) Tj 1.497222 0 Td 48.611111 Tz (prior ) Tj 1.808333 0 Td 48.611111 Tz (to ) Tj 0.991667 0 Td 55.092593 Tz (each ) Tj 1.75 0 Td 52.146465 Tz (experiment. ) Tj 51.428571 0 0 51.428571 0 2402.782166 Tm 25.219444 0 Td 51.446759 Tz (Faradaic ) Tj 2.722222 0 Td 46.666667 Tz (efficiency ) Tj 3.033333 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 54.444444 Tz (determined ) Tj 3.5 0 Td 52.662037 Tz (with ) Tj 1.516667 0 Td 59.953704 Tz (50 ) Tj 1.166667 0 Td 66.435185 Tz (LM ) Tj 1.011111 0 Td 59.722222 Tz (complex ) Tj 2.761111 0 Td 55.092593 Tz (2 ) Tj 51.428571 0 0 51.428571 0 2362.688889 Tm 25.2 0 Td 45.37037 Tz (at ) Tj 0.836111 0 Td 55.092593 Tz (an ) Tj 0.991667 0 Td 51.388889 Tz (applied ) Tj 2.469444 0 Td 47.170782 Tz (potential ) Tj 2.858333 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 51.851852 Tz (-1.3 ) Tj 1.594444 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 54.282407 Tz (-1.4 ) Tj 1.633333 0 Td 81.018519 Tz (V ) Tj 0.836111 0 Td 51.851852 Tz (vs ) Tj 0.952778 0 Td 63.194444 Tz (SHE. ) Tj 1.847222 0 Td 62.654321 Tz (The ) Tj 52.857143 0 0 52.857143 0 2324.049505 Tm 24.518919 0 Td 59.384384 Tz (Volume ) Tj 2.364865 0 Td 53.603604 Tz (of ) Tj 0.813514 0 Td 81.981982 Tz (H ) Tj 0.945946 0 Td 55.18018 Tz (produced ) Tj 2.875676 0 Td 52.027027 Tz (during ) Tj 2.043243 0 Td 44.66967 Tz (electrolysis ) Tj 3.462162 0 Td 59.90991 Tz (was ) Tj 1.305405 0 Td 53.288288 Tz (determined ) Tj 51.428571 0 0 51.428571 0 2284.142857 Tm 25.180556 0 Td 61.574074 Tz (by ) Tj 0.991667 0 Td 75.617284 Tz (GC-TCD ) Tj 2.936111 0 Td 55.092593 Tz (or ) Tj 0.913889 0 Td 57.523148 Tz (measured ) Tj 3.013889 0 Td 59.953704 Tz (by ) Tj 0.952778 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 52.932099 Tz (gas ) Tj 1.225 0 Td 45.37037 Tz (buret. ) Tj 1.905556 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 54.208754 Tz (experiments ) Tj 51.428571 0 0 51.428571 0 2245.60688 Tm 25.180556 0 Td 59.953704 Tz (were ) Tj 1.613889 0 Td 56.17284 Tz (performed ) Tj 3.208333 0 Td 45.37037 Tz (at ) Tj 0.738889 0 Td 60.925926 Tz (22C. ) Tj 2.022222 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 55.740741 Tz (vapor ) Tj 1.827778 0 Td 50.636574 Tz (pressure ) Tj 2.586111 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 54.444444 Tz (water ) Tj 1.788889 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 2204.676294 Tm 25.2 0 Td 61.574074 Tz (22C. ) Tj 2.002778 0 Td 50.555556 Tz (\(19.8 ) Tj 1.711111 0 Td 73.888889 Tz (mmHg\) ) Tj 2.391667 0 Td 62.654321 Tz (was ) Tj 1.283333 0 Td 50.411523 Tz (corrected ) Tj 2.877778 0 Td 46.990741 Tz (in ) Tj 0.738889 0 Td 48.316498 Tz (calculating ) Tj 3.344444 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 49.537037 Tz (current ) Tj 52.857143 0 0 52.857143 0 2168.445013 Tm 24.518919 0 Td 45.405405 Tz (efficiency ) Tj 2.932432 0 Td 59.90991 Tz (of ) Tj 0.87027 0 Td 59.90991 Tz (H, ) Tj 0.945946 0 Td 49.017199 Tz (production. ) Tj 51.428571 0 0 51.428571 0 2126.519608 Tm 25.2 0 Td 43.75 Tz (3. ) Tj 0.758333 0 Td 55.092593 Tz (General ) Tj 2.605556 0 Td 54.012346 Tz (Procedure ) Tj 3.169444 0 Td 47.530864 Tz (for ) Tj 1.108333 0 Td 49.074074 Tz (Photocatalytic ) Tj 4.413889 0 Td 59.548611 Tz (Hydrogen ) Tj 3.130556 0 Td 63.194444 Tz (Produc ) Tj 40 0 0 40 0 2092 Tm 32.375 0 Td 62.5 Tz (tion ) Tj 51.428571 0 0 51.428571 0 2048.652118 Tm 25.938889 0 Td 57.253086 Tz (For ) Tj 1.244444 0 Td 55.362654 Tz (photoinduced ) Tj 4.219444 0 Td 57.118056 Tz (hydrogen ) Tj 3.033333 0 Td 48.287037 Tz (evolution, ) Tj 3.188889 0 Td 53.472222 Tz (each ) Tj 1.594444 0 Td 57.79321 Tz (sample ) Tj 2.313889 0 Td 62.654321 Tz (was ) Tj 51.428571 0 0 51.428571 0 2009.601504 Tm 25.2 0 Td 53.06713 Tz (prepared ) Tj 2.741667 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 57.253086 Tz (130 ) Tj 1.263889 0 Td 79.398148 Tz (mL ) Tj 1.147222 0 Td 49.789562 Tz (rectangular ) Tj 3.461111 0 Td 46.666667 Tz (flask ) Tj 1.555556 0 Td 51.527778 Tz (containing ) Tj 3.325 0 Td 56.712963 Tz (10 ) Tj 0.894444 0 Td 81.018519 Tz (mL ) Tj 1.166667 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 1968.719298 Tm 25.277778 0 Td 46.450617 Tz (1.0 ) Tj 1.011111 0 Td 103.703704 Tz (M ) Tj 0.777778 0 Td 74.537037 Tz (pH ) Tj 1.069444 0 Td 50.771605 Tz (4.0 ) Tj 1.030556 0 Td 48.148148 Tz (acetate ) Tj 2.197222 0 Td 49.151235 Tz (buffer ) Tj 1.886111 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 48.611111 Tz (the ) Tj 1.011111 0 Td 53.472222 Tz (presence ) Tj 2.702778 0 Td 58.333333 Tz (of ) Tj 1.069444 0 Td 62.546296 Tz (Ru\(bpy\)Cl. ) Tj 51.428571 0 0 51.428571 0 1927.350785 Tm 25.219444 0 Td 46.180556 Tz (\(0.5 ) Tj 1.380556 0 Td 67.24537 Tz (mM\), ) Tj 1.847222 0 Td 49.826389 Tz (ascorbic ) Tj 2.663889 0 Td 50.231481 Tz (acid ) Tj 1.458333 0 Td 43.75 Tz (\(0.1 ) Tj 1.380556 0 Td 58.333333 Tz (M\), ) Tj 1.283333 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 58.333333 Tz (2 ) Tj 0.602778 0 Td 48.611111 Tz (\(5.0 ) Tj 1.419444 0 Td 56.712963 Tz (uM\). ) Tj 51.428571 0 0 51.428571 0 1888.680851 Tm 25.2 0 Td 63.734568 Tz (The ) Tj 1.477778 0 Td 49.016204 Tz (solution ) Tj 2.702778 0 Td 62.654321 Tz (was ) Tj 1.497222 0 Td 50.771605 Tz (sealed ) Tj 2.177778 0 Td 53.472222 Tz (with ) Tj 1.652778 0 Td 51.851852 Tz (a ) Tj 0.680556 0 Td 53.703704 Tz (septum, ) Tj 2.625 0 Td 55.092593 Tz (degassed ) Tj 3.013889 0 Td 55.740741 Tz (under ) Tj 52.857143 0 0 52.857143 0 1847.055627 Tm 24.5 0 Td 61.486486 Tz (vacuum ) Tj 2.478378 0 Td 57.807808 Tz (and ) Tj 1.286486 0 Td 48.198198 Tz (flushed ) Tj 2.232432 0 Td 52.815315 Tz (with ) Tj 1.475676 0 Td 64.324324 Tz (Argas ) Tj 2.156757 0 Td 49.189189 Tz (\(with ) Tj 1.740541 0 Td 77.252252 Tz (5% ) Tj 1.154054 0 Td 81.981982 Tz (CH ) Tj 1.494595 0 Td 50.45045 Tz (as ) Tj 0.832432 0 Td 44.932432 Tz (internal ) Tj 51.428571 0 0 51.428571 0 1808.20603 Tm 25.219444 0 Td 50.05144 Tz (standard\) ) Tj 2.975 0 Td 51.851852 Tz (four ) Tj 1.516667 0 Td 51.851852 Tz (times ) Tj 1.827778 0 Td 52.391975 Tz (before ) Tj 2.177778 0 Td 44.290123 Tz (irradiation. ) Tj 3.461111 0 Td 64.814815 Tz (The ) Tj 1.438889 0 Td 55.555556 Tz (samples ) Tj 2.663889 0 Td 58.333333 Tz (were ) Tj 51.428571 0 0 51.428571 0 1770.778325 Tm 25.2 0 Td 46.666667 Tz (irradiated ) Tj 2.936111 0 Td 59.953704 Tz (by ) Tj 0.894444 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 76.697531 Tz (LED ) Tj 1.555556 0 Td 43.425926 Tz (light ) Tj 1.477778 0 Td 55.902778 Tz (\(450 ) Tj 1.516667 0 Td 63.734568 Tz (nm\) ) Tj 1.283333 0 Td 45.37037 Tz (at ) Tj 0.7 0 Td 62.384259 Tz (room ) Tj 1.691667 0 Td 52.441077 Tz (temperature ) Tj 3.636111 0 Td 53.472222 Tz (with ) Tj 51.428571 0 0 51.428571 0 1730.579345 Tm 25.2 0 Td 50.636574 Tz (constant ) Tj 2.741667 0 Td 41.409465 Tz (stirring. ) Tj 2.547222 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 58.796296 Tz (amounts ) Tj 2.8 0 Td 56.712963 Tz (of ) Tj 0.875 0 Td 57.118056 Tz (hydrogen ) Tj 3.072222 0 Td 54.62963 Tz (evolved ) Tj 2.605556 0 Td 59.143519 Tz (were ) Tj 51.428571 0 0 51.428571 0 1693.099502 Tm 25.2 0 Td 54.768519 Tz (determined ) Tj 3.5 0 Td 59.953704 Tz (by ) Tj 0.952778 0 Td 52.932099 Tz (gas ) Tj 1.186111 0 Td 56.712963 Tz (chromatography ) Tj 5.016667 0 Td 52.5 Tz (using ) Tj 1.769444 0 Td 51.851852 Tz (a ) Tj 0.602778 0 Td 76.157407 Tz (HP ) Tj 1.108333 0 Td 60.763889 Tz (5890 ) Tj 1.672222 0 Td 45.910494 Tz (series ) Tj 51.428571 0 0 51.428571 0 1651.693069 Tm 25.219444 0 Td 37.268519 Tz (II ) Tj 0.661111 0 Td 62.654321 Tz (Gas ) Tj 1.322222 0 Td 58.333333 Tz (Chromatograph ) Tj 4.763889 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 79.938272 Tz (TCD ) Tj 1.652778 0 Td 49.421296 Tz (detector ) Tj 2.508333 0 Td 55.092593 Tz (or ) Tj 0.855556 0 Td 57.928241 Tz (measured ) Tj 2.936111 0 Td 61.574074 Tz (by ) Tj 51.428571 0 0 51.428571 0 1610.468983 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 52.932099 Tz (gas ) Tj 1.186111 0 Td 48.148148 Tz (burette ) Tj 2.177778 0 Td 53.472222 Tz (placed ) Tj 2.1 0 Td 46.990741 Tz (in ) Tj 0.738889 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 47.962963 Tz (circulated ) Tj 3.091667 0 Td 53.796296 Tz (water ) Tj 1.75 0 Td 52.662037 Tz (bath ) Tj 1.477778 0 Td 53.796296 Tz (maintained ) Tj 3.402778 0 Td 45.37037 Tz (at ) Tj 38.571429 0 0 38.571429 0 1577 Tm 33.6 0 Td 72.016461 Tz (22O ) Tj 1.711111 0 Td 69.135802 Tz (C. ) Tj 51.428571 0 0 51.428571 0 1498.443439 Tm 29.205556 0 Td 34.567901 Tz (II. ) Tj 0.913889 0 Td 50.378788 Tz (Preparation ) Tj 3.577778 0 Td 58.333333 Tz (and ) Tj 1.361111 0 Td 54.503367 Tz (Experiments ) Tj 51.428571 0 0 51.428571 0 1420.384615 Tm 32.355556 0 Td 61.111111 Tz (Example ) Tj 2.877778 0 Td 35.648148 Tz (1 ) Tj 51.428571 0 0 51.428571 0 1337.270073 Tm 26.561111 0 Td 51.131687 Tz (Synthesis ) Tj 2.994444 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 50.028935 Tz (Characterization ) Tj 5.055556 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 63.888889 Tz (Complex ) Tj 2.994444 0 Td 32.407407 Tz (1 ) Tj 0.505556 0 Td 61.574074 Tz (and ) Tj 51.428571 0 0 51.428571 0 1302.116883 Tm 32.297222 0 Td 63.425926 Tz (Complex ) Tj 2.916667 0 Td 55.092593 Tz (2 ) Tj 52.857143 0 0 52.857143 0 1213.848329 Tm 25.218919 0 Td 62.012012 Tz (The ) Tj 1.324324 0 Td 47.691441 Tz (reaction ) Tj 2.497297 0 Td 59.90991 Tz (of ) Tj 0.813514 0 Td 74.887387 Tz (CoC1.6HO ) Tj 3.840541 0 Td 51.238739 Tz (with ) Tj 1.532432 0 Td 64.414414 Tz (DPA-Bpy ) Tj 2.97027 0 Td 44.144144 Tz (in ) Tj 0.775676 0 Td 46.946947 Tz (refluxing ) Tj 51.428571 0 0 51.428571 0 1171.00369 Tm 25.2 0 Td 95.601852 Tz (CHCN ) Tj 2.508333 0 Td 44.444444 Tz (results ) Tj 2.1 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 50 Tz (reddish ) Tj 2.294444 0 Td 55.092593 Tz (cloudy ) Tj 2.177778 0 Td 46.450617 Tz (solution. ) Tj 2.702778 0 Td 51.851852 Tz (After ) Tj 1.730556 0 Td 40.06734 Tz (filtration, ) Tj 52.857143 0 0 52.857143 0 1128 Tm 24.5 0 Td 49.399399 Tz (the ) Tj 1.116216 0 Td 38.626126 Tz (filtrate ) Tj 2.043243 0 Td 63.063063 Tz (was ) Tj 1.362162 0 Td 47.927928 Tz (dried ) Tj 1.683784 0 Td 54.234234 Tz (under ) Tj 1.835135 0 Td 61.486486 Tz (vacuum ) Tj 2.459459 0 Td 56.756757 Tz (and ) Tj 1.248649 0 Td 59.384384 Tz (washed ) Tj 2.364865 0 Td 52.027027 Tz (with ) Tj 1.494595 0 Td 77.777778 Tz (EtO ) Tj 51.428571 0 0 51.428571 0 1093.976398 Tm 25.180556 0 Td 45.37037 Tz (to ) Tj 0.777778 0 Td 49.259259 Tz (yield ) Tj 1.672222 0 Td 59.722222 Tz (Co\(DPA-Bpy\)Cl. ) Tj 5.366667 0 Td 57.118056 Tz (\(complex ) Tj 3.013889 0 Td 45.37037 Tz (1\) ) Tj 0.738889 0 Td 50.231481 Tz (as ) Tj 0.816667 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 48.287037 Tz (light-pink ) Tj 3.052778 0 Td 84.259259 Tz (pow ) Tj 51.428571 0 0 51.428571 0 1045 Tm 25.2 0 Td 52.932099 Tz (der ) Tj 1.186111 0 Td 60.185185 Tz (\(Scheme ) Tj 2.858333 0 Td 37.808642 Tz (1\). ) Tj 51.428571 0 0 51.428571 0 1008.783626 Tm 25.938889 0 Td 52.932099 Tz (Refluxing ) Tj 3.266667 0 Td 56.712963 Tz (an ) Tj 1.088889 0 Td 57.407407 Tz (aqueous ) Tj 2.838889 0 Td 48.611111 Tz (solution ) Tj 2.780556 0 Td 56.712963 Tz (of ) Tj 0.991667 0 Td 63.888889 Tz (Complex ) Tj 3.15 0 Td 35.648148 Tz (1 ) Tj 0.738889 0 Td 45.37037 Tz (in ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 966.206289 Tm 25.2 0 Td 53.06713 Tz (presence ) Tj 2.741667 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 70.486111 Tz (AgPF ) Tj 2.158333 0 Td 49.691358 Tz (led ) Tj 1.069444 0 Td 48.611111 Tz (to ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 52.932099 Tz (formation ) Tj 3.052778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 56.712963 Tz (an ) Tj 0.875 0 Td 58.333333 Tz (aqua ) Tj 1.613889 0 Td 59.259259 Tz (complex ) Tj 52.857143 0 0 52.857143 0 924.395604 Tm 24.708108 0 Td 65.165165 Tz (Co\(DPA-Bpy\)\(OH\) ) Tj 6.12973 0 Td 57.387387 Tz (\(PF\), ) Tj 2.024324 0 Td 55.18018 Tz (\(complex ) Tj 2.875676 0 Td 42.042042 Tz (2\). ) Tj 0.945946 0 Td 63.063063 Tz (The ) Tj 1.343243 0 Td 49.74975 Tz (oxidation ) Tj 2.894595 0 Td 56.756757 Tz (of ) Tj 51.428571 0 0 51.428571 0 883.25931 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.897222 0 Td 35.648148 Tz (1 ) Tj 0.563889 0 Td 63.194444 Tz (by ) Tj 1.030556 0 Td 70.486111 Tz (AgPF ) Tj 2.275 0 Td 49.691358 Tz (led ) Tj 1.205556 0 Td 43.75 Tz (to ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 52.572016 Tz (formation ) Tj 3.169444 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 60.648148 Tz (complex ) Tj 2.838889 0 Td 43.75 Tz (2. ) Tj 57.142857 0 0 57.142857 0 838 Tm 22.6625 0 Td 53.666667 Tz (which ) Tj 1.8375 0 Td 55.416667 Tz (showed ) Tj 2.205 0 Td 51.041667 Tz (an ) Tj 0.84 0 Td 47.25 Tz (EPR-silent ) Tj 3.0275 0 Td 69.027778 Tz (Co' ) Tj 1.4875 0 Td 45.208333 Tz (center ) Tj 1.82 0 Td 47.25 Tz (\(FIG. ) Tj 1.645 0 Td 42.291667 Tz (4b\). ) Tj 40 0 0 40 0 720.086957 Tm 38.925 0 Td 63.888889 Tz (Scheme ) Tj 2.5 0 Td 41.666667 Tz (1. ) Tj 0.7 0 Td 51.851852 Tz (Synthesis ) Tj 2.975 0 Td 58.333333 Tz (of ) Tj 0.85 0 Td 37.5 Tz (1 ) Tj 0.525 0 Td 56.944444 Tz (and ) Tj 1.225 0 Td 41.666667 Tz (2. ) Tj 114.285714 0 0 114.285714 0 598 Tm 14.42875 0 Td 75.833333 Tz (rs ) Tj 40 0 0 40 0 563.041096 Tm 40.825 0 Td 95.833333 Tz (N ) Tj 1.675 0 Td 208.333333 Tz (2 ) Tj 40 0 0 40 0 486 Tm 45.075 0 Td 76.666667 Tz (CoCl2-6H2O ) Tj 20 0 0 20 0 470 Tm 89.9 0 Td 929.166667 Tz (He ) Tj 38.571429 0 0 38.571429 0 439 Tm 47.937037 0 Td 80.37037 Tz (CH3CN ) Tj 40 0 0 40 0 224 Tm 36.325 0 Td 91.071429 Tz (DPA-Bpy ) Tj 1.428571 0 0 1.428571 0 681 Tm 909.3 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 280 0 obj << /Length 1 >> stream q endstream endobj 281 0 obj << /Length 27487 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 14.505556 0 Td 76.157407 Tz (21 ) Tj 40 0 0 40 0 2913 Tm 17.35 0 Td 67.083333 Tz (-continued ) Tj 51.428571 0 0 51.428571 0 1757.919236 Tm 7.641667 0 Td 45.37037 Tz (a\) ) Tj 0.816667 0 Td 50.771605 Tz (Synthesis ) Tj 3.013889 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 60.966435 Tz (Co\(DPA-Bpy\)Cl]Cl ) Tj 6.125 0 Td 59.548611 Tz (\(Complex ) Tj 3.188889 0 Td 43.75 Tz (1\) ) Tj 51.428571 0 0 51.428571 0 1713.621622 Tm 13.086111 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 52.662037 Tz (Analysis ) Tj 52.857143 0 0 52.857143 0 1619.296296 Tm 6.810811 0 Td 59.90991 Tz (To ) Tj 0.908108 0 Td 53.603604 Tz (a ) Tj 0.567568 0 Td 47.691441 Tz (refluxed ) Tj 2.497297 0 Td 47.691441 Tz (solution ) Tj 2.478378 0 Td 56.756757 Tz (of ) Tj 0.813514 0 Td 59.90991 Tz (CoCl2.6H2O ) Tj 3.802703 0 Td 50.45045 Tz (\(0.207 ) Tj 2.005405 0 Td 44.144144 Tz (g. ) Tj 0.832432 0 Td 31.531532 Tz (1 ) Tj 0.491892 0 Td 62.432432 Tz (mmol\) ) Tj 52.857143 0 0 52.857143 0 1578.44782 Tm 6.091892 0 Td 45.720721 Tz (in ) Tj 0.87027 0 Td 55.18018 Tz (10 ) Tj 0.908108 0 Td 81.981982 Tz (mL ) Tj 1.22973 0 Td 92.22973 Tz (CHCN ) Tj 2.497297 0 Td 60.960961 Tz (was ) Tj 1.362162 0 Td 56.126126 Tz (added ) Tj 1.948649 0 Td 53.997748 Tz (dropwise ) Tj 2.837838 0 Td 53.603604 Tz (a ) Tj 0.586486 0 Td 47.691441 Tz (solution ) Tj 2.554054 0 Td 55.18018 Tz (of ) Tj 0.908108 0 Td 42.252252 Tz (1-\(2, ) Tj 51.428571 0 0 51.428571 0 1543.108959 Tm 6.261111 0 Td 49.494949 Tz (2'-bipyridin-6-methyl\) ) Tj 7 0 Td 50.951646 Tz (N.N'-Bis\(2-pyridyl ) Tj 6.008333 0 Td 53.240741 Tz (methyl\) ) Tj 2.683333 0 Td 59.62963 Tz (amine ) Tj 51.428571 0 0 51.428571 0 1497.984476 Tm 6.280556 0 Td 59.053498 Tz (\(DPA-Bpy, ) Tj 3.441667 0 Td 56.944444 Tz (0.367g, ) Tj 2.683333 0 Td 35.648148 Tz (1 ) Tj 0.563889 0 Td 64.166667 Tz (mmol\) ) Tj 2.138889 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 51.851852 Tz (5 ) Tj 0.563889 0 Td 85.87963 Tz (mL ) Tj 1.205556 0 Td 95.601852 Tz (CHCN ) Tj 2.547222 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 52.932099 Tz (period ) Tj 51.428571 0 0 51.428571 0 1455.311558 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 50.231481 Tz (15 ) Tj 0.836111 0 Td 51.851852 Tz (mins. ) Tj 1.730556 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 46.450617 Tz (resulting ) Tj 2.683333 0 Td 54.552469 Tz (cloudy ) Tj 2.177778 0 Td 48.206019 Tz (solution ) Tj 2.527778 0 Td 61.574074 Tz (was ) Tj 1.322222 0 Td 49.421296 Tz (refluxed ) Tj 2.547222 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 51.851852 Tz (6 ) Tj 51.428571 0 0 51.428571 0 1413.042781 Tm 6.241667 0 Td 49.691358 Tz (hrs ) Tj 1.205556 0 Td 60.493827 Tz (and ) Tj 1.4 0 Td 51.851852 Tz (then ) Tj 1.594444 0 Td 42.534722 Tz (filtered ) Tj 2.372222 0 Td 53.703704 Tz (through ) Tj 2.566667 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 48.611111 Tz (glass ) Tj 1.827778 0 Td 36.458333 Tz (frit ) Tj 1.205556 0 Td 59.41358 Tz (membrane. ) Tj 3.538889 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 1372.882709 Tm 6.261111 0 Td 39.699074 Tz (filtrate ) Tj 2.119444 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 53.148148 Tz (evaporated ) Tj 3.402778 0 Td 55.740741 Tz (under ) Tj 1.847222 0 Td 54.62963 Tz (reduced ) Tj 2.488889 0 Td 48.251029 Tz (pressure, ) Tj 2.819444 0 Td 50.411523 Tz (dissolved ) Tj 2.916667 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 1328.989196 Tm 6.261111 0 Td 67.12963 Tz (minimum ) Tj 2.975 0 Td 61.574074 Tz (amount ) Tj 2.352778 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 82.962963 Tz (CHCN, ) Tj 2.663889 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 59.953704 Tz (washed ) Tj 2.352778 0 Td 51.851852 Tz (with ) Tj 1.438889 0 Td 47.685185 Tz (diethyl ) Tj 2.177778 0 Td 49.907407 Tz (ether ) Tj 51.428571 0 0 51.428571 0 1292.02578 Tm 6.241667 0 Td 45.37037 Tz (to ) Tj 0.875 0 Td 48.611111 Tz (yield ) Tj 1.730556 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 53.703704 Tz (product ) Tj 2.508333 0 Td 50.231481 Tz (as ) Tj 0.894444 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 44.074074 Tz (light ) Tj 1.594444 0 Td 54.282407 Tz (pink ) Tj 1.575 0 Td 54.62963 Tz (powder. ) Tj 2.586111 0 Td 48.070988 Tz (Yield, ) Tj 2.061111 0 Td 51.851852 Tz (0.17 ) Tj 1.536111 0 Td 61.574074 Tz (g ) Tj 51.428571 0 0 51.428571 0 1245 Tm 6.280556 0 Td 54.552469 Tz (\(33%\). ) Tj 2.138889 0 Td 52.5 Tz (Anal. ) Tj 1.769444 0 Td 57.037037 Tz (Calcd ) Tj 1.925 0 Td 48.611111 Tz (for ) Tj 1.030556 0 Td 75.108932 Tz (CHCl2CoNs.\(H2O\)s: ) Tj 7.875 0 Td 55.092593 Tz (C, ) Tj 0.875 0 Td 50.231481 Tz (52.69; ) Tj 48.571429 0 0 48.571429 0 1205 Tm 6.65 0 Td 60.04902 Tz (H, ) Tj 1.091176 0 Td 51.470588 Tz (4.61; ) Tj 1.955882 0 Td 58.333333 Tz (N, ) Tj 1.173529 0 Td 51.470588 Tz (13.36. ) Tj 2.244118 0 Td 58.905229 Tz (Found: ) Tj 2.532353 0 Td 58.333333 Tz (C, ) Tj 1.091176 0 Td 52.042484 Tz (52.52; ) Tj 2.285294 0 Td 61.764706 Tz (H, ) Tj 1.111765 0 Td 51.470588 Tz (4.55; ) Tj 1.955882 0 Td 58.333333 Tz (N, ) Tj 1.194118 0 Td 50.326797 Tz (13.33. ) Tj 51.428571 0 0 51.428571 0 1164.88946 Tm 6.261111 0 Td 61.111111 Tz (ESI-MS: ) Tj 2.994444 0 Td 54.73251 Tz (m/z"461.1 ) Tj 3.441667 0 Td 52.932099 Tz (\(Calcd ) Tj 2.352778 0 Td 56.712963 Tz (m/z" ) Tj 1.769444 0 Td 48.611111 Tz (for ) Tj 1.438889 0 Td 60.709877 Tz (Co\(DPA-Bpy\)Cl." ) Tj 51.428571 0 0 51.428571 0 1120 Tm 6.261111 0 Td 48.611111 Tz (461.8\). ) Tj 57.142857 0 0 57.142857 0 1081.366492 Tm 6.3 0 Td 55.416667 Tz (The ) Tj 1.1725 0 Td 40.833333 Tz (crystal ) Tj 1.9075 0 Td 42.453704 Tz (structure ) Tj 2.4325 0 Td 51.041667 Tz (of ) Tj 0.7175 0 Td 43.75 Tz (the ) Tj 0.945 0 Td 69.027778 Tz (Co' ) Tj 1.4175 0 Td 52.5 Tz (form ) Tj 1.435 0 Td 51.041667 Tz (of ) Tj 0.7 0 Td 53.333333 Tz (complex ) Tj 2.4675 0 Td 32.083333 Tz (1 ) Tj 0.42 0 Td 47.25 Tz (\(FIG. ) Tj 51.428571 0 0 51.428571 0 1041.237624 Tm 6.3 0 Td 48.611111 Tz (1\) ) Tj 0.758333 0 Td 55.092593 Tz (confirmed ) Tj 3.208333 0 Td 45.37037 Tz (that ) Tj 1.322222 0 Td 66.666667 Tz (DPA-Bpy ) Tj 3.033333 0 Td 50.231481 Tz (serves ) Tj 2.022222 0 Td 50.231481 Tz (as ) Tj 0.816667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 51.041667 Tz (pentadentate ) Tj 3.888889 0 Td 51.311728 Tz (ligand ) Tj 51.428571 0 0 51.428571 0 997.427848 Tm 6.241667 0 Td 54.282407 Tz (with ) Tj 1.555556 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 71.296296 Tz (Co ) Tj 1.088889 0 Td 50.771605 Tz (center ) Tj 2.041667 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 51.851852 Tz (a ) Tj 0.602778 0 Td 46.8107 Tz (distorted ) Tj 2.741667 0 Td 50.87963 Tz (octahedral ) Tj 3.286111 0 Td 57.118056 Tz (geometry ) Tj 3.013889 0 Td 54.282407 Tz (with ) Tj 51.428571 0 0 51.428571 0 958.515337 Tm 6.241667 0 Td 61.574074 Tz (two ) Tj 1.341667 0 Td 46.018519 Tz (trans ) Tj 1.594444 0 Td 49.691358 Tz (pyridines ) Tj 2.897222 0 Td 50.925926 Tz (groups, ) Tj 2.372222 0 Td 49.074074 Tz (similar ) Tj 2.255556 0 Td 43.75 Tz (to ) Tj 0.738889 0 Td 46.180556 Tz (that ) Tj 1.283333 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 62.457912 Tz (Ru\(DPA-Bpy\) ) Tj 58.571429 0 0 58.571429 0 915.245707 Tm 5.497561 0 Td 43.394309 Tz (Cls. ) Tj 1.77561 0 Td 56.910569 Tz (The ) Tj 1.212195 0 Td 50.745257 Tz (UV-vis ) Tj 2.031707 0 Td 48.729675 Tz (spectrum ) Tj 2.543902 0 Td 52.642276 Tz (of ) Tj 0.768293 0 Td 55.284553 Tz (Complex ) Tj 2.595122 0 Td 34.146341 Tz (1 ) Tj 0.495122 0 Td 39.837398 Tz (in ) Tj 0.665854 0 Td 48.943089 Tz (water ) Tj 1.656098 0 Td 52.926829 Tz (shows ) Tj 51.428571 0 0 51.428571 0 872.023384 Tm 6.241667 0 Td 61.574074 Tz (two ) Tj 1.4 0 Td 49.074074 Tz (intense ) Tj 2.333333 0 Td 56.388889 Tz (bands ) Tj 1.983333 0 Td 46.990741 Tz (at ) Tj 0.816667 0 Td 60.493827 Tz (247 ) Tj 1.341667 0 Td 59.41358 Tz (and ) Tj 1.341667 0 Td 62.654321 Tz (300 ) Tj 1.419444 0 Td 72.916667 Tz (nm ) Tj 1.166667 0 Td 58.333333 Tz (from ) Tj 1.711111 0 Td 50.231481 Tz (ligand ) Tj 2.294444 0 Td 55.902778 Tz (t-st ) Tj 51.428571 0 0 51.428571 0 829.713755 Tm 6.241667 0 Td 44.830247 Tz (transitions, ) Tj 3.402778 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 52.256944 Tz (shoulder ) Tj 2.663889 0 Td 58.333333 Tz (peak ) Tj 1.575 0 Td 43.75 Tz (at ) Tj 0.7 0 Td 60.493827 Tz (337 ) Tj 1.302778 0 Td 60.493827 Tz (nm, ) Tj 1.263889 0 Td 60.493827 Tz (and ) Tj 1.263889 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 64.814815 Tz (weak ) Tj 1.730556 0 Td 52.662037 Tz (shoulder ) Tj 51.428571 0 0 51.428571 0 788 Tm 6.261111 0 Td 45.37037 Tz (at ) Tj 0.855556 0 Td 61.574074 Tz (420 ) Tj 1.458333 0 Td 72.916667 Tz (nm ) Tj 1.244444 0 Td 57.523148 Tz (from ) Tj 1.75 0 Td 52.5 Tz (metal ) Tj 1.944444 0 Td 54.012346 Tz (d-d ) Tj 1.322222 0 Td 45.046296 Tz (transition ) Tj 3.072222 0 Td 51.851852 Tz (\(FIG. ) Tj 1.905556 0 Td 44.290123 Tz (2\). ) Tj 1.088889 0 Td 64.814815 Tz (The ) Tj 1.555556 0 Td 71.296296 Tz (EPR ) Tj 51.428571 0 0 51.428571 0 750.923845 Tm 6.280556 0 Td 54.6875 Tz (spectrum ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.875 0 Td 59.259259 Tz (complex ) Tj 2.819444 0 Td 32.407407 Tz (1 ) Tj 0.525 0 Td 50.05144 Tz (exhibited ) Tj 2.975 0 Td 57.407407 Tz (rhombic ) Tj 2.683333 0 Td 44.290123 Tz (splitting ) Tj 2.605556 0 Td 49.537037 Tz (pattern ) Tj 51.428571 0 0 51.428571 0 707.642487 Tm 6.241667 0 Td 54.282407 Tz (with ) Tj 1.536111 0 Td 64.814815 Tz (g ) Tj 0.661111 0 Td 50.771605 Tz (values ) Tj 2.061111 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 46.666667 Tz (5.56, ) Tj 1.672222 0 Td 48.611111 Tz (3.95, ) Tj 1.691667 0 Td 60.493827 Tz (and ) Tj 1.380556 0 Td 46.018519 Tz (1.98, ) Tj 1.633333 0 Td 51.851852 Tz (suggesting ) Tj 3.383333 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 60.763889 Tz (pres ) Tj 58.571429 0 0 58.571429 0 665.278075 Tm 5.497561 0 Td 48.373984 Tz (ence ) Tj 1.365854 0 Td 52.642276 Tz (of ) Tj 0.734146 0 Td 51.219512 Tz (a ) Tj 0.495122 0 Td 44.896116 Tz (high-spin ) Tj 2.629268 0 Td 57.859079 Tz (Co' ) Tj 1.280488 0 Td 44.579946 Tz (center ) Tj 1.77561 0 Td 46.097561 Tz (\(FIG. ) Tj 1.604878 0 Td 42.682927 Tz (4a\). ) Tj 51.428571 0 0 51.428571 0 625.723404 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 48.611111 Tz (cyclic ) Tj 2.041667 0 Td 60.763889 Tz (voltammogram ) Tj 4.627778 0 Td 61.574074 Tz (of ) Tj 0.875 0 Td 59.722222 Tz (complex ) Tj 2.838889 0 Td 32.407407 Tz (1 ) Tj 0.525 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 95.601852 Tz (CHCN ) Tj 2.547222 0 Td 60.493827 Tz (dis ) Tj 51.428571 0 0 51.428571 0 582.295918 Tm 6.261111 0 Td 51.203704 Tz (plays ) Tj 1.808333 0 Td 49.259259 Tz (three ) Tj 1.769444 0 Td 47.638889 Tz (reversible ) Tj 3.15 0 Td 54.444444 Tz (redox ) Tj 1.886111 0 Td 47.314815 Tz (potentials ) Tj 3.130556 0 Td 45.37037 Tz (at ) Tj 0.816667 0 Td 47.314815 Tz (0.35, ) Tj 1.75 0 Td 50.771605 Tz (-0.94, ) Tj 2.080556 0 Td 61.574074 Tz (and ) Tj 60 0 0 60 0 539.841969 Tm 5.383333 0 Td 46.111111 Tz (-1.53 ) Tj 1.65 0 Td 72.222222 Tz (V ) Tj 0.65 0 Td 41.666667 Tz (\(vs ) Tj 0.966667 0 Td 50.555556 Tz (SHE\), ) Tj 1.75 0 Td 43.888889 Tz (assignable ) Tj 2.85 0 Td 37.5 Tz (to ) Tj 0.666667 0 Td 76.388889 Tz (Co', ) Tj 2.066667 0 Td 61.111111 Tz (Co', ) Tj 1.7 0 Td 50 Tz (and ) Tj 1.133333 0 Td 62.5 Tz (Co', ) Tj 51.428571 0 0 51.428571 0 500.871959 Tm 6.261111 0 Td 48.611111 Tz (respectively ) Tj 3.752778 0 Td 55.092593 Tz (\(FIGS. ) Tj 2.255556 0 Td 58.333333 Tz (5a ) Tj 0.952778 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 46.990741 Tz (5b\). ) Tj 1.419444 0 Td 46.990741 Tz (In ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 62.384259 Tz (same ) Tj 1.75 0 Td 48.148148 Tz (region, ) Tj 2.294444 0 Td 50.771605 Tz (ligand ) Tj 51.428571 0 0 51.428571 0 457.084211 Tm 6.280556 0 Td 67.12963 Tz (DPA-Bpy ) Tj 3.072222 0 Td 55.092593 Tz (does ) Tj 1.594444 0 Td 50.771605 Tz (not ) Tj 1.147222 0 Td 62.384259 Tz (show ) Tj 1.788889 0 Td 57.253086 Tz (any ) Tj 1.322222 0 Td 53.796296 Tz (redox ) Tj 1.866667 0 Td 54.372428 Tz (behaviour ) Tj 3.169444 0 Td 51.203704 Tz (\(FIG. ) Tj 1.788889 0 Td 46.180556 Tz (5c\). ) Tj 51.428571 0 0 51.428571 0 381.188571 Tm 7.408333 0 Td 51.851852 Tz (b\) ) Tj 0.855556 0 Td 51.131687 Tz (Synthesis ) Tj 3.013889 0 Td 58.333333 Tz (of ) Tj 1.011111 0 Td 67.407407 Tz (Co\(DPA-Bpy\)\(OH\) ) Tj 6.319444 0 Td 65.625 Tz (\(PF\) ) Tj 2.061111 0 Td 78.587963 Tz (\(Com ) Tj 51.428571 0 0 51.428571 0 340.560284 Tm 11.919444 0 Td 52.662037 Tz (plex ) Tj 1.497222 0 Td 50.231481 Tz (2\) ) Tj 0.836111 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 53.06713 Tz (Analysis ) Tj 51.428571 0 0 51.428571 0 254.649513 Tm 7 0 Td 61.574074 Tz (To ) Tj 1.108333 0 Td 55.092593 Tz (a ) Tj 0.7 0 Td 48.611111 Tz (solution ) Tj 2.702778 0 Td 59.953704 Tz (of ) Tj 1.186111 0 Td 60.763889 Tz (Co\(DPA-Bpy\)Cl]Cl ) Tj 6.241667 0 Td 52.777778 Tz (\(0.2665 ) Tj 2.586111 0 Td 45.37037 Tz (g, ) Tj 0.933333 0 Td 52.662037 Tz (0.54 ) Tj 51.428571 0 0 51.428571 0 211.486339 Tm 6.261111 0 Td 64.814815 Tz (mmol\) ) Tj 2.275 0 Td 43.75 Tz (in ) Tj 0.933333 0 Td 51.851852 Tz (15 ) Tj 0.972222 0 Td 82.638889 Tz (mL ) Tj 1.302778 0 Td 108.564815 Tz (HO ) Tj 1.633333 0 Td 61.574074 Tz (was ) Tj 1.438889 0 Td 57.685185 Tz (added ) Tj 2.061111 0 Td 55.092593 Tz (dropwise ) Tj 2.936111 0 Td 55.092593 Tz (a ) Tj 0.661111 0 Td 48.611111 Tz (solution ) Tj 2.644444 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 169.288515 Tm 6.261111 0 Td 71.296296 Tz (AgPF ) Tj 2.294444 0 Td 52.314815 Tz (\(0.4554 ) Tj 2.527778 0 Td 43.75 Tz (g, ) Tj 0.913889 0 Td 46.450617 Tz (1.8 ) Tj 1.147222 0 Td 64.166667 Tz (mmol\) ) Tj 2.216667 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 56.712963 Tz (10 ) Tj 0.972222 0 Td 82.638889 Tz (mL ) Tj 1.244444 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 105.324074 Tz (HO ) Tj 1.575 0 Td 56.388889 Tz (under ) Tj 1.925 0 Td 66.435185 Tz (Ar ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.444444 0 Td 77.777778 Tz (22 ) Tj 51.428571 0 0 51.428571 0 2914.841432 Tm 25.2 0 Td 53.030303 Tz (atmosphere. ) Tj 3.752778 0 Td 64.814815 Tz (The ) Tj 1.438889 0 Td 47.800926 Tz (reaction ) Tj 2.605556 0 Td 53.240741 Tz (mixture ) Tj 2.508333 0 Td 60.493827 Tz (was ) Tj 1.380556 0 Td 49.421296 Tz (refluxed ) Tj 2.644444 0 Td 47.530864 Tz (for ) Tj 1.147222 0 Td 53.472222 Tz (12 ) Tj 0.913889 0 Td 43.75 Tz (hrs. ) Tj 51.428571 0 0 51.428571 0 2872.760351 Tm 25.2 0 Td 51.851852 Tz (After ) Tj 1.808333 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 46.843434 Tz (precipitate ) Tj 3.325 0 Td 62.654321 Tz (was ) Tj 1.4 0 Td 42.939815 Tz (filtered ) Tj 2.294444 0 Td 53.703704 Tz (through ) Tj 2.508333 0 Td 42.12963 Tz (celite, ) Tj 2.022222 0 Td 55.092593 Tz (water ) Tj 1.886111 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 2827.282051 Tm 25.2 0 Td 60.648148 Tz (removed ) Tj 2.819444 0 Td 56.388889 Tz (under ) Tj 1.963889 0 Td 54.62963 Tz (reduced ) Tj 2.566667 0 Td 50.636574 Tz (pressure ) Tj 2.722222 0 Td 58.333333 Tz (and ) Tj 1.322222 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 49.537037 Tz (residue ) Tj 2.372222 0 Td 61.574074 Tz (was ) Tj 1.419444 0 Td 59.41358 Tz (dis ) Tj 48.571429 0 0 48.571429 0 2784 Tm 26.702941 0 Td 55.473856 Tz (Solved ) Tj 2.45 0 Td 48.039216 Tz (in ) Tj 1.070588 0 Td 70.098039 Tz (minimum ) Tj 3.417647 0 Td 65.196078 Tz (amount ) Tj 2.779412 0 Td 61.764706 Tz (of ) Tj 1.111765 0 Td 56.427015 Tz (methanol, ) Tj 3.5 0 Td 64.624183 Tz (washed ) Tj 2.779412 0 Td 57.47549 Tz (with ) Tj 51.428571 0 0 51.428571 0 2741.463054 Tm 25.2 0 Td 47.685185 Tz (diethyl ) Tj 2.158333 0 Td 44.830247 Tz (ether, ) Tj 1.769444 0 Td 58.333333 Tz (and ) Tj 1.225 0 Td 49.907407 Tz (dried ) Tj 1.672222 0 Td 55.740741 Tz (under ) Tj 1.827778 0 Td 62.654321 Tz (vacuum ) Tj 2.45 0 Td 43.75 Tz (to ) Tj 0.719444 0 Td 49.691358 Tz (get ) Tj 1.05 0 Td 49.691358 Tz (the ) Tj 1.011111 0 Td 54.552469 Tz (yellow ) Tj 2.177778 0 Td 47.314815 Tz (solid ) Tj 51.428571 0 0 51.428571 0 2700.13369 Tm 25.394444 0 Td 66.975309 Tz (Co\(DPA-Bpy\)\(OH\) ) Tj 6.3 0 Td 66.435185 Tz (\(PF\) ) Tj 2.313889 0 Td 60.358796 Tz (\(Complex ) Tj 3.325 0 Td 51.851852 Tz (2\) ) Tj 1.030556 0 Td 48.070988 Tz (Yield: ) Tj 2.216667 0 Td 52.662037 Tz (0.39 ) Tj 1.672222 0 Td 68.055556 Tz (g ) Tj 52.857143 0 0 52.857143 0 2653.184466 Tm 24.537838 0 Td 53.078078 Tz (\(88%\). ) Tj 2.156757 0 Td 58.558559 Tz (ESI-MS: ) Tj 2.686486 0 Td 54.654655 Tz (m/z'587.9 ) Tj 3.178378 0 Td 52.027027 Tz (\(Calcd ) Tj 2.081081 0 Td 54.391892 Tz (m/z" ) Tj 1.57027 0 Td 46.246246 Tz (for ) Tj 1.040541 0 Td 59.121622 Tz ([Co\(DPA-Bpy\) ) Tj 44.857143 0 0 44.857143 0 2610.98249 Tm 28.914013 0 Td 80.502477 Tz (\(OH\)\(PF\), ) Tj 6.55414 0 Td 54.670913 Tz (588.4\). ) Tj 4.414013 0 Td 60.191083 Tz (Anal. ) Tj 3.968153 0 Td 66.135881 Tz (Calcd ) Tj 4.079618 0 Td 56.970984 Tz (for ) Tj 50 0 0 50 0 2564 Tm 25.92 0 Td 83.333333 Tz (C.H.CoF ) Tj 3.78 0 Td 98.095238 Tz (sNOPHO: ) Tj 4.64 0 Td 56.666667 Tz (C, ) Tj 1.16 0 Td 52.222222 Tz (30.82; ) Tj 2.48 0 Td 55 Tz (H, ) Tj 1.16 0 Td 49.333333 Tz (2.70: ) Tj 2.04 0 Td 58.333333 Tz (N, ) Tj 1.22 0 Td 48.666667 Tz (7.81. ) Tj 48.571429 0 0 48.571429 0 2522 Tm 26.702941 0 Td 59.477124 Tz (Found: ) Tj 2.408824 0 Td 58.333333 Tz (C, ) Tj 0.967647 0 Td 53.186275 Tz (30.73; ) Tj 2.223529 0 Td 60.04902 Tz (H, ) Tj 1.008824 0 Td 50.784314 Tz (2.81; ) Tj 1.811765 0 Td 60.04902 Tz (N, ) Tj 1.008824 0 Td 50.098039 Tz (7.80. ) Tj 51.428571 0 0 51.428571 0 2470.866225 Tm 25.919444 0 Td 63.599537 Tz (Compared ) Tj 3.286111 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 59.722222 Tz (complex ) Tj 2.819444 0 Td 38.888889 Tz (1, ) Tj 0.738889 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 58.333333 Tz (2 ) Tj 0.622222 0 Td 49.421296 Tz (displays ) Tj 2.605556 0 Td 59.953704 Tz (an ) Tj 0.952778 0 Td 60.493827 Tz (absorp ) Tj 51.428571 0 0 51.428571 0 2421 Tm 25.180556 0 Td 46.990741 Tz (tion ) Tj 1.341667 0 Td 59.143519 Tz (band ) Tj 1.594444 0 Td 45.37037 Tz (at ) Tj 0.758333 0 Td 60.493827 Tz (470 ) Tj 1.283333 0 Td 72.916667 Tz (nm ) Tj 1.108333 0 Td 57.523148 Tz (from ) Tj 1.613889 0 Td 53.148148 Tz (metal ) Tj 1.788889 0 Td 54.012346 Tz (d-d ) Tj 1.186111 0 Td 45.046296 Tz (transition ) Tj 2.916667 0 Td 52.5 Tz (\(FIG. ) Tj 1.808333 0 Td 41.049383 Tz (2\). ) Tj 0.952778 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 2378.867322 Tm 25.2 0 Td 64.814815 Tz (pK, ) Tj 1.341667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.030556 0 Td 52.441077 Tz (coordinated ) Tj 3.636111 0 Td 110.185185 Tz (HO ) Tj 1.497222 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 60.185185 Tz (complex ) Tj 2.683333 0 Td 58.333333 Tz (2 ) Tj 0.544444 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 54.444444 Tz (determined ) Tj 3.422222 0 Td 45.37037 Tz (to ) Tj 51.428571 0 0 51.428571 0 2336.452736 Tm 25.180556 0 Td 61.574074 Tz (be ) Tj 0.894444 0 Td 50.771605 Tz (5.0 ) Tj 1.05 0 Td 58.333333 Tz (by ) Tj 0.875 0 Td 41.666667 Tz (fitting ) Tj 1.905556 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 74.537037 Tz (pH ) Tj 1.069444 0 Td 41.769547 Tz (titration ) Tj 2.430556 0 Td 54.444444 Tz (curve ) Tj 1.769444 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 59.259259 Tz (complex ) Tj 2.663889 0 Td 58.333333 Tz (2 ) Tj 0.525 0 Td 58.333333 Tz (from ) Tj 1.555556 0 Td 76.157407 Tz (pH ) Tj 51.428571 0 0 51.428571 0 2290 Tm 25.258333 0 Td 35.648148 Tz (1 ) Tj 0.583333 0 Td 43.75 Tz (to ) Tj 0.777778 0 Td 58.333333 Tz (9 ) Tj 0.602778 0 Td 53.148148 Tz (\(FIG. ) Tj 1.827778 0 Td 43.209877 Tz (3\). ) Tj 51.428571 0 0 51.428571 0 2236.579809 Tm 25.938889 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 48.611111 Tz (1.0 ) Tj 1.088889 0 Td 106.944444 Tz (M ) Tj 0.894444 0 Td 57.79321 Tz (sodium ) Tj 2.372222 0 Td 54.73251 Tz (phosphate ) Tj 3.188889 0 Td 48.611111 Tz (buffer ) Tj 1.944444 0 Td 45.37037 Tz (at ) Tj 0.758333 0 Td 76.157407 Tz (pH ) Tj 1.147222 0 Td 44.560185 Tz (7.0, ) Tj 1.322222 0 Td 59.722222 Tz (complex ) Tj 2.761111 0 Td 55.092593 Tz (2 ) Tj 51.428571 0 0 51.428571 0 2191.343137 Tm 25.2 0 Td 47.800926 Tz (exhibits ) Tj 2.45 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 55.497685 Tz (sequence ) Tj 2.838889 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 60.493827 Tz (two ) Tj 1.283333 0 Td 54.444444 Tz (redox ) Tj 1.769444 0 Td 51.851852 Tz (events ) Tj 2.041667 0 Td 51.851852 Tz (centered ) Tj 2.644444 0 Td 42.12963 Tz (at ) Tj 0.680556 0 Td 51.851852 Tz (0.15 ) Tj 1.419444 0 Td 60.493827 Tz (and ) Tj 60 0 0 60 0 2148.614865 Tm 21.616667 0 Td 47.777778 Tz (0.90 ) Tj 1.75 0 Td 72.222222 Tz (V ) Tj 0.766667 0 Td 42.592593 Tz (\(vs ) Tj 1.1 0 Td 51.111111 Tz (SHE\), ) Tj 1.866667 0 Td 45.940171 Tz (corresponding ) Tj 3.9 0 Td 41.666667 Tz (to ) Tj 0.833333 0 Td 92.592593 Tz (Co' ) Tj 1.983333 0 Td 50.925926 Tz (and ) Tj 1.233333 0 Td 62.5 Tz (Co', ) Tj 60 0 0 60 0 2107.346991 Tm 21.583333 0 Td 42.12963 Tz (respectively ) Tj 3.283333 0 Td 45 Tz (\(FIG. ) Tj 1.633333 0 Td 39.583333 Tz (15\). ) Tj 1.183333 0 Td 55.555556 Tz (The ) Tj 1.233333 0 Td 93.518519 Tz (Co' ) Tj 1.933333 0 Td 46.759259 Tz (couple ) Tj 1.916667 0 Td 42.361111 Tz (displays ) Tj 2.283333 0 Td 50 Tz (a ) Tj 0.533333 0 Td 81.944444 Tz (pH ) Tj 51.428571 0 0 51.428571 0 2064.188602 Tm 25.2 0 Td 55.452675 Tz (dependent ) Tj 3.383333 0 Td 55.092593 Tz (redox ) Tj 2.022222 0 Td 47.530864 Tz (potential ) Tj 2.975 0 Td 52.777778 Tz (change, ) Tj 2.625 0 Td 53.472222 Tz (with ) Tj 1.691667 0 Td 55.092593 Tz (a ) Tj 0.738889 0 Td 50.555556 Tz (slope ) Tj 1.925 0 Td 56.712963 Tz (of ) Tj 0.991667 0 Td 60.493827 Tz (-48 ) Tj 51.428571 0 0 51.428571 0 2019.597701 Tm 25.2 0 Td 72.592593 Tz (mV/pH ) Tj 2.586111 0 Td 45.37037 Tz (in ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 53.148148 Tz (range ) Tj 1.983333 0 Td 59.953704 Tz (of ) Tj 0.991667 0 Td 74.537037 Tz (pH ) Tj 1.283333 0 Td 51.851852 Tz (5-8 ) Tj 1.380556 0 Td 51.851852 Tz (\(FIG. ) Tj 1.983333 0 Td 43.209877 Tz (6\), ) Tj 1.186111 0 Td 51.851852 Tz (suggesting ) Tj 3.480556 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 1977.598972 Tm 25.2 0 Td 53.009259 Tz (proton-coupled ) Tj 4.9 0 Td 49.016204 Tz (electron ) Tj 2.819444 0 Td 47.395833 Tz (transfer ) Tj 2.702778 0 Td 49.016204 Tz (process. ) Tj 2.897222 0 Td 57.928241 Tz (However, ) Tj 3.247222 0 Td 50.771605 Tz (the ) Tj 60 0 0 60 0 1937.547945 Tm 21.6 0 Td 90.740741 Tz (Co' ) Tj 2.016667 0 Td 46.759259 Tz (couple ) Tj 2 0 Td 47.222222 Tz (only ) Tj 1.466667 0 Td 48.412698 Tz (changes ) Tj 2.366667 0 Td 39.236111 Tz (slightly ) Tj 2.233333 0 Td 47.222222 Tz (over ) Tj 1.45 0 Td 63.888889 Tz (pH ) Tj 1.2 0 Td 37.5 Tz (1-5. ) Tj 1.233333 0 Td 55.555556 Tz (The ) Tj 51.428571 0 0 51.428571 0 1893.179747 Tm 25.219444 0 Td 54.282407 Tz (Pourbaix ) Tj 2.819444 0 Td 56.481481 Tz (diagram ) Tj 2.605556 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 51.851852 Tz (2 ) Tj 0.583333 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 48.287037 Tz (consistent ) Tj 3.091667 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 68.055556 Tz (pKa ) Tj 1.458333 0 Td 56.712963 Tz (of ) Tj 57.142857 0 0 57.142857 0 1850.210867 Tm 22.68 0 Td 44.722222 Tz (4.8 ) Tj 0.98 0 Td 41.805556 Tz (for ) Tj 0.91 0 Td 44.722222 Tz (the ) Tj 0.9275 0 Td 69.027778 Tz (Co' ) Tj 1.9075 0 Td 83.125 Tz (OH ) Tj 1.365 0 Td 42.65625 Tz (species, ) Tj 2.205 0 Td 43.75 Tz (similar ) Tj 1.9775 0 Td 40.833333 Tz (to ) Tj 0.6475 0 Td 40.833333 Tz (that ) Tj 1.1025 0 Td 47.760417 Tz (obtained ) Tj 2.4325 0 Td 53.229167 Tz (from ) Tj 51.428571 0 0 51.428571 0 1810.943662 Tm 25.2 0 Td 74.537037 Tz (pH ) Tj 1.147222 0 Td 42.12963 Tz (titration ) Tj 2.527778 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 42.12963 Tz (2. ) Tj 51.428571 0 0 51.428571 0 1710.04 Tm 32.355556 0 Td 61.111111 Tz (Example ) Tj 2.8 0 Td 58.333333 Tz (2 ) Tj 51.428571 0 0 51.428571 0 1599.688889 Tm 26.658333 0 Td 50.771605 Tz (Synthesis ) Tj 2.975 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 69.270833 Tz (DPA-ABpy ) Tj 3.597222 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 55.740741 Tz (Metal ) Tj 1.925 0 Td 60.493827 Tz (Complexes ) Tj 3.5 0 Td 58.333333 Tz (3 ) Tj 40 0 0 40 0 1561 Tm 42.55 0 Td 76.388889 Tz (and ) Tj 1.65 0 Td 79.166667 Tz (4 ) Tj 51.428571 0 0 51.428571 0 1462.166879 Tm 25.919444 0 Td 63.194444 Tz (To ) Tj 0.933333 0 Td 53.240741 Tz (provide ) Tj 2.411111 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 49.826389 Tz (possible ) Tj 2.586111 0 Td 57.973251 Tz (H-bonding ) Tj 3.325 0 Td 56.944444 Tz (network ) Tj 2.547222 0 Td 45.37037 Tz (to ) Tj 0.758333 0 Td 77.777778 Tz (M-H ) Tj 1.575 0 Td 50 Tz (species ) Tj 51.428571 0 0 51.428571 0 1419.619165 Tm 25.2 0 Td 52.932099 Tz (during ) Tj 2.158333 0 Td 56.712963 Tz (H2 ) Tj 0.933333 0 Td 50.378788 Tz (production, ) Tj 3.558333 0 Td 56.712963 Tz (an ) Tj 0.894444 0 Td 72.376543 Tz (NMe-group ) Tj 4.141667 0 Td 61.574074 Tz (was ) Tj 1.322222 0 Td 52.175926 Tz (introduced ) Tj 3.344444 0 Td 45.37037 Tz (into ) Tj 51.428571 0 0 51.428571 0 1379.011933 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 66.666667 Tz (DPA-Bpy ) Tj 3.013889 0 Td 47.800926 Tz (scaffold ) Tj 2.45 0 Td 60.984848 Tz (\(DPA-ABpy\), ) Tj 4.238889 0 Td 58.333333 Tz (which ) Tj 1.944444 0 Td 62.654321 Tz (was ) Tj 1.341667 0 Td 51.262626 Tz (synthesized ) Tj 51.428571 0 0 51.428571 0 1334.537445 Tm 25.180556 0 Td 55.092593 Tz (based ) Tj 1.925 0 Td 56.712963 Tz (on ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 51.851852 Tz (following ) Tj 3.052778 0 Td 63.734568 Tz (Scheme ) Tj 2.547222 0 Td 42.12963 Tz (2. ) Tj 40 0 0 40 0 1214.046512 Tm 37.825 0 Td 63.194444 Tz (Scheme ) Tj 2.45 0 Td 43.75 Tz (2. ) Tj 0.725 0 Td 51.851852 Tz (Synthesis ) Tj 2.975 0 Td 58.333333 Tz (of ) Tj 0.95 0 Td 82.407407 Tz (DPA-ABpy. ) Tj 40 0 0 40 0 1118.333333 Tm 35.85 0 Td 208.333333 Tz (N ) Tj 6.725 0 Td 60.416667 Tz (BuLi ) Tj 20 0 0 20 0 1090 Tm 83.6 0 Td 397.222222 Tz (-e- ) Tj 35.714286 0 0 35.714286 0 1057.227273 Tm 40.824 0 Td 140 Tz (2 ) Tj 3.948 0 Td 98 Tz (OH ) Tj 2.24 0 Td 80.888889 Tz (BuSnCl ) Tj 31.428571 0 0 31.428571 0 1025 Tm 41.3 0 Td 76.893939 Tz (Br ) Tj 4.072727 0 Td 121.969697 Tz (N ) Tj 47.142857 0 0 47.142857 0 971 Tm 40.133333 0 Td 90.151515 Tz (21 ) Tj 38.571429 0 0 38.571429 0 891 Tm 49.051852 0 Td 155.555556 Tz (N ) Tj 31.428571 0 0 31.428571 0 867 Tm 61.504545 0 Td 121.969697 Tz (N ) Tj 40 0 0 40 0 760 Tm 47.55 0 Td 54.62963 Tz (Pd\(PPh3\)3 ) Tj 40 0 0 40 0 588 Tm 48.275 0 Td 54.166667 Tz (PPh3, ) Tj 1.825 0 Td 60.416667 Tz (CBra ) Tj 20 0 0 20 0 568 Tm 96.15 0 Td 720.833333 Tz (-- ) Tj 37.142857 0 0 37.142857 0 409.5625 Tm 52.446154 0 Td 103.205128 Tz (N ) Tj 4.253846 0 Td 183.974359 Tz (N ) Tj 58.571429 0 0 58.571429 0 374 Tm 33.27561 0 Td 29.878049 Tz (ii ) Tj 1.809756 0 Td 17.073171 Tz (|| ) Tj 37.142857 0 0 37.142857 0 341.462687 Tm 55.111538 0 Td 103.205128 Tz (N ) Tj 1.588462 0 Td 98.717949 Tz (21 ) Tj 31.428571 0 0 31.428571 0 287 Tm 61.027273 0 Td 90.151515 Tz (DIPEA ) Tj 1.428571 0 0 1.428571 0 2336 Tm 394.1 0 Td 116.666667 Tz ( ) Tj 1.428571 0 0 1.428571 0 892 Tm 905.8 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 282 0 obj << /Length 1 >> stream q endstream endobj 283 0 obj << /Length 32047 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.113514 0 Td 75.675676 Tz (23 ) Tj 40 0 0 40 0 2913 Tm 17.35 0 Td 67.083333 Tz (-continued ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 40 0 0 40 0 2401 Tm 21.95 0 Td 91.666667 Tz (DPA-ABPy ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 51.428571 0 0 51.428571 0 2288.732165 Tm 7 0 Td 61.574074 Tz (The ) Tj 1.341667 0 Td 48.611111 Tz (reaction ) Tj 2.527778 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 70.081019 Tz (DPA-ABpy ) Tj 3.558333 0 Td 52.662037 Tz (with ) Tj 1.497222 0 Td 72.792023 Tz (Ni\(CHCN\)\(BF\), ) Tj 5.930556 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 2248 Tm 6.261111 0 Td 76.157407 Tz (Co\(CHCN\) ) Tj 3.927778 0 Td 66.435185 Tz (\(PF\) ) Tj 2.236111 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 55.092593 Tz (a ) Tj 0.758333 0 Td 59.62963 Tz (mixed ) Tj 2.177778 0 Td 48.206019 Tz (solution ) Tj 2.702778 0 Td 59.953704 Tz (of ) Tj 0.972222 0 Td 62.87037 Tz (acetone/HO ) Tj 51.428571 0 0 51.428571 0 2211.501326 Tm 6.280556 0 Td 46.666667 Tz (\(1:9\) ) Tj 1.827778 0 Td 43.981481 Tz (results ) Tj 2.255556 0 Td 45.37037 Tz (in ) Tj 0.952778 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 52.572016 Tz (formation ) Tj 3.247222 0 Td 59.953704 Tz (of ) Tj 1.225 0 Td 66.840278 Tz (Ni\(DPA-ABpy\)\(HO\) ) Tj 51.428571 0 0 51.428571 0 2175.451962 Tm 6.319444 0 Td 61.574074 Tz (IBF ) Tj 2.158333 0 Td 57.118056 Tz (\(complex ) Tj 2.994444 0 Td 50.231481 Tz (3\) ) Tj 0.875 0 Td 59.41358 Tz (and ) Tj 1.497222 0 Td 72.453704 Tz (Co\(DPA-ABpy\)PF ) Tj 7.136111 0 Td 57.523148 Tz (\(complex ) Tj 51.428571 0 0 51.428571 0 2133.584071 Tm 6.261111 0 Td 43.209877 Tz (4\), ) Tj 1.030556 0 Td 46.367521 Tz (respectively. ) Tj 51.428571 0 0 51.428571 0 2091.30821 Tm 6.980556 0 Td 56.388889 Tz (X-ray ) Tj 2.041667 0 Td 45.694444 Tz (structural ) Tj 3.072222 0 Td 48.611111 Tz (analysis ) Tj 2.683333 0 Td 56.712963 Tz (of ) Tj 0.952778 0 Td 56.893004 Tz (complexes ) Tj 3.441667 0 Td 59.259259 Tz (complex ) Tj 2.819444 0 Td 55.092593 Tz (3 ) Tj 0.661111 0 Td 61.574074 Tz (and ) Tj 51.428571 0 0 51.428571 0 2047.116883 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.897222 0 Td 55.092593 Tz (4 ) Tj 0.680556 0 Td 55.092593 Tz (confirmed ) Tj 3.325 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 50.771605 Tz (coordination ) Tj 4.005556 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 69.270833 Tz (DPA-ABpy ) Tj 3.694444 0 Td 46.990741 Tz (to ) Tj 51.428571 0 0 51.428571 0 2005.901863 Tm 6.261111 0 Td 53.796296 Tz (metal ) Tj 1.827778 0 Td 49.074074 Tz (centers ) Tj 2.294444 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 51.58179 Tz (pentadentate ) Tj 3.927778 0 Td 46.759259 Tz (ligand. ) Tj 2.236111 0 Td 58.981481 Tz (While ) Tj 2.002778 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 57.118056 Tz (Nicenter ) Tj 51.428571 0 0 51.428571 0 1964.070932 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 59.259259 Tz (complex ) Tj 2.819444 0 Td 55.092593 Tz (3 ) Tj 0.680556 0 Td 40.509259 Tz (is ) Tj 0.816667 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 55.092593 Tz (an ) Tj 1.030556 0 Td 49.907407 Tz (octahedral ) Tj 3.325 0 Td 53.292181 Tz (geometry, ) Tj 3.247222 0 Td 51.851852 Tz (with ) Tj 1.594444 0 Td 49.691358 Tz (the ) Tj 1.244444 0 Td 50.771605 Tz (6th ) Tj 51.428571 0 0 51.428571 0 1923.087719 Tm 6.261111 0 Td 50.771605 Tz (ligand ) Tj 2.022222 0 Td 54.444444 Tz (being ) Tj 1.827778 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 50.462963 Tz (solvent ) Tj 2.333333 0 Td 50.555556 Tz (molecular, ) Tj 3.266667 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 68.055556 Tz (Co ) Tj 1.088889 0 Td 49.691358 Tz (center ) Tj 1.983333 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 60.185185 Tz (complex ) Tj 51.428571 0 0 51.428571 0 1883.2873 Tm 6.261111 0 Td 61.574074 Tz (4 ) Tj 0.544444 0 Td 52.932099 Tz (adopts ) Tj 2.1 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 47.395833 Tz (triganol ) Tj 2.469444 0 Td 53.030303 Tz (bipyramidal ) Tj 3.694444 0 Td 57.118056 Tz (geometry ) Tj 2.936111 0 Td 49.421296 Tz (\(see ) Tj 1.380556 0 Td 55.092593 Tz (FIG. ) Tj 1.536111 0 Td 58.333333 Tz (18a ) Tj 1.263889 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 1836 Tm 6.280556 0 Td 55.092593 Tz (FIG. ) Tj 1.613889 0 Td 48.611111 Tz (18b\). ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 51.428571 0 0 51.428571 0 1764.04 Tm 13.416667 0 Td 61.111111 Tz (Example ) Tj 2.780556 0 Td 58.333333 Tz (3 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 51.428571 0 0 51.428571 0 1682 Tm 13.3 0 Td 47.260802 Tz (Electrolysis ) Tj 51.428571 0 0 51.428571 0 1593.308901 Tm 7 0 Td 61.574074 Tz (To ) Tj 0.972222 0 Td 50.636574 Tz (evaluate ) Tj 2.644444 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 49.537037 Tz (current ) Tj 2.294444 0 Td 46.666667 Tz (efficiency ) Tj 3.033333 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 87.5 Tz (H ) Tj 0.991667 0 Td 50.673401 Tz (production, ) Tj 3.577778 0 Td 55.092593 Tz (bulk ) Tj 51.428571 0 0 51.428571 0 1552.785166 Tm 6.261111 0 Td 45.910494 Tz (electrolysis ) Tj 3.558333 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 47.530864 Tz (1.0 ) Tj 1.088889 0 Td 103.703704 Tz (M ) Tj 0.855556 0 Td 55.092593 Tz (phosphate ) Tj 3.188889 0 Td 49.151235 Tz (buffer ) Tj 1.983333 0 Td 45.37037 Tz (at ) Tj 0.738889 0 Td 76.157407 Tz (pH ) Tj 1.166667 0 Td 55.092593 Tz (7 ) Tj 0.583333 0 Td 62.654321 Tz (was ) Tj 1.361111 0 Td 49.074074 Tz (carried ) Tj 51.428571 0 0 51.428571 0 1511.366337 Tm 6.261111 0 Td 52.932099 Tz (out ) Tj 1.147222 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 53.06713 Tz (presence ) Tj 2.722222 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 60.185185 Tz (complex ) Tj 2.702778 0 Td 58.333333 Tz (2 ) Tj 0.583333 0 Td 55.092593 Tz (under ) Tj 1.827778 0 Td 62.384259 Tz (room ) Tj 1.691667 0 Td 53.030303 Tz (temperature ) Tj 3.675 0 Td 45.37037 Tz (at ) Tj 51.428571 0 0 51.428571 0 1467.730238 Tm 6.261111 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 47.170782 Tz (potential ) Tj 2.702778 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 53.472222 Tz (-1.4 ) Tj 1.458333 0 Td 81.018519 Tz (V ) Tj 0.661111 0 Td 48.611111 Tz (\(vs ) Tj 1.069444 0 Td 58.333333 Tz (SHE\). ) Tj 1.925 0 Td 61.574074 Tz (The ) Tj 1.263889 0 Td 59.259259 Tz (amounts ) Tj 2.663889 0 Td 55.092593 Tz (of ) Tj 0.797222 0 Td 87.5 Tz (H ) Tj 0.933333 0 Td 57.118056 Tz (produced ) Tj 51.428571 0 0 51.428571 0 1429.425178 Tm 6.261111 0 Td 52.932099 Tz (during ) Tj 2.041667 0 Td 46.180556 Tz (electrolysis ) Tj 3.5 0 Td 51.851852 Tz (or ) Tj 0.738889 0 Td 49.537037 Tz (photocatalysis ) Tj 4.355556 0 Td 58.333333 Tz (were ) Tj 1.575 0 Td 54.12037 Tz (determined ) Tj 3.402778 0 Td 59.953704 Tz (by ) Tj 0.855556 0 Td 55.092593 Tz (gas ) Tj 51.428571 0 0 51.428571 0 1385.307206 Tm 6.261111 0 Td 56.712963 Tz (chromatography ) Tj 5.016667 0 Td 53.148148 Tz (using ) Tj 1.827778 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 76.157407 Tz (HP ) Tj 1.127778 0 Td 59.953704 Tz (5890 ) Tj 1.711111 0 Td 45.37037 Tz (series ) Tj 1.925 0 Td 37.268519 Tz (II ) Tj 0.7 0 Td 62.654321 Tz (Gas ) Tj 1.380556 0 Td 65.625 Tz (Chromato ) Tj 58.571429 0 0 58.571429 0 1341.934783 Tm 5.497561 0 Td 48.943089 Tz (graph ) Tj 1.604878 0 Td 46.95122 Tz (with ) Tj 1.297561 0 Td 48.373984 Tz (a ) Tj 0.392683 0 Td 73.03523 Tz (TCD ) Tj 1.468293 0 Td 43.394309 Tz (detector ) Tj 2.219512 0 Td 47.804878 Tz (\(Molecular ) Tj 2.987805 0 Td 43.821138 Tz (sieve ) Tj 1.468293 0 Td 78.252033 Tz (5A ) Tj 1.058537 0 Td 51.626016 Tz (column\) ) Tj 2.304878 0 Td 46.95122 Tz (or ) Tj 51.428571 0 0 51.428571 0 1303.201739 Tm 6.261111 0 Td 58.333333 Tz (measured ) Tj 3.052778 0 Td 50 Tz (volumetrically ) Tj 4.452778 0 Td 59.953704 Tz (by ) Tj 0.972222 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 52.932099 Tz (gas ) Tj 1.205556 0 Td 45.37037 Tz (burette. ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 51.428571 0 0 51.428571 0 2969 Tm 33.444444 0 Td 79.398148 Tz (24 ) Tj 51.428571 0 0 51.428571 0 2919.620335 Tm 25.219444 0 Td 52.932099 Tz (Suggested ) Tj 3.130556 0 Td 46.990741 Tz (that ) Tj 1.438889 0 Td 59.259259 Tz (complex ) Tj 2.8 0 Td 55.092593 Tz (2 ) Tj 0.661111 0 Td 38.888889 Tz (is ) Tj 0.777778 0 Td 53.240741 Tz (capable ) Tj 2.547222 0 Td 56.712963 Tz (of ) Tj 0.894444 0 Td 49.907407 Tz (catalyzing ) Tj 3.286111 0 Td 53.472222 Tz (proton ) Tj 52.857143 0 0 52.857143 0 2869 Tm 24.5 0 Td 50.1001 Tz (reduction ) Tj 2.913514 0 Td 45.720721 Tz (to ) Tj 0.813514 0 Td 58.333333 Tz (H, ) Tj 0.983784 0 Td 55.968468 Tz (from ) Tj 1.589189 0 Td 46.846847 Tz (neutral ) Tj 2.175676 0 Td 47.297297 Tz (water. ) Tj 51.428571 0 0 51.428571 0 2795.04 Tm 32.355556 0 Td 61.111111 Tz (Example ) Tj 2.8 0 Td 58.333333 Tz (4 ) Tj 51.428571 0 0 51.428571 0 2704.444444 Tm 29.438889 0 Td 52.777778 Tz (Control ) Tj 2.488889 0 Td 47.530864 Tz (Potential ) Tj 2.858333 0 Td 54.79798 Tz (Experiments ) Tj 51.428571 0 0 51.428571 0 2617.541333 Tm 25.919444 0 Td 63.194444 Tz (To ) Tj 1.069444 0 Td 54.012346 Tz (determine ) Tj 3.227778 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 49.109687 Tz (overpotential ) Tj 4.141667 0 Td 49.691358 Tz (for ) Tj 1.147222 0 Td 52.932099 Tz (proton ) Tj 2.255556 0 Td 49.691358 Tz (reduction ) Tj 3.013889 0 Td 59.953704 Tz (by ) Tj 51.428571 0 0 51.428571 0 2576.313131 Tm 25.2 0 Td 59.259259 Tz (complex ) Tj 2.780556 0 Td 45.37037 Tz (2, ) Tj 0.836111 0 Td 48.148148 Tz (control ) Tj 2.313889 0 Td 47.530864 Tz (potential ) Tj 2.858333 0 Td 53.619529 Tz (experiments ) Tj 3.85 0 Td 51.851852 Tz (using ) Tj 1.827778 0 Td 56.712963 Tz (an ) Tj 1.011111 0 Td 55.632716 Tz (H-type ) Tj 51.428571 0 0 51.428571 0 2529.878825 Tm 25.2 0 Td 50.987654 Tz (electrochemical ) Tj 4.919444 0 Td 42.12963 Tz (cell ) Tj 1.341667 0 Td 59.953704 Tz (were ) Tj 1.730556 0 Td 52.824074 Tz (performed. ) Tj 3.5 0 Td 52.175926 Tz (Controlled ) Tj 3.422222 0 Td 47.170782 Tz (potential ) Tj 51.428571 0 0 51.428571 0 2486.45917 Tm 25.2 0 Td 45.910494 Tz (electrolysis ) Tj 3.713889 0 Td 61.574074 Tz (was ) Tj 1.536111 0 Td 55.452675 Tz (conducted ) Tj 3.383333 0 Td 46.990741 Tz (in ) Tj 1.05 0 Td 46.450617 Tz (1.0 ) Tj 1.263889 0 Td 103.703704 Tz (M ) Tj 1.030556 0 Td 58.873457 Tz (sodium ) Tj 2.508333 0 Td 55.092593 Tz (phosphate ) Tj 51.428571 0 0 51.428571 0 2443.772105 Tm 25.180556 0 Td 49.151235 Tz (buffer ) Tj 1.925 0 Td 45.37037 Tz (at ) Tj 0.719444 0 Td 72.916667 Tz (pH ) Tj 1.088889 0 Td 55.092593 Tz (7 ) Tj 0.544444 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 58.333333 Tz (an ) Tj 0.933333 0 Td 55.092593 Tz (H-type ) Tj 2.138889 0 Td 48.251029 Tz (gas-tight ) Tj 2.761111 0 Td 51.041667 Tz (dual ) Tj 1.419444 0 Td 58.333333 Tz (compartment ) Tj 4.025 0 Td 40.185185 Tz (cell. ) Tj 57.142857 0 0 57.142857 0 2398.007926 Tm 22.6625 0 Td 81.666667 Tz (A ) Tj 0.665 0 Td 51.25 Tz (mercury ) Tj 2.345 0 Td 48.854167 Tz (pool ) Tj 1.365 0 Td 48.125 Tz (with ) Tj 1.3475 0 Td 49.583333 Tz (a ) Tj 0.5075 0 Td 45 Tz (surface ) Tj 2.0475 0 Td 45.208333 Tz (area ) Tj 1.295 0 Td 55.416667 Tz (of ) Tj 0.7525 0 Td 44.722222 Tz (4.9 ) Tj 1.015 0 Td 65.625 Tz (cm ) Tj 1.26 0 Td 55.416667 Tz (was ) Tj 1.19 0 Td 50.3125 Tz (used ) Tj 1.4 0 Td 45.208333 Tz (as ) Tj 51.428571 0 0 51.428571 0 2355.788945 Tm 25.180556 0 Td 58.333333 Tz (working ) Tj 2.741667 0 Td 49.331276 Tz (electrode ) Tj 2.936111 0 Td 46.180556 Tz (that ) Tj 1.4 0 Td 61.574074 Tz (was ) Tj 1.438889 0 Td 54.372428 Tz (connected ) Tj 3.188889 0 Td 54.166667 Tz (through ) Tj 2.586111 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 54.282407 Tz (platinum ) Tj 51.428571 0 0 51.428571 0 2310.951553 Tm 25.180556 0 Td 55.092593 Tz (wire ) Tj 1.497222 0 Td 52.932099 Tz (placed ) Tj 2.080556 0 Td 46.990741 Tz (at ) Tj 0.758333 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 56.712963 Tz (bottom ) Tj 2.255556 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 56.944444 Tz (mercury ) Tj 2.547222 0 Td 49.259259 Tz (pool. ) Tj 1.672222 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 49.016204 Tz (solution ) Tj 51.428571 0 0 51.428571 0 2270.05314 Tm 25.180556 0 Td 63.734568 Tz (was ) Tj 1.380556 0 Td 43.981481 Tz (stirred ) Tj 2.080556 0 Td 49.259259 Tz (constantly ) Tj 3.208333 0 Td 52.391975 Tz (during ) Tj 2.119444 0 Td 48.935185 Tz (controlled ) Tj 3.15 0 Td 46.8107 Tz (potential ) Tj 2.741667 0 Td 51.851852 Tz (electroly ) Tj 51.428571 0 0 51.428571 0 2227.678261 Tm 25.219444 0 Td 41.049383 Tz (sis ) Tj 0.972222 0 Td 51.851852 Tz (experiments. ) Tj 51.428571 0 0 51.428571 0 2180.731932 Tm 25.919444 0 Td 87.5 Tz (A ) Tj 0.719444 0 Td 53.877315 Tz (platinum ) Tj 2.838889 0 Td 57.685185 Tz (gauze ) Tj 1.983333 0 Td 47.962963 Tz (wire, ) Tj 1.711111 0 Td 55.092593 Tz (used ) Tj 1.555556 0 Td 51.851852 Tz (as ) Tj 0.855556 0 Td 47.890947 Tz (auxiliary ) Tj 2.838889 0 Td 47.638889 Tz (electrode, ) Tj 3.111111 0 Td 62.654321 Tz (was ) Tj 51.428571 0 0 51.428571 0 2138.162762 Tm 25.2 0 Td 52.932099 Tz (placed ) Tj 2.119444 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 49.907407 Tz (other ) Tj 1.672222 0 Td 58.333333 Tz (compartment ) Tj 4.044444 0 Td 45.37037 Tz (partition ) Tj 2.702778 0 Td 56.712963 Tz (from ) Tj 1.594444 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 49.016204 Tz (Solution ) Tj 51.428571 0 0 51.428571 0 2093.843137 Tm 25.2 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 57.87037 Tz (working ) Tj 2.663889 0 Td 47.638889 Tz (electrode. ) Tj 3.091667 0 Td 60.648148 Tz (Aqueous ) Tj 2.780556 0 Td 62.962963 Tz (Ag/AgCl ) Tj 2.897222 0 Td 49.691358 Tz (electrode ) Tj 2.936111 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 2050.577114 Tm 25.180556 0 Td 56.712963 Tz (used ) Tj 1.594444 0 Td 48.611111 Tz (as ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 50.411523 Tz (reference ) Tj 2.916667 0 Td 47.314815 Tz (electrode. ) Tj 3.111111 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 57.87037 Tz (working ) Tj 2.644444 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 48.251029 Tz (auxiliary ) Tj 51.428571 0 0 51.428571 0 2010.657993 Tm 25.2 0 Td 56.983025 Tz (compartments ) Tj 4.375 0 Td 53.472222 Tz (both ) Tj 1.555556 0 Td 52.572016 Tz (contained ) Tj 3.111111 0 Td 51.851852 Tz (22.5 ) Tj 1.536111 0 Td 82.638889 Tz (mL ) Tj 1.225 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 46.548822 Tz (electrolyte ) Tj 3.344444 0 Td 59.953704 Tz (solu ) Tj 51.428571 0 0 51.428571 0 1969.562738 Tm 25.180556 0 Td 44.074074 Tz (tion, ) Tj 1.613889 0 Td 58.333333 Tz (which ) Tj 2.022222 0 Td 59.953704 Tz (were ) Tj 1.691667 0 Td 52.824074 Tz (thoroughly ) Tj 3.461111 0 Td 54.6875 Tz (degassed ) Tj 2.897222 0 Td 58.333333 Tz (by ) Tj 0.991667 0 Td 53.703704 Tz (purging ) Tj 2.508333 0 Td 53.472222 Tz (with ) Tj 1.536111 0 Td 66.435185 Tz (Ar ) Tj 51.428571 0 0 51.428571 0 1928.064118 Tm 25.2 0 Td 49.691358 Tz (for ) Tj 1.030556 0 Td 63.194444 Tz (30 ) Tj 0.952778 0 Td 60.493827 Tz (min ) Tj 1.263889 0 Td 49.259259 Tz (prior ) Tj 1.633333 0 Td 45.37037 Tz (to ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 51.58179 Tz (experiments. ) Tj 3.966667 0 Td 51.041667 Tz (Faradaic ) Tj 2.644444 0 Td 46.990741 Tz (efficiency ) Tj 3.033333 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 1885.667906 Tm 25.2 0 Td 54.768519 Tz (determined ) Tj 3.441667 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 61.574074 Tz (50 ) Tj 0.952778 0 Td 77.777778 Tz (uM ) Tj 1.127778 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 55.092593 Tz (2 ) Tj 0.505556 0 Td 45.37037 Tz (at ) Tj 0.719444 0 Td 56.712963 Tz (an ) Tj 0.855556 0 Td 51.388889 Tz (applied ) Tj 2.333333 0 Td 46.8107 Tz (potential ) Tj 2.722222 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1844.435768 Tm 25.219444 0 Td 52.662037 Tz (-1.3 ) Tj 1.497222 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 53.472222 Tz (-1.4 ) Tj 1.536111 0 Td 81.018519 Tz (V ) Tj 0.719444 0 Td 51.851852 Tz (vs ) Tj 0.875 0 Td 63.194444 Tz (SHE. ) Tj 1.75 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 53.914141 Tz (experiments ) Tj 3.791667 0 Td 59.143519 Tz (were ) Tj 1.613889 0 Td 56.893004 Tz (performed ) Tj 51.428571 0 0 51.428571 0 1801.248996 Tm 25.2 0 Td 45.37037 Tz (at ) Tj 0.816667 0 Td 54.012346 Tz (22 ) Tj 1.283333 0 Td 51.851852 Tz (C. ) Tj 0.933333 0 Td 58.333333 Tz (and ) Tj 1.322222 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 54.444444 Tz (vapor ) Tj 1.866667 0 Td 51.041667 Tz (pressure ) Tj 2.722222 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 55.092593 Tz (water ) Tj 1.886111 0 Td 45.37037 Tz (at ) Tj 0.797222 0 Td 64.814815 Tz (22C. ) Tj 2.236111 0 Td 49.907407 Tz (\(19.8 ) Tj 51.428571 0 0 51.428571 0 1761.062127 Tm 25.2 0 Td 75.185185 Tz (mmHg\) ) Tj 2.430556 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 50.411523 Tz (corrected ) Tj 2.877778 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 48.316498 Tz (calculating ) Tj 3.325 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 49.537037 Tz (current ) Tj 2.197222 0 Td 46.990741 Tz (efficiency ) Tj 3.013889 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 1722.608696 Tm 25.219444 0 Td 58.333333 Tz (He ) Tj 0.952778 0 Td 50.378788 Tz (production. ) Tj 51.428571 0 0 51.428571 0 1677.772358 Tm 25.938889 0 Td 55.092593 Tz (FIG. ) Tj 1.633333 0 Td 61.574074 Tz (8 ) Tj 0.661111 0 Td 49.016204 Tz (displays ) Tj 2.683333 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 54.552469 Tz (charge ) Tj 2.255556 0 Td 51.041667 Tz (build-up ) Tj 2.761111 0 Td 55.092593 Tz (over ) Tj 1.594444 0 Td 53.240741 Tz (200-sec ) Tj 2.527778 0 Td 59.953704 Tz (elec ) Tj 52.857143 0 0 52.857143 0 1636.052356 Tm 24.5 0 Td 43.75 Tz (trolysis ) Tj 2.327027 0 Td 44.144144 Tz (at ) Tj 0.756757 0 Td 48.348348 Tz (varied ) Tj 1.967568 0 Td 46.036036 Tz (potentials ) Tj 2.989189 0 Td 47.297297 Tz (for ) Tj 1.078378 0 Td 58.333333 Tz (50 ) Tj 0.945946 0 Td 78.828829 Tz (uM ) Tj 1.154054 0 Td 58.558559 Tz (complex ) Tj 2.686486 0 Td 56.756757 Tz (2 ) Tj 0.586486 0 Td 45.720721 Tz (in ) Tj 0.813514 0 Td 47.297297 Tz (1.0 ) Tj 1.097297 0 Td 104.054054 Tz (M ) Tj 51.428571 0 0 51.428571 0 1594.86443 Tm 25.2 0 Td 54.73251 Tz (phosphate ) Tj 3.266667 0 Td 49.151235 Tz (buffer ) Tj 2.061111 0 Td 45.37037 Tz (at ) Tj 0.875 0 Td 72.916667 Tz (pH ) Tj 1.205556 0 Td 43.75 Tz (7. ) Tj 0.875 0 Td 56.388889 Tz (There ) Tj 2.041667 0 Td 37.268519 Tz (is ) Tj 0.816667 0 Td 58.333333 Tz (no ) Tj 1.05 0 Td 45.959596 Tz (significant ) Tj 3.344444 0 Td 54.012346 Tz (charge ) Tj 51.428571 0 0 51.428571 0 1553.296296 Tm 25.2 0 Td 56.860269 Tz (consumption ) Tj 4.161111 0 Td 48.611111 Tz (for ) Tj 1.205556 0 Td 49.305556 Tz (overpotentials ) Tj 4.530556 0 Td 58.981481 Tz (below ) Tj 2.197222 0 Td 54.444444 Tz (-0.55 ) Tj 2.041667 0 Td 48.611111 Tz (V, ) Tj 0.991667 0 Td 58.333333 Tz (and ) Tj 1.438889 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1510.437262 Tm 25.2 0 Td 45.37037 Tz (catalytic ) Tj 2.741667 0 Td 49.074074 Tz (current ) Tj 2.313889 0 Td 48.611111 Tz (for ) Tj 1.088889 0 Td 52.391975 Tz (proton ) Tj 2.158333 0 Td 50.771605 Tz (reduction ) Tj 3.033333 0 Td 51.851852 Tz (occurs ) Tj 2.138889 0 Td 43.75 Tz (at ) Tj 0.777778 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 62.654321 Tz (overpo ) Tj 60 0 0 60 0 1465 Tm 21.583333 0 Td 37.301587 Tz (tential ) Tj 1.833333 0 Td 50 Tz (of ) Tj 0.816667 0 Td 47.777778 Tz (-0.60 ) Tj 1.7 0 Td 69.444444 Tz (V ) Tj 0.7 0 Td 43.518519 Tz (\(-1.01 ) Tj 1.916667 0 Td 69.444444 Tz (V ) Tj 0.7 0 Td 44.444444 Tz (vs ) Tj 0.816667 0 Td 50.555556 Tz (SHE\), ) Tj 1.816667 0 Td 42.777778 Tz (close ) Tj 1.566667 0 Td 37.5 Tz (to ) Tj 0.75 0 Td 41.666667 Tz (the ) Tj 1.016667 0 Td 72.222222 Tz (Co' ) Tj 51.428571 0 0 51.428571 0 1426.112 Tm 25.2 0 Td 53.472222 Tz (couple ) Tj 2.158333 0 Td 46.990741 Tz (at ) Tj 0.816667 0 Td 54.444444 Tz (-0.90 ) Tj 1.866667 0 Td 87.5 Tz (V ) Tj 0.777778 0 Td 47.530864 Tz (\(vs ) Tj 1.108333 0 Td 59.62963 Tz (SHE\). ) Tj 51.428571 0 0 51.428571 0 1384.412518 Tm 25.938889 0 Td 57.253086 Tz (For ) Tj 1.283333 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 58.333333 Tz (2 ) Tj 0.641667 0 Td 45.37037 Tz (in ) Tj 0.855556 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 53.796296 Tz (range ) Tj 1.886111 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 61.574074 Tz (50 ) Tj 1.030556 0 Td 62.384259 Tz (uM-1 ) Tj 1.866667 0 Td 76.697531 Tz (mM, ) Tj 1.633333 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 50 Tz (current ) Tj 52.857143 0 0 52.857143 0 1341.415233 Tm 24.518919 0 Td 45.405405 Tz (efficiency ) Tj 2.894595 0 Td 56.756757 Tz (of ) Tj 0.775676 0 Td 66.846847 Tz (99+1% ) Tj 2.194595 0 Td 49.399399 Tz (\(Table ) Tj 1.92973 0 Td 50.45045 Tz (2\) ) Tj 0.737838 0 Td 62.012012 Tz (was ) Tj 1.267568 0 Td 50.844595 Tz (obtained ) Tj 2.610811 0 Td 45.195195 Tz (for ) Tj 1.021622 0 Td 45.720721 Tz (H. ) Tj 0.889189 0 Td 49.74975 Tz (evolution ) Tj 51.428571 0 0 51.428571 0 1300.642857 Tm 25.2 0 Td 43.75 Tz (at ) Tj 0.758333 0 Td 74.537037 Tz (pH ) Tj 1.166667 0 Td 55.092593 Tz (7 ) Tj 0.583333 0 Td 51.311728 Tz (\(Table ) Tj 2.080556 0 Td 42.12963 Tz (2\). ) Tj 38.571429 0 0 38.571429 0 1236 Tm 40.625926 0 Td 101.111111 Tz (TABLE ) Tj 3.396296 0 Td 73.45679 Tz (2 ) Tj 40 0 0 40 0 1168.365169 Tm 31.175 0 Td 54.861111 Tz (Experimental ) Tj 4.225 0 Td 44.047619 Tz (results ) Tj 2.1 0 Td 58.333333 Tz (from ) Tj 1.7 0 Td 47.5 Tz (controlled-potential ) Tj 5.95 0 Td 45.833333 Tz (electrolysis ) Tj 3.575 0 Td 58.333333 Tz (on ) Tj 0.95 0 Td 58.333333 Tz (2 ) Tj 0.625 0 Td 45.833333 Tz (in ) Tj 41.428571 0 0 41.428571 0 1132.90566 Tm 35.217241 0 Td 60.344828 Tz (1.OM ) Tj 1.665517 0 Td 53.639847 Tz (phosphate ) Tj 3.113793 0 Td 46.934866 Tz (buffer ) Tj 1.882759 0 Td 42.241379 Tz (at ) Tj 0.748276 0 Td 68.390805 Tz (pH ) Tj 1.110345 0 Td 26.149425 Tz (7. ) Tj 40 0 0 40 0 938.778325 Tm 27.15 0 Td 55.952381 Tz (Applied ) Tj 2.675 0 Td 45.416667 Tz (Potential, ) Tj 40 0 0 40 0 903 Tm 27.2 0 Td 60.416667 Tz (\(V ) Tj 0.95 0 Td 54.166667 Tz (vs ) Tj 0.9 0 Td 66.666667 Tz (SHE\) ) Tj 40 0 0 40 0 870 Tm 27.175 0 Td 61.979167 Tz (Coulombs ) Tj 3.25 0 Td 52.777778 Tz (\(C\) ) Tj 40 0 0 40 0 836 Tm 27.175 0 Td 55.833333 Tz (Calcd ) Tj 1.9 0 Td 63.194444 Tz (Volume ) Tj 2.55 0 Td 56.25 Tz (of ) Tj 0.925 0 Td 58.333333 Tz (H2 ) Tj 40 0 0 40 0 803 Tm 27.2 0 Td 60.416667 Tz (\(mL\) ) Tj 31.428571 0 0 31.428571 0 776 Tm 34.586364 0 Td 75.30303 Tz (Obsd ) Tj 2.545455 0 Td 79.545455 Tz (Volume ) Tj 40 0 0 40 0 740.632653 Tm 27.175 0 Td 61.805556 Tz (Change ) Tj 2.5 0 Td 60.416667 Tz (\(mL\) ) Tj 40 0 0 40 0 704.92 Tm 27.175 0 Td 58.333333 Tz (Expt ) Tj 1.65 0 Td 58.333333 Tz (H. ) Tj 0.975 0 Td 63.194444 Tz (Volume ) Tj 40 0 0 40 0 670 Tm 27.2 0 Td 60.416667 Tz (\(mL\) ) Tj 40 0 0 40 0 640.403846 Tm 27.175 0 Td 53.571429 Tz (Current ) Tj 2.5 0 Td 49.166667 Tz (Efficiency ) Tj 40 0 0 40 0 604 Tm 27.2 0 Td 58.333333 Tz (\(%\) ) Tj 51.428571 0 0 51.428571 0 466.222506 Tm 7 0 Td 72.106481 Tz (When ) Tj 2.002778 0 Td 56.944444 Tz (mercury ) Tj 2.644444 0 Td 54.282407 Tz (pool ) Tj 1.575 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 55.902778 Tz (used ) Tj 1.575 0 Td 50.231481 Tz (as ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 57.87037 Tz (working ) Tj 2.663889 0 Td 47.638889 Tz (electrode, ) Tj 3.325 0 Td 45.37037 Tz (60 ) Tj 51.428571 0 0 51.428571 0 424.525935 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 48.611111 Tz (cyclic ) Tj 1.963889 0 Td 61.033951 Tz (voltammogram ) Tj 4.588889 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 47.530864 Tz (1.0 ) Tj 1.011111 0 Td 106.944444 Tz (M ) Tj 0.836111 0 Td 58.333333 Tz (sodium ) Tj 2.294444 0 Td 55.092593 Tz (phosphate ) Tj 3.130556 0 Td 49.151235 Tz (buffer ) Tj 51.428571 0 0 51.428571 0 379.687417 Tm 6.261111 0 Td 45.37037 Tz (at ) Tj 0.836111 0 Td 74.537037 Tz (pH ) Tj 1.205556 0 Td 58.333333 Tz (7 ) Tj 0.680556 0 Td 61.574074 Tz (showed ) Tj 2.566667 0 Td 55.092593 Tz (no ) Tj 0.991667 0 Td 45.959596 Tz (significant ) Tj 3.344444 0 Td 49.537037 Tz (current ) Tj 2.352778 0 Td 46.990741 Tz (at ) Tj 0.836111 0 Td 47.314815 Tz (potentials ) Tj 3.169444 0 Td 62.384259 Tz (more ) Tj 51.428571 0 0 51.428571 0 336.335188 Tm 6.241667 0 Td 48.611111 Tz (positive ) Tj 2.663889 0 Td 51.851852 Tz (than ) Tj 1.594444 0 Td 55.092593 Tz (-1.6 ) Tj 1.633333 0 Td 87.5 Tz (V ) Tj 0.855556 0 Td 53.472222 Tz (vs ) Tj 0.991667 0 Td 76.697531 Tz (SHE ) Tj 1.730556 0 Td 51.851852 Tz (\(FIG. ) Tj 1.925 0 Td 43.209877 Tz (7\). ) Tj 1.166667 0 Td 57.523148 Tz (However, ) Tj 3.130556 0 Td 46.990741 Tz (in ) Tj 0.933333 0 Td 48.611111 Tz (the ) Tj 51.428571 0 0 51.428571 0 297.78825 Tm 6.261111 0 Td 53.06713 Tz (presence ) Tj 2.741667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 59.722222 Tz (complex ) Tj 2.683333 0 Td 43.75 Tz (2, ) Tj 0.719444 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 50.231481 Tz (strong ) Tj 1.963889 0 Td 49.537037 Tz (current ) Tj 2.236111 0 Td 55.092593 Tz (appeared ) Tj 2.780556 0 Td 46.990741 Tz (at ) Tj 0.719444 0 Td 55.740741 Tz (-1.20 ) Tj 1.847222 0 Td 87.5 Tz (V ) Tj 51.428571 0 0 51.428571 0 251.475728 Tm 6.261111 0 Td 53.472222 Tz (vs ) Tj 0.836111 0 Td 75.617284 Tz (SHE ) Tj 1.536111 0 Td 54.503367 Tz (concomitant ) Tj 3.752778 0 Td 53.472222 Tz (with ) Tj 1.477778 0 Td 52.932099 Tz (gas ) Tj 1.127778 0 Td 54.166667 Tz (bubbles ) Tj 2.430556 0 Td 50.87963 Tz (formation, ) Tj 3.247222 0 Td 58.333333 Tz (which ) Tj 1.944444 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 212.926342 Tm 6.261111 0 Td 54.73251 Tz (confirmed ) Tj 3.15 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 58.333333 Tz (be ) Tj 0.913889 0 Td 87.5 Tz (H ) Tj 0.972222 0 Td 61.574074 Tz (by ) Tj 0.952778 0 Td 75.07716 Tz (GC-TCD ) Tj 2.897222 0 Td 49.016204 Tz (analysis ) Tj 2.586111 0 Td 62.037037 Tz (\(GC-gas ) Tj 2.8 0 Td 67.515432 Tz (chroma ) Tj 51.428571 0 0 51.428571 0 172.014688 Tm 6.241667 0 Td 50.771605 Tz (tography, ) Tj 3.052778 0 Td 61.574074 Tz (TCD=thermal ) Tj 4.375 0 Td 50.501543 Tz (conductivity ) Tj 3.986111 0 Td 45.37037 Tz (detector\). ) Tj 3.052778 0 Td 62.654321 Tz (The ) Tj 1.438889 0 Td 53.148148 Tz (study ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 41.428571 0 0 41.428571 0 1065.868132 Tm 40.47931 0 Td 58.333333 Tz (Sample ) Tj 2.341379 0 Td 63.697318 Tz (Number ) Tj 30 0 0 30 0 1004 Tm 46.266667 0 Td 55.555556 Tz (1 ) Tj 2.866667 0 Td 77.777778 Tz (2 ) Tj 2.9 0 Td 72.222222 Tz (3 ) Tj 2.866667 0 Td 88.888889 Tz (4 ) Tj 3.433333 0 Td 72.222222 Tz (5 ) Tj 3.933333 0 Td 72.222222 Tz (6 ) Tj 3.333333 0 Td 77.777778 Tz (7 ) Tj 2.966667 0 Td 72.222222 Tz (8 ) Tj 2.866667 0 Td 77.777778 Tz (9 ) Tj 30 0 0 30 0 942 Tm 45.333333 0 Td 93.055556 Tz (-140 ) Tj 2.933333 0 Td 73.333333 Tz (-1.40 ) Tj 2.9 0 Td 73.333333 Tz (-1.40 ) Tj 2.9 0 Td 73.333333 Tz (-1.40 ) Tj 3.633333 0 Td 73.333333 Tz (-1.40 ) Tj 3.866667 0 Td 73.333333 Tz (-1.30 ) Tj 3.166667 0 Td 74.444444 Tz (-1.30 ) Tj 2.933333 0 Td 73.333333 Tz (-1.30 ) Tj 2.9 0 Td 73.333333 Tz (-1.30 ) Tj 30 0 0 30 0 876 Tm 45.4 0 Td 92.592593 Tz (222 ) Tj 2.9 0 Td 66.666667 Tz (22.1 ) Tj 2.933333 0 Td 69.444444 Tz (28.0 ) Tj 2.9 0 Td 69.444444 Tz (28.2 ) Tj 3.633333 0 Td 68.055556 Tz (63.6 ) Tj 3.833333 0 Td 69.444444 Tz (20.3 ) Tj 3.233333 0 Td 68.055556 Tz (24.O ) Tj 2.866667 0 Td 88.888889 Tz (311 ) Tj 2.9 0 Td 72.222222 Tz (42.4 ) Tj 30 0 0 30 0 842 Tm 45.866667 0 Td 70.833333 Tz (2.78 ) Tj 2.9 0 Td 70.833333 Tz (2.76 ) Tj 2.933333 0 Td 69.444444 Tz (3.49 ) Tj 2.9 0 Td 69.444444 Tz (3.52 ) Tj 3.633333 0 Td 68.055556 Tz (7.93 ) Tj 3.866667 0 Td 68.055556 Tz (2.53 ) Tj 3.166667 0 Td 69.444444 Tz (3.03 ) Tj 2.966667 0 Td 68.055556 Tz (3.87 ) Tj 2.866667 0 Td 69.444444 Tz (S.28 ) Tj 30 0 0 30 0 776 Tm 45.866667 0 Td 66.666667 Tz (2.8 ) Tj 2.9 0 Td 66.666667 Tz (2.8 ) Tj 2.933333 0 Td 64.814815 Tz (3.5 ) Tj 2.9 0 Td 66.666667 Tz (3.6 ) Tj 3.666667 0 Td 62.962963 Tz (8.2 ) Tj 3.833333 0 Td 66.666667 Tz (2.6 ) Tj 3.166667 0 Td 66.666667 Tz (3.0 ) Tj 2.933333 0 Td 64.814815 Tz (3.9 ) Tj 2.9 0 Td 64.814815 Tz (5.3 ) Tj 30 0 0 30 0 709 Tm 45.866667 0 Td 66.666667 Tz (2.7 ) Tj 2.9 0 Td 66.666667 Tz (2.7 ) Tj 2.933333 0 Td 68.518519 Tz (3.4 ) Tj 2.9 0 Td 64.814815 Tz (3.5 ) Tj 3.666667 0 Td 62.962963 Tz (8.0 ) Tj 3.833333 0 Td 64.814815 Tz (2.5 ) Tj 3.166667 0 Td 66.666667 Tz (2.9 ) Tj 2.933333 0 Td 64.814815 Tz (3.8 ) Tj 2.9 0 Td 66.666667 Tz (5.2 ) Tj 30 0 0 30 0 643 Tm 45.4 0 Td 69.444444 Tz (98.6 ) Tj 2.866667 0 Td 70.833333 Tz (98.9 ) Tj 2.9 0 Td 72.222222 Tz (97.6 ) Tj 2.933333 0 Td 70.833333 Tz (99.6 ) Tj 3.2 0 Td 70 Tz (100.7 ) Tj 3.9 0 Td 67.777778 Tz (100.1 ) Tj 3.566667 0 Td 72.222222 Tz (96.4 ) Tj 2.9 0 Td 68.055556 Tz (98.1 ) Tj 2.9 0 Td 72.222222 Tz (97.8 ) Tj 51.428571 0 0 51.428571 0 465.997494 Tm 25.919444 0 Td 72.106481 Tz (When ) Tj 1.963889 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 49.259259 Tz (controlled ) Tj 3.169444 0 Td 46.8107 Tz (potential ) Tj 2.741667 0 Td 54.768519 Tz (experiment ) Tj 3.480556 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 56.17284 Tz (conducted ) Tj 51.428571 0 0 51.428571 0 421.449057 Tm 25.2 0 Td 45.37037 Tz (at ) Tj 0.738889 0 Td 52.662037 Tz (-1.3 ) Tj 1.497222 0 Td 81.018519 Tz (V ) Tj 0.719444 0 Td 47.530864 Tz (\(vs ) Tj 1.088889 0 Td 59.62963 Tz (SHE\), ) Tj 2.002778 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 51.041667 Tz (Faradaic ) Tj 2.663889 0 Td 46.666667 Tz (efficiency ) Tj 3.033333 0 Td 61.574074 Tz (was ) Tj 1.322222 0 Td 54.768519 Tz (determined ) Tj 51.428571 0 0 51.428571 0 377.210174 Tm 25.180556 0 Td 45.37037 Tz (to ) Tj 0.855556 0 Td 56.712963 Tz (be ) Tj 0.952778 0 Td 62.654321 Tz (98+2%. ) Tj 2.527778 0 Td 72.916667 Tz (On ) Tj 1.166667 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 48.611111 Tz (basis ) Tj 1.730556 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 61.574074 Tz (consumed ) Tj 3.208333 0 Td 52.314815 Tz (charges ) Tj 2.488889 0 Td 55.092593 Tz (over ) Tj 1.613889 0 Td 38.888889 Tz (1 ) Tj 0.563889 0 Td 64.814815 Tz (h ) Tj 51.428571 0 0 51.428571 0 338.462366 Tm 25.180556 0 Td 55.092593 Tz (bulk ) Tj 1.613889 0 Td 45.640432 Tz (electrolysis ) Tj 3.577778 0 Td 46.990741 Tz (at ) Tj 0.855556 0 Td 53.472222 Tz (-1.4 ) Tj 1.594444 0 Td 81.018519 Tz (V ) Tj 0.816667 0 Td 47.530864 Tz (\(vs ) Tj 1.147222 0 Td 68.055556 Tz (SHE\) ) Tj 1.925 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 48.611111 Tz (1.0 ) Tj 1.147222 0 Td 106.944444 Tz (M ) Tj 0.913889 0 Td 55.092593 Tz (phosphate ) Tj 51.428571 0 0 51.428571 0 296.290323 Tm 25.180556 0 Td 49.151235 Tz (buffer ) Tj 1.963889 0 Td 45.37037 Tz (at ) Tj 0.758333 0 Td 72.916667 Tz (pH ) Tj 1.127778 0 Td 55.092593 Tz (7 ) Tj 0.563889 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 53.472222 Tz (presence ) Tj 2.780556 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 61.574074 Tz (50 ) Tj 0.972222 0 Td 79.398148 Tz (uM ) Tj 1.186111 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 45.37037 Tz (2, ) Tj 0.797222 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 50.231481 Tz (H. ) Tj 51.428571 0 0 51.428571 0 253.4 Tm 25.2 0 Td 50.771605 Tz (evolution ) Tj 2.936111 0 Td 44.965278 Tz (activity ) Tj 2.352778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 51.851852 Tz (2 ) Tj 0.525 0 Td 62.654321 Tz (was ) Tj 1.322222 0 Td 49.259259 Tz (calculated ) Tj 3.15 0 Td 43.75 Tz (to ) Tj 0.719444 0 Td 58.333333 Tz (be ) Tj 0.933333 0 Td 58.333333 Tz (1400 ) Tj 1.594444 0 Td 71.296296 Tz (L ) Tj 57.142857 0 0 57.142857 0 210.994012 Tm 22.68 0 Td 46.666667 Tz (H. ) Tj 1.085 0 Td 50.3125 Tz (\(mol ) Tj 1.5575 0 Td 40.833333 Tz (cat\) ) Tj 1.82 0 Td 78.75 Tz (h\(cm ) Tj 2.5375 0 Td 60.520833 Tz (Hg\)' ) Tj 1.855 0 Td 47.25 Tz (\(FIG. ) Tj 1.7325 0 Td 44.479167 Tz (9a\), ) Tj 1.4 0 Td 46.666667 Tz (or ) Tj 0.875 0 Td 49.583333 Tz (a ) Tj 0.63 0 Td 47.03125 Tz (turnover ) Tj 58.571429 0 0 58.571429 0 169.8 Tm 22.126829 0 Td 55.01355 Tz (number ) Tj 2.15122 0 Td 57.479675 Tz (\(TON\) ) Tj 1.895122 0 Td 54.065041 Tz (of ) Tj 0.75122 0 Td 55.487805 Tz (>300 ) Tj 1.502439 0 Td 55.01355 Tz (mol ) Tj 1.229268 0 Td 35.094851 Tz (H., ) Tj 0.870732 0 Td 49.796748 Tz (\(mol ) Tj 1.4 0 Td 45.054201 Tz (cat\)', ) Tj 1.826829 0 Td 45.528455 Tz (suggesting ) Tj 2.919512 0 Td 44.579946 Tz (the ) Tj 1.428571 0 0 1.428571 0 2806 Tm 502.6 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 284 0 obj << /Length 1 >> stream q endstream endobj 285 0 obj << /Length 47213 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.113514 0 Td 77.252252 Tz (25 ) Tj 51.428571 0 0 51.428571 0 2915.228856 Tm 6.261111 0 Td 55.092593 Tz (reduced ) Tj 2.527778 0 Td 57.523148 Tz (form ) Tj 1.613889 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 58.333333 Tz (2 ) Tj 0.602778 0 Td 37.268519 Tz (is ) Tj 0.661111 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 51.311728 Tz (highly ) Tj 2.061111 0 Td 43.930041 Tz (efficient ) Tj 2.547222 0 Td 51.557239 Tz (electrocata ) Tj 51.428571 0 0 51.428571 0 2872.644231 Tm 6.261111 0 Td 44.560185 Tz (lyst ) Tj 1.205556 0 Td 48.611111 Tz (for ) Tj 0.972222 0 Td 52.932099 Tz (proton ) Tj 2.080556 0 Td 50.411523 Tz (reduction ) Tj 2.897222 0 Td 45.37037 Tz (in ) Tj 0.719444 0 Td 47.685185 Tz (neutral ) Tj 2.158333 0 Td 56.481481 Tz (aqueous ) Tj 2.547222 0 Td 46.090535 Tz (solution. ) Tj 2.702778 0 Td 61.033951 Tz (FIG.9b ) Tj 51.428571 0 0 51.428571 0 2829.646326 Tm 6.261111 0 Td 48.611111 Tz (also ) Tj 1.419444 0 Td 50.636574 Tz (Suggests ) Tj 2.644444 0 Td 46.990741 Tz (that ) Tj 1.322222 0 Td 50.771605 Tz (the ) Tj 1.088889 0 Td 45.775463 Tz (activity ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 59.259259 Tz (complex ) Tj 2.702778 0 Td 58.333333 Tz (2 ) Tj 0.583333 0 Td 53.292181 Tz (decreased ) Tj 3.091667 0 Td 45.37037 Tz (after ) Tj 51.428571 0 0 51.428571 0 2786.045455 Tm 6.261111 0 Td 61.574074 Tz (more ) Tj 1.75 0 Td 51.041667 Tz (than ) Tj 1.477778 0 Td 51.851852 Tz (3 ) Tj 0.602778 0 Td 61.574074 Tz (h ) Tj 0.622222 0 Td 44.373219 Tz (electrolysis. ) Tj 52.857143 0 0 52.857143 0 2742.635007 Tm 6.810811 0 Td 46.946947 Tz (Catalytic ) Tj 2.762162 0 Td 45.720721 Tz (H. ) Tj 0.851351 0 Td 51.396396 Tz (production ) Tj 3.235135 0 Td 44.144144 Tz (at ) Tj 0.662162 0 Td 53.603604 Tz (a ) Tj 0.472973 0 Td 45.545546 Tz (potential ) Tj 2.62973 0 Td 54.234234 Tz (lower ) Tj 1.778378 0 Td 48.873874 Tz (than ) Tj 1.362162 0 Td 46.246246 Tz (the ) Tj 0.964865 0 Td 69.369369 Tz (Co ) Tj 58.571429 0 0 58.571429 0 2700.7314 Tm 5.497561 0 Td 47.899729 Tz (couple ) Tj 1.895122 0 Td 51.219512 Tz (of ) Tj 0.7 0 Td 52.439024 Tz (complex ) Tj 2.407317 0 Td 54.065041 Tz (2 ) Tj 0.529268 0 Td 46.160795 Tz (suggested ) Tj 2.697561 0 Td 39.837398 Tz (that ) Tj 1.143902 0 Td 49.322493 Tz (Co' ) Tj 1.092683 0 Td 51.930894 Tz (form ) Tj 1.45122 0 Td 49.796748 Tz (of ) Tj 0.717073 0 Td 52.439024 Tz (complex ) Tj 2.407317 0 Td 48.373984 Tz (2 ) Tj 51.428571 0 0 51.428571 0 2654.098266 Tm 6.261111 0 Td 38.888889 Tz (is ) Tj 0.758333 0 Td 50.084175 Tz (responsible ) Tj 3.538889 0 Td 48.611111 Tz (for ) Tj 1.05 0 Td 52.932099 Tz (proton ) Tj 2.197222 0 Td 50.05144 Tz (reduction ) Tj 2.975 0 Td 48.611111 Tz (\(see ) Tj 1.419444 0 Td 63.734568 Tz (Scheme ) Tj 2.547222 0 Td 41.049383 Tz (2\). ) Tj 25.714286 0 0 25.714286 0 2762 Tm 46.822222 0 Td 32.407407 Tz (s ) Tj 51.428571 0 0 51.428571 0 2577.087248 Tm 13.416667 0 Td 61.111111 Tz (Example ) Tj 2.8 0 Td 55.092593 Tz (5 ) Tj 51.428571 0 0 51.428571 0 2487.176471 Tm 10.713889 0 Td 49.305556 Tz (Photocatalytic ) Tj 4.375 0 Td 51.851852 Tz (H. ) Tj 1.05 0 Td 52.824074 Tz (Production ) Tj 52.857143 0 0 52.857143 0 2401.280657 Tm 6.810811 0 Td 47.972973 Tz (Photocatalytic ) Tj 4.237838 0 Td 45.720721 Tz (H. ) Tj 0.87027 0 Td 51.081081 Tz (production ) Tj 3.197297 0 Td 58.333333 Tz (by ) Tj 0.87027 0 Td 57.657658 Tz (complex ) Tj 2.591892 0 Td 53.603604 Tz (2 ) Tj 0.472973 0 Td 51.081081 Tz (using ) Tj 1.683784 0 Td 48.873874 Tz (ascorbic ) Tj 58.571429 0 0 58.571429 0 2356.617978 Tm 5.497561 0 Td 44.817073 Tz (acid ) Tj 1.263415 0 Td 45.528455 Tz (as ) Tj 0.768293 0 Td 43.038618 Tz (electron ) Tj 2.287805 0 Td 50.650407 Tz (donor ) Tj 1.707317 0 Td 51.219512 Tz (and ) Tj 1.365854 0 Td 57.542909 Tz (Ru\(bpy\)," ) Tj 3.312195 0 Td 44.105691 Tz (as ) Tj 0.75122 0 Td 43.441734 Tz (photosensitizer ) Tj 51.428571 0 0 51.428571 0 2312.905753 Tm 6.241667 0 Td 63.734568 Tz (was ) Tj 1.361111 0 Td 53.472222 Tz (performed. ) Tj 3.480556 0 Td 49.907407 Tz (Photolysis ) Tj 3.247222 0 Td 53.619529 Tz (experiments ) Tj 3.772222 0 Td 59.953704 Tz (were ) Tj 1.652778 0 Td 48.148148 Tz (carried ) Tj 2.255556 0 Td 51.851852 Tz (out ) Tj 1.147222 0 Td 50.231481 Tz (in ) Tj 51.428571 0 0 51.428571 0 2267.042553 Tm 6.338889 0 Td 56.712963 Tz (10 ) Tj 0.855556 0 Td 81.018519 Tz (mL ) Tj 1.166667 0 Td 48.611111 Tz (1.0 ) Tj 1.030556 0 Td 103.703704 Tz (M ) Tj 0.797222 0 Td 48.148148 Tz (acetate ) Tj 2.177778 0 Td 49.151235 Tz (buffer ) Tj 1.905556 0 Td 48.206019 Tz (solution ) Tj 2.469444 0 Td 46.990741 Tz (at ) Tj 0.719444 0 Td 72.916667 Tz (pH ) Tj 1.069444 0 Td 50.771605 Tz (4.0 ) Tj 1.030556 0 Td 51.527778 Tz (containing ) Tj 3.266667 0 Td 46.450617 Tz (0.1 ) Tj 58.571429 0 0 58.571429 0 2225.069378 Tm 5.497561 0 Td 52.168022 Tz (Mascorbic ) Tj 2.970732 0 Td 44.817073 Tz (acid ) Tj 1.195122 0 Td 52.168022 Tz (and ) Tj 1.07561 0 Td 42.682927 Tz (0.5 ) Tj 0.921951 0 Td 64.9729 Tz (mMIRu\(bpy\)". ) Tj 4.84878 0 Td 51.219512 Tz (Each ) Tj 1.4 0 Td 49.322493 Tz (sample ) Tj 1.929268 0 Td 55.01355 Tz (was ) Tj 51.428571 0 0 51.428571 0 2181.601504 Tm 6.261111 0 Td 53.06713 Tz (prepared ) Tj 2.741667 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 57.253086 Tz (130 ) Tj 1.263889 0 Td 79.398148 Tz (mL ) Tj 1.147222 0 Td 50.084175 Tz (rectangular ) Tj 3.461111 0 Td 46.666667 Tz (flask ) Tj 1.575 0 Td 51.203704 Tz (containing ) Tj 3.305556 0 Td 56.712963 Tz (10 ) Tj 0.894444 0 Td 81.018519 Tz (mL ) Tj 1.166667 0 Td 56.712963 Tz (of ) Tj 52.857143 0 0 52.857143 0 2136.418546 Tm 6.072973 0 Td 48.348348 Tz (buffer ) Tj 1.92973 0 Td 45.720721 Tz (in ) Tj 0.775676 0 Td 49.399399 Tz (the ) Tj 1.097297 0 Td 52.027027 Tz (presence ) Tj 2.743243 0 Td 55.18018 Tz (of ) Tj 1.059459 0 Td 65.900901 Tz (Ru\(bpy\)Cl. ) Tj 4.181081 0 Td 49.268018 Tz (ascorbic ) Tj 2.610811 0 Td 45.405405 Tz (acid, ) Tj 1.57027 0 Td 59.90991 Tz (and ) Tj 51.428571 0 0 51.428571 0 2093.953307 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.780556 0 Td 43.75 Tz (2. ) Tj 0.777778 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 46.666667 Tz (flask ) Tj 1.672222 0 Td 60.493827 Tz (was ) Tj 1.380556 0 Td 50.231481 Tz (sealed ) Tj 2.1 0 Td 52.662037 Tz (with ) Tj 1.555556 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 53.703704 Tz (septum, ) Tj 2.547222 0 Td 55.497685 Tz (degassed ) Tj 51.428571 0 0 51.428571 0 2046 Tm 6.241667 0 Td 57.037037 Tz (under ) Tj 2.022222 0 Td 58.333333 Tz (vacuum, ) Tj 2.780556 0 Td 59.41358 Tz (and ) Tj 1.4 0 Td 49.537037 Tz (flushed ) Tj 2.411111 0 Td 52.662037 Tz (with ) Tj 1.575 0 Td 64.814815 Tz (Ar ) Tj 1.088889 0 Td 50.555556 Tz (\(with ) Tj 1.847222 0 Td 79.398148 Tz (5% ) Tj 1.263889 0 Td 87.5 Tz (CH\) ) Tj 1.886111 0 Td 51.851852 Tz (four ) Tj 51.428571 0 0 51.428571 0 2005.72549 Tm 6.241667 0 Td 53.148148 Tz (times ) Tj 1.75 0 Td 48.611111 Tz (to ) Tj 0.777778 0 Td 60.493827 Tz (remove ) Tj 2.333333 0 Td 59.41358 Tz (any ) Tj 1.244444 0 Td 44.290123 Tz (air ) Tj 0.933333 0 Td 47.395833 Tz (present. ) Tj 2.508333 0 Td 59.143519 Tz (Each ) Tj 1.613889 0 Td 57.253086 Tz (sample ) Tj 2.255556 0 Td 60.493827 Tz (was ) Tj 1.302778 0 Td 46.666667 Tz (irradiated ) Tj 51.428571 0 0 51.428571 0 1961.824108 Tm 6.241667 0 Td 61.574074 Tz (by ) Tj 0.894444 0 Td 56.712963 Tz (an ) Tj 0.894444 0 Td 75.617284 Tz (LED ) Tj 1.516667 0 Td 45.37037 Tz (light ) Tj 1.516667 0 Td 55.092593 Tz (\(450 ) Tj 1.477778 0 Td 64.814815 Tz (nm\) ) Tj 1.322222 0 Td 43.75 Tz (at ) Tj 0.7 0 Td 61.574074 Tz (room ) Tj 1.672222 0 Td 52.73569 Tz (temperature ) Tj 3.636111 0 Td 52.662037 Tz (with ) Tj 1.438889 0 Td 50.636574 Tz (constant ) Tj 51.428571 0 0 51.428571 0 1920.517576 Tm 6.280556 0 Td 41.769547 Tz (stirring. ) Tj 2.45 0 Td 63.734568 Tz (The ) Tj 1.341667 0 Td 58.333333 Tz (amounts ) Tj 2.663889 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 56.712963 Tz (H2 ) Tj 0.952778 0 Td 56.712963 Tz (produced ) Tj 2.916667 0 Td 52.932099 Tz (during ) Tj 2.080556 0 Td 49.768519 Tz (photocatalysis ) Tj 51.428571 0 0 51.428571 0 1876.161209 Tm 6.241667 0 Td 59.953704 Tz (were ) Tj 1.691667 0 Td 54.768519 Tz (determined ) Tj 3.519444 0 Td 59.953704 Tz (by ) Tj 0.991667 0 Td 52.932099 Tz (gas ) Tj 1.205556 0 Td 56.944444 Tz (chromatography ) Tj 5.055556 0 Td 52.5 Tz (using ) Tj 1.827778 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 76.157407 Tz (HP ) Tj 1.127778 0 Td 60.763889 Tz (5890 ) Tj 51.428571 0 0 51.428571 0 1830.296933 Tm 6.280556 0 Td 45.37037 Tz (series ) Tj 1.847222 0 Td 37.268519 Tz (II ) Tj 0.641667 0 Td 62.654321 Tz (Gas ) Tj 1.341667 0 Td 58.333333 Tz (Chromatograph ) Tj 4.763889 0 Td 52.662037 Tz (with ) Tj 1.458333 0 Td 51.851852 Tz (a ) Tj 0.486111 0 Td 82.098765 Tz (TCD ) Tj 1.691667 0 Td 49.016204 Tz (detector ) Tj 2.527778 0 Td 63.888889 Tz (\(Molecu ) Tj 58.571429 0 0 58.571429 0 1790.487212 Tm 5.497561 0 Td 38.888889 Tz (lar ) Tj 0.887805 0 Td 43.252033 Tz (sieve ) Tj 1.502439 0 Td 48.373984 Tz (5 ) Tj 0.512195 0 Td 76.829268 Tz (A ) Tj 0.64878 0 Td 50.406504 Tz (column\) ) Tj 2.321951 0 Td 48.373984 Tz (or ) Tj 0.75122 0 Td 50.863821 Tz (measured ) Tj 2.646341 0 Td 43.902439 Tz (volumetrically ) Tj 3.892683 0 Td 52.642276 Tz (by ) Tj 0.819512 0 Td 48.373984 Tz (a ) Tj 0.495122 0 Td 47.425474 Tz (gas ) Tj 40 0 0 40 0 1753 Tm 8.025 0 Td 58.854167 Tz (burette. ) Tj 51.428571 0 0 51.428571 0 1703 Tm 7 0 Td 66.435185 Tz (As ) Tj 1.147222 0 Td 62.222222 Tz (shown ) Tj 2.216667 0 Td 43.75 Tz (in ) Tj 0.913889 0 Td 56.388889 Tz (FIGS. ) Tj 2.080556 0 Td 55.092593 Tz (16 ) Tj 0.991667 0 Td 59.41358 Tz (and ) Tj 1.438889 0 Td 51.041667 Tz (10a, ) Tj 1.555556 0 Td 53.292181 Tz (formation ) Tj 3.188889 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 87.5 Tz (H ) Tj 1.108333 0 Td 62.654321 Tz (was ) Tj 51.428571 0 0 51.428571 0 1665.2 Tm 6.261111 0 Td 54.282407 Tz (observed ) Tj 2.975 0 Td 59.953704 Tz (upon ) Tj 1.808333 0 Td 49.583333 Tz (photolysis ) Tj 3.344444 0 Td 68.055556 Tz (\(LED ) Tj 1.983333 0 Td 44.722222 Tz (light ) Tj 1.691667 0 Td 43.75 Tz (at ) Tj 0.875 0 Td 61.574074 Tz (450 ) Tj 1.458333 0 Td 62.654321 Tz (nm\) ) Tj 1.477778 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 50.771605 Tz (the ) Tj 52.857143 0 0 52.857143 0 1622.202086 Tm 6.091892 0 Td 56.756757 Tz (above ) Tj 1.910811 0 Td 72.522523 Tz (pH ) Tj 1.097297 0 Td 59.90991 Tz (4 ) Tj 0.605405 0 Td 46.903153 Tz (solution ) Tj 2.478378 0 Td 45.720721 Tz (in ) Tj 0.775676 0 Td 48.348348 Tz (the ) Tj 1.078378 0 Td 52.027027 Tz (presence ) Tj 2.724324 0 Td 53.603604 Tz (of ) Tj 0.832432 0 Td 48.348348 Tz (5.0 ) Tj 1.116216 0 Td 78.828829 Tz (uM ) Tj 1.172973 0 Td 58.108108 Tz (complex ) Tj 2.667568 0 Td 42.567568 Tz (2. ) Tj 52.857143 0 0 52.857143 0 1578.235862 Tm 6.091892 0 Td 62.012012 Tz (The ) Tj 1.418919 0 Td 75.675676 Tz (H ) Tj 1.021622 0 Td 49.399399 Tz (evolution ) Tj 2.951351 0 Td 50.45045 Tz (process ) Tj 2.383784 0 Td 52.552553 Tz (ceased ) Tj 2.156757 0 Td 47.297297 Tz (in ) Tj 0.87027 0 Td 55.18018 Tz (-3 ) Tj 0.964865 0 Td 44.144144 Tz (h, ) Tj 0.794595 0 Td 52.815315 Tz (with ) Tj 1.551351 0 Td 53.603604 Tz (a ) Tj 0.567568 0 Td 79.87988 Tz (TON ) Tj 1.721622 0 Td 56.756757 Tz (of ) Tj 58.571429 0 0 58.571429 0 1537.07393 Tm 5.497561 0 Td 54.634146 Tz (>1600 ) Tj 1.843902 0 Td 54.065041 Tz (mol ) Tj 1.178049 0 Td 36.04336 Tz (H., ) Tj 0.904878 0 Td 48.373984 Tz (\(mol ) Tj 1.382927 0 Td 54.065041 Tz (cat\). ) Tj 1.843902 0 Td 50.863821 Tz (However, ) Tj 2.646341 0 Td 43.631436 Tz (nearly ) Tj 1.758537 0 Td 66.395664 Tz (90% ) Tj 1.382927 0 Td 48.373984 Tz (of ) Tj 0.734146 0 Td 43.631436 Tz (the ) Tj 0.990244 0 Td 45.528455 Tz (H. ) Tj 51.428571 0 0 51.428571 0 1496.057971 Tm 6.261111 0 Td 54.62963 Tz (evolved ) Tj 2.488889 0 Td 50.771605 Tz (within ) Tj 2.022222 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 37.592593 Tz (first ) Tj 1.283333 0 Td 56.712963 Tz (hour ) Tj 1.497222 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 44.290123 Tz (irradiation, ) Tj 3.363889 0 Td 53.098291 Tz (corresponding ) Tj 4.336111 0 Td 46.990741 Tz (to ) Tj 58.571429 0 0 58.571429 0 1454.743823 Tm 5.497561 0 Td 45.528455 Tz (a ) Tj 0.478049 0 Td 45.528455 Tz (turnover ) Tj 2.356098 0 Td 47.109304 Tz (frequency ) Tj 2.74878 0 Td 53.495935 Tz (\(TOF\) ) Tj 1.792683 0 Td 49.796748 Tz (of ) Tj 0.768293 0 Td 51.219512 Tz (1500 ) Tj 1.417073 0 Td 54.065041 Tz (mol ) Tj 1.178049 0 Td 45.528455 Tz (H. ) Tj 0.887805 0 Td 49.796748 Tz (\(mol ) Tj 1.382927 0 Td 39.837398 Tz (cat\) ) Tj 1.263415 0 Td 56.910569 Tz ('h' ) Tj 51.428571 0 0 51.428571 0 1411 Tm 6.280556 0 Td 52.5 Tz (\(FIG. ) Tj 1.847222 0 Td 46.180556 Tz (16\). ) Tj 52.857143 0 0 52.857143 0 1371.361508 Tm 6.810811 0 Td 59.90991 Tz (To ) Tj 0.927027 0 Td 52.202202 Tz (determine ) Tj 2.989189 0 Td 48.348348 Tz (the ) Tj 1.021622 0 Td 74.099099 Tz (pH ) Tj 1.040541 0 Td 44.594595 Tz (effects ) Tj 2.043243 0 Td 58.333333 Tz (on ) Tj 0.927027 0 Td 47.297297 Tz (H. ) Tj 0.889189 0 Td 50.1001 Tz (evolution ) Tj 2.856757 0 Td 49.74975 Tz (catalyzed ) Tj 2.875676 0 Td 59.90991 Tz (by ) Tj 51.428571 0 0 51.428571 0 1332.735294 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.702778 0 Td 42.12963 Tz (2, ) Tj 0.7 0 Td 49.608262 Tz (light-induced ) Tj 4.083333 0 Td 56.712963 Tz (H2 ) Tj 0.933333 0 Td 51.131687 Tz (evolution ) Tj 2.936111 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 56.17284 Tz (performed ) Tj 3.227778 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1288.299492 Tm 6.261111 0 Td 74.537037 Tz (pH ) Tj 1.147222 0 Td 53.148148 Tz (range ) Tj 1.788889 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 54.012346 Tz (3-6 ) Tj 1.205556 0 Td 56.388889 Tz (under ) Tj 1.886111 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 50.555556 Tz (conditions ) Tj 3.266667 0 Td 51.49177 Tz (described ) Tj 2.994444 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 54.282407 Tz (FIG. ) Tj 1.555556 0 Td 48.611111 Tz (16. ) Tj 51.428571 0 0 51.428571 0 1246.829146 Tm 6.261111 0 Td 72.916667 Tz (An ) Tj 1.05 0 Td 62.5 Tz (optimum ) Tj 2.8 0 Td 76.157407 Tz (pH ) Tj 1.088889 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 51.851852 Tz (4.0 ) Tj 1.088889 0 Td 61.574074 Tz (was ) Tj 1.302778 0 Td 54.6875 Tz (observed ) Tj 2.819444 0 Td 47.530864 Tz (for ) Tj 1.030556 0 Td 87.5 Tz (H ) Tj 0.952778 0 Td 50.771605 Tz (evolution ) Tj 2.955556 0 Td 51.851852 Tz (\(FIG. ) Tj 51.428571 0 0 51.428571 0 1206.904642 Tm 6.3 0 Td 43.75 Tz (11\). ) Tj 1.283333 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 57.79321 Tz (pH-dependent ) Tj 4.355556 0 Td 45.37037 Tz (activity ) Tj 2.391667 0 Td 54.012346 Tz (has ) Tj 1.166667 0 Td 57.523148 Tz (been ) Tj 1.633333 0 Td 46.759259 Tz (related ) Tj 2.177778 0 Td 45.37037 Tz (to ) Tj 0.777778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 68.055556 Tz (pKa ) Tj 48.571429 0 0 48.571429 0 1164 Tm 6.629412 0 Td 61.764706 Tz (of ) Tj 0.864706 0 Td 53.615196 Tz (ascorbic ) Tj 2.820588 0 Td 49.411765 Tz (acid, ) Tj 1.770588 0 Td 52.156863 Tz (since ) Tj 1.811765 0 Td 36.029412 Tz (it ) Tj 0.658824 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 54.473039 Tz (believed ) Tj 2.882353 0 Td 48.039216 Tz (that ) Tj 1.379412 0 Td 53.186275 Tz (ascorbic ) Tj 2.820588 0 Td 53.186275 Tz (acid ) Tj 1.523529 0 Td 49.754902 Tz (acts ) Tj 51.428571 0 0 51.428571 0 1122.965422 Tm 6.261111 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 53.472222 Tz (both ) Tj 1.516667 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 52.391975 Tz (proton ) Tj 2.138889 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 48.611111 Tz (electron ) Tj 2.605556 0 Td 56.388889 Tz (donor ) Tj 1.925 0 Td 47.530864 Tz (for ) Tj 1.108333 0 Td 56.712963 Tz (H2 ) Tj 0.991667 0 Td 50.378788 Tz (production. ) Tj 52.857143 0 0 52.857143 0 1082.306864 Tm 6.810811 0 Td 59.90991 Tz (To ) Tj 0.945946 0 Td 50.45045 Tz (explore ) Tj 2.327027 0 Td 48.348348 Tz (the ) Tj 1.097297 0 Td 55.495495 Tz (dependence ) Tj 3.556757 0 Td 53.603604 Tz (of ) Tj 0.813514 0 Td 81.981982 Tz (H ) Tj 0.945946 0 Td 44.144144 Tz (activity ) Tj 2.364865 0 Td 56.756757 Tz (on ) Tj 0.908108 0 Td 48.348348 Tz (the ) Tj 1.097297 0 Td 61.486486 Tz (concen ) Tj 51.428571 0 0 51.428571 0 1041.870926 Tm 6.241667 0 Td 45.37037 Tz (tration ) Tj 2.294444 0 Td 58.333333 Tz (of ) Tj 0.991667 0 Td 59.722222 Tz (complex ) Tj 2.877778 0 Td 43.75 Tz (2, ) Tj 0.913889 0 Td 49.907407 Tz (photolysis ) Tj 3.363889 0 Td 54.208754 Tz (experiments ) Tj 3.966667 0 Td 59.143519 Tz (were ) Tj 1.788889 0 Td 71.296296 Tz (con ) Tj 51.428571 0 0 51.428571 0 998.074442 Tm 6.261111 0 Td 54.012346 Tz (ducted ) Tj 2.236111 0 Td 51.851852 Tz (using ) Tj 1.827778 0 Td 45.730453 Tz (different ) Tj 2.722222 0 Td 50.854701 Tz (concentration ) Tj 4.238889 0 Td 61.574074 Tz (of ) Tj 0.894444 0 Td 59.722222 Tz (complex ) Tj 2.780556 0 Td 58.333333 Tz (2 ) Tj 0.641667 0 Td 50.925926 Tz (\(0.5-50 ) Tj 51.428571 0 0 51.428571 0 954.488712 Tm 6.319444 0 Td 66.975309 Tz (uM\) ) Tj 1.438889 0 Td 45.37037 Tz (at ) Tj 0.777778 0 Td 74.537037 Tz (pH ) Tj 1.147222 0 Td 44.560185 Tz (4.0. ) Tj 1.302778 0 Td 66.435185 Tz (As ) Tj 1.05 0 Td 62.87037 Tz (shown ) Tj 2.177778 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 52.662037 Tz (FIG. ) Tj 1.594444 0 Td 48.611111 Tz (12, ) Tj 1.127778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 50.854701 Tz (concentration ) Tj 4.238889 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 916.355795 Tm 6.261111 0 Td 59.259259 Tz (complex ) Tj 2.819444 0 Td 58.333333 Tz (2 ) Tj 0.7 0 Td 52.932099 Tz (has ) Tj 1.283333 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 49.259259 Tz (great ) Tj 1.788889 0 Td 49.691358 Tz (influence ) Tj 2.994444 0 Td 56.712963 Tz (on ) Tj 1.030556 0 Td 50.771605 Tz (the ) Tj 1.225 0 Td 49.85755 Tz (light-induced ) Tj 4.238889 0 Td 56.712963 Tz (H2 ) Tj 51.428571 0 0 51.428571 0 872.278174 Tm 6.261111 0 Td 50.771605 Tz (evolution ) Tj 3.247222 0 Td 45.37037 Tz (activity ) Tj 2.683333 0 Td 45.37037 Tz (in ) Tj 1.069444 0 Td 53.148148 Tz (terms ) Tj 2.1 0 Td 59.953704 Tz (of ) Tj 1.088889 0 Td 82.098765 Tz (TON ) Tj 1.963889 0 Td 60.493827 Tz (and ) Tj 1.536111 0 Td 62.384259 Tz (TOF, ) Tj 2.022222 0 Td 59.62963 Tz (which ) Tj 51.428571 0 0 51.428571 0 831.915173 Tm 6.261111 0 Td 51.49177 Tz (increased ) Tj 2.955556 0 Td 45.619658 Tz (significantly ) Tj 3.733333 0 Td 46.990741 Tz (at ) Tj 0.758333 0 Td 55.092593 Tz (lower ) Tj 1.827778 0 Td 50.356125 Tz (concentration ) Tj 4.141667 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 43.930041 Tz (catalyst. ) Tj 2.547222 0 Td 61.574074 Tz (At ) Tj 58.571429 0 0 58.571429 0 788.550067 Tm 5.514634 0 Td 54.065041 Tz (50 ) Tj 0.853659 0 Td 69.715447 Tz (uM ) Tj 1.058537 0 Td 52.439024 Tz (complex ) Tj 2.407317 0 Td 38.414634 Tz (2, ) Tj 0.665854 0 Td 48.373984 Tz (a ) Tj 0.460976 0 Td 73.03523 Tz (TON ) Tj 1.519512 0 Td 52.642276 Tz (of ) Tj 0.75122 0 Td 54.776423 Tz (~450 ) Tj 1.502439 0 Td 54.065041 Tz (mol ) Tj 1.229268 0 Td 42.682927 Tz (H. ) Tj 0.853659 0 Td 50.50813 Tz (\(mol ) Tj 1.417073 0 Td 47.235772 Tz (cat\)' ) Tj 1.656098 0 Td 54.065041 Tz (and ) Tj 58.571429 0 0 58.571429 0 746 Tm 5.497561 0 Td 65.447154 Tz (TOF ) Tj 1.34878 0 Td 51.219512 Tz (of ) Tj 0.682927 0 Td 53.116531 Tz (410 ) Tj 1.126829 0 Td 53.116531 Tz (mol ) Tj 1.160976 0 Td 45.528455 Tz (H. ) Tj 0.836585 0 Td 48.373984 Tz (\(mol ) Tj 1.331707 0 Td 40.54878 Tz (cat\) ) Tj 1.246341 0 Td 56.910569 Tz ('h' ) Tj 1.229268 0 Td 51.930894 Tz (were ) Tj 1.365854 0 Td 43.631436 Tz (obtained. ) Tj 2.543902 0 Td 50.863821 Tz (However, ) Tj 51.428571 0 0 51.428571 0 706.37234 Tm 6.261111 0 Td 45.37037 Tz (at ) Tj 0.875 0 Td 47.530864 Tz (1.0 ) Tj 1.283333 0 Td 66.435185 Tz (LM ) Tj 1.069444 0 Td 59.722222 Tz (complex ) Tj 2.761111 0 Td 45.37037 Tz (2, ) Tj 0.836111 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 82.098765 Tz (TON ) Tj 1.75 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 75.617284 Tz (TOF ) Tj 1.613889 0 Td 51.131687 Tz (increased ) Tj 3.013889 0 Td 51.311728 Tz (drasti ) Tj 58.571429 0 0 58.571429 0 663.905028 Tm 5.497561 0 Td 40.97561 Tz (cally ) Tj 1.519512 0 Td 38.414634 Tz (to ) Tj 0.717073 0 Td 54.776423 Tz (4400 ) Tj 1.553659 0 Td 55.01355 Tz (mol ) Tj 1.263415 0 Td 46.95122 Tz (H. ) Tj 0.973171 0 Td 49.085366 Tz (\(mol ) Tj 1.417073 0 Td 47.804878 Tz (cat\)' ) Tj 1.741463 0 Td 53.116531 Tz (and ) Tj 1.195122 0 Td 54.065041 Tz (4000 ) Tj 1.553659 0 Td 54.065041 Tz (mol ) Tj 1.263415 0 Td 35.094851 Tz (H., ) Tj 0.939024 0 Td 49.796748 Tz (\(mol ) Tj 58.571429 0 0 58.571429 0 624.976998 Tm 5.497561 0 Td 40.54878 Tz (cat\) ) Tj 1.280488 0 Td 49.796748 Tz ('h', ) Tj 1.331707 0 Td 41.150719 Tz (respectively. ) Tj 3.312195 0 Td 56.910569 Tz (The ) Tj 1.143902 0 Td 50.365854 Tz (dependence ) Tj 3.158537 0 Td 46.95122 Tz (of ) Tj 0.64878 0 Td 72.086721 Tz (TON ) Tj 1.434146 0 Td 52.168022 Tz (and ) Tj 1.041463 0 Td 67.344173 Tz (TOF ) Tj 1.34878 0 Td 55.487805 Tz (on ) Tj 51.428571 0 0 51.428571 0 581.26087 Tm 6.261111 0 Td 46.990741 Tz (catalyst ) Tj 2.761111 0 Td 50.356125 Tz (concentration ) Tj 4.511111 0 Td 47.530864 Tz (indicates ) Tj 3.091667 0 Td 46.990741 Tz (that ) Tj 1.633333 0 Td 50.771605 Tz (the ) Tj 1.477778 0 Td 52.572016 Tz (formation ) Tj 3.402778 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 541.782003 Tm 6.241667 0 Td 51.49177 Tz (binuclear ) Tj 3.013889 0 Td 51.851852 Tz (or ) Tj 0.855556 0 Td 52.73569 Tz (polynuclear ) Tj 3.733333 0 Td 50 Tz (species ) Tj 2.430556 0 Td 55.740741 Tz (might ) Tj 1.905556 0 Td 59.953704 Tz (be ) Tj 1.011111 0 Td 52.662037 Tz (involved ) Tj 2.819444 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 499.797814 Tm 6.261111 0 Td 47.530864 Tz (inactivation ) Tj 3.694444 0 Td 56.712963 Tz (of ) Tj 0.855556 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 43.75 Tz (2. ) Tj 51.428571 0 0 51.428571 0 425.087248 Tm 13.416667 0 Td 61.111111 Tz (Example ) Tj 2.819444 0 Td 55.092593 Tz (6 ) Tj 51.428571 0 0 51.428571 0 340.995604 Tm 10.286111 0 Td 52.777778 Tz (Control ) Tj 2.488889 0 Td 49.907407 Tz (Photolysis ) Tj 3.286111 0 Td 55.092593 Tz (Experiments ) Tj 51.428571 0 0 51.428571 0 256.246415 Tm 7 0 Td 61.574074 Tz (To ) Tj 1.030556 0 Td 46.585648 Tz (identify ) Tj 2.508333 0 Td 46.759259 Tz (factors ) Tj 2.236111 0 Td 50.084175 Tz (responsible ) Tj 3.577778 0 Td 47.530864 Tz (for ) Tj 1.108333 0 Td 47.530864 Tz (the ) Tj 1.147222 0 Td 54.344729 Tz (decomposition ) Tj 4.491667 0 Td 59.953704 Tz (of ) Tj 51.428571 0 0 51.428571 0 213.22807 Tm 6.261111 0 Td 48.842593 Tz (photocatalytic ) Tj 4.375 0 Td 56.712963 Tz (H2 ) Tj 0.972222 0 Td 50.411523 Tz (evolution ) Tj 2.955556 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 58.333333 Tz (above ) Tj 1.963889 0 Td 51.388889 Tz (system, ) Tj 2.411111 0 Td 58.333333 Tz (one ) Tj 1.263889 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 58.571429 0 0 58.571429 0 173.538462 Tm 5.480488 0 Td 43.252033 Tz (three ) Tj 1.502439 0 Td 51.504065 Tz (components ) Tj 3.295122 0 Td 42.999097 Tz (\(ascorbic ) Tj 2.509756 0 Td 40.406504 Tz (acid, ) Tj 1.639024 0 Td 60.704607 Tz (Ru\(bpy\)", ) Tj 3.482927 0 Td 45.528455 Tz (or ) Tj 0.7 0 Td 53.252033 Tz (complex ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 77.252252 Tz (26 ) Tj 51.428571 0 0 51.428571 0 2913 Tm 25.2 0 Td 50.231481 Tz (2\) ) Tj 0.972222 0 Td 62.654321 Tz (was ) Tj 1.497222 0 Td 58.333333 Tz (added ) Tj 2.119444 0 Td 43.75 Tz (to ) Tj 0.913889 0 Td 58.333333 Tz (a ) Tj 0.7 0 Td 49.016204 Tz (reaction ) Tj 2.741667 0 Td 46.018519 Tz (flask ) Tj 1.691667 0 Td 46.018519 Tz (after ) Tj 1.730556 0 Td 50.771605 Tz (the ) Tj 1.244444 0 Td 49.331276 Tz (cessation ) Tj 3.091667 0 Td 56.712963 Tz (H2 ) Tj 52.857143 0 0 52.857143 0 2870.900875 Tm 24.518919 0 Td 49.399399 Tz (evolution ) Tj 2.894595 0 Td 45.720721 Tz (to ) Tj 0.794595 0 Td 50.45045 Tz (see ) Tj 1.135135 0 Td 44.144144 Tz (if ) Tj 0.681081 0 Td 75.675676 Tz (H ) Tj 0.983784 0 Td 51.396396 Tz (production ) Tj 3.291892 0 Td 52.972973 Tz (could ) Tj 1.816216 0 Td 55.18018 Tz (be ) Tj 0.908108 0 Td 52.815315 Tz (resumed. ) Tj 51.428571 0 0 51.428571 0 2828.514286 Tm 25.919444 0 Td 53.877315 Tz (Addition ) Tj 2.780556 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 58.333333 Tz (any ) Tj 1.263889 0 Td 57.253086 Tz (one ) Tj 1.244444 0 Td 55.092593 Tz (of ) Tj 0.758333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 49.259259 Tz (three ) Tj 1.672222 0 Td 55.387205 Tz (components, ) Tj 3.869444 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 61.574074 Tz (same ) Tj 51.428571 0 0 51.428571 0 2786.072993 Tm 25.2 0 Td 61.033951 Tz (amount ) Tj 2.313889 0 Td 51.851852 Tz (as ) Tj 0.777778 0 Td 46.990741 Tz (that ) Tj 1.263889 0 Td 55.902778 Tz (used ) Tj 1.516667 0 Td 43.75 Tz (in ) Tj 0.680556 0 Td 49.305556 Tz (photocatalytic ) Tj 4.336111 0 Td 46.090535 Tz (reaction, ) Tj 2.663889 0 Td 47.800926 Tz (resulted ) Tj 2.45 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 56.712963 Tz (no ) Tj 52.857143 0 0 52.857143 0 2745.146067 Tm 24.537838 0 Td 44.430794 Tz (significant ) Tj 3.159459 0 Td 58.858859 Tz (amount ) Tj 2.345946 0 Td 55.18018 Tz (of ) Tj 0.87027 0 Td 78.828829 Tz (H ) Tj 0.945946 0 Td 49.189189 Tz (formation, ) Tj 3.216216 0 Td 50.45045 Tz (suggesting ) Tj 3.216216 0 Td 49.399399 Tz (the ) Tj 1.116216 0 Td 70 Tz (decom ) Tj 51.428571 0 0 51.428571 0 2706.264706 Tm 25.2 0 Td 48.611111 Tz (position ) Tj 2.586111 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 39.969136 Tz (all ) Tj 0.952778 0 Td 49.259259 Tz (three ) Tj 1.730556 0 Td 49.074074 Tz (species ) Tj 2.333333 0 Td 52.662037 Tz (occurred ) Tj 2.761111 0 Td 52.932099 Tz (during ) Tj 2.119444 0 Td 49.305556 Tz (photocatalytic ) Tj 52.857143 0 0 52.857143 0 2662.504294 Tm 24.518919 0 Td 85.135135 Tz (H ) Tj 0.927027 0 Td 47.612613 Tz (evolution. ) Tj 3.027027 0 Td 55.18018 Tz (Both ) Tj 1.475676 0 Td 58.108108 Tz (complex ) Tj 2.591892 0 Td 63.063063 Tz (2 ) Tj 0.510811 0 Td 57.807808 Tz (and ) Tj 1.172973 0 Td 47.927928 Tz (photosensitizer ) Tj 4.427027 0 Td 55.968468 Tz (need ) Tj 1.494595 0 Td 44.144144 Tz (to ) Tj 0.681081 0 Td 56.756757 Tz (be ) Tj 51.428571 0 0 51.428571 0 2620.525745 Tm 25.2 0 Td 58.333333 Tz (added ) Tj 2.002778 0 Td 45.37037 Tz (to ) Tj 0.875 0 Td 57.253086 Tz (resume ) Tj 2.333333 0 Td 87.5 Tz (H ) Tj 1.05 0 Td 50.084175 Tz (production, ) Tj 3.616667 0 Td 52.662037 Tz (with ) Tj 1.555556 0 Td 70.486111 Tz (~37% ) Tj 2.002778 0 Td 61.574074 Tz (more ) Tj 1.788889 0 Td 84.259259 Tz (H ) Tj 1.011111 0 Td 68.055556 Tz (pro ) Tj 51.428571 0 0 51.428571 0 2576 Tm 25.2 0 Td 51.388889 Tz (duction ) Tj 2.469444 0 Td 51.851852 Tz (\(FIG. ) Tj 1.886111 0 Td 45.37037 Tz (14\). ) Tj 1.380556 0 Td 62.654321 Tz (The ) Tj 1.4 0 Td 49.421296 Tz (addition ) Tj 2.625 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 52.662037 Tz (both ) Tj 1.555556 0 Td 50.231481 Tz (ascorbic ) Tj 2.702778 0 Td 50.231481 Tz (acid ) Tj 1.458333 0 Td 60.493827 Tz (and ) Tj 57.142857 0 0 57.142857 0 2537.446927 Tm 22.8725 0 Td 66.354167 Tz (Ru\(bpy\)" ) Tj 3.5175 0 Td 43.75 Tz (also ) Tj 1.365 0 Td 44.722222 Tz (led ) Tj 1.12 0 Td 40.833333 Tz (to ) Tj 0.805 0 Td 53.958333 Tz (an ) Tj 0.945 0 Td 44.479167 Tz (increase ) Tj 2.45 0 Td 51.041667 Tz (of ) Tj 0.875 0 Td 78.75 Tz (H ) Tj 1.015 0 Td 46.018519 Tz (evolution ) Tj 2.7825 0 Td 53.958333 Tz (by ) Tj 38.571429 0 0 38.571429 0 2501 Tm 33.625926 0 Td 82.962963 Tz (-10%. ) Tj 52.857143 0 0 52.857143 0 2454.005076 Tm 25.256757 0 Td 56.362613 Tz (However, ) Tj 2.875676 0 Td 55.18018 Tz (no ) Tj 0.851351 0 Td 44.430794 Tz (significant ) Tj 3.064865 0 Td 59.384384 Tz (amount ) Tj 2.27027 0 Td 53.603604 Tz (of ) Tj 0.737838 0 Td 85.135135 Tz (H ) Tj 0.908108 0 Td 60.960961 Tz (was ) Tj 1.210811 0 Td 55.574324 Tz (produced ) Tj 2.8 0 Td 64.63964 Tz (when ) Tj 51.428571 0 0 51.428571 0 2412.862843 Tm 25.180556 0 Td 54.282407 Tz (both ) Tj 1.497222 0 Td 50.636574 Tz (ascorbic ) Tj 2.625 0 Td 51.851852 Tz (acid ) Tj 1.438889 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 58.796296 Tz (complex ) Tj 2.702778 0 Td 55.092593 Tz (2 ) Tj 0.563889 0 Td 58.333333 Tz (were ) Tj 1.594444 0 Td 53.472222 Tz (added, ) Tj 2.138889 0 Td 51.851852 Tz (Suggesting ) Tj 3.305556 0 Td 55.092593 Tz (a ) Tj 58.571429 0 0 58.571429 0 2373.865291 Tm 22.126829 0 Td 49.085366 Tz (complete ) Tj 2.526829 0 Td 48.155097 Tz (decomposition ) Tj 3.943902 0 Td 49.796748 Tz (of ) Tj 0.939024 0 Td 56.594399 Tz (Ru\(bpy\)," ) Tj 3.295122 0 Td 48.373984 Tz (under ) Tj 1.604878 0 Td 43.631436 Tz (the ) Tj 0.973171 0 Td 43.038618 Tz (reaction ) Tj 51.428571 0 0 51.428571 0 2328.281988 Tm 25.2 0 Td 48.316498 Tz (conditions. ) Tj 3.383333 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 50.501543 Tz (coordination ) Tj 3.869444 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 48.611111 Tz (acetate ) Tj 2.255556 0 Td 49.691358 Tz (ion ) Tj 1.088889 0 Td 48.611111 Tz (to ) Tj 0.797222 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 55.092593 Tz (2 ) Tj 0.563889 0 Td 51.851852 Tz (or ) Tj 58.571429 0 0 58.571429 0 2289.111111 Tm 22.109756 0 Td 44.579946 Tz (the ) Tj 0.956098 0 Td 41.49729 Tz (substitution ) Tj 3.141463 0 Td 51.219512 Tz (of ) Tj 0.682927 0 Td 53.116531 Tz (bpy ) Tj 1.126829 0 Td 45.054201 Tz (ligand ) Tj 1.758537 0 Td 41.260163 Tz (in ) Tj 0.870732 0 Td 64.735772 Tz (Ru\(bpy\)" ) Tj 3.260976 0 Td 52.642276 Tz (by ) Tj 0.785366 0 Td 42.682927 Tz (acetate ) Tj 1.963415 0 Td 45.528455 Tz (ion ) Tj 51.428571 0 0 51.428571 0 2249.421569 Tm 25.2 0 Td 69.135802 Tz (may ) Tj 1.477778 0 Td 49.259259 Tz (contribute ) Tj 3.169444 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 54.344729 Tz (decomposition ) Tj 4.511111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 49.074074 Tz (photocatalytic ) Tj 4.394444 0 Td 63.734568 Tz (sys ) Tj 51.428571 0 0 51.428571 0 2203.39498 Tm 25.180556 0 Td 60.493827 Tz (tem ) Tj 1.438889 0 Td 47.530864 Tz (for ) Tj 1.166667 0 Td 87.5 Tz (H ) Tj 1.108333 0 Td 48.287037 Tz (evolution. ) Tj 3.286111 0 Td 52.391975 Tz (Furthermore, ) Tj 4.102778 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 53.472222 Tz (presence ) Tj 2.877778 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 47.314815 Tz (trace ) Tj 51.428571 0 0 51.428571 0 2161.646154 Tm 25.2 0 Td 61.033951 Tz (amount ) Tj 2.411111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 44.290123 Tz (air ) Tj 1.011111 0 Td 43.75 Tz (in ) Tj 0.758333 0 Td 48.611111 Tz (reaction ) Tj 2.547222 0 Td 46.666667 Tz (flask ) Tj 1.613889 0 Td 68.055556 Tz (may ) Tj 1.458333 0 Td 47.800926 Tz (also ) Tj 1.380556 0 Td 50.231481 Tz (lead ) Tj 1.4 0 Td 48.611111 Tz (to ) Tj 0.777778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 71.944444 Tz (decom ) Tj 51.428571 0 0 51.428571 0 2123.945274 Tm 25.2 0 Td 48.611111 Tz (position ) Tj 2.547222 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 45.37037 Tz (catalytic ) Tj 2.683333 0 Td 51.388889 Tz (system. ) Tj 2.391667 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 61.033951 Tz (amount ) Tj 2.411111 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 56.712963 Tz (H2 ) Tj 0.972222 0 Td 56.712963 Tz (produced ) Tj 2.936111 0 Td 46.990741 Tz (in ) Tj 52.857143 0 0 52.857143 0 2080.378446 Tm 24.5 0 Td 49.399399 Tz (the ) Tj 1.040541 0 Td 51.632883 Tz (presence ) Tj 2.62973 0 Td 53.603604 Tz (of ) Tj 0.718919 0 Td 43.093093 Tz (air ) Tj 0.908108 0 Td 40.990991 Tz (is ) Tj 0.624324 0 Td 52.027027 Tz (only ) Tj 1.418919 0 Td 71.471471 Tz (40% ) Tj 1.437838 0 Td 55.18018 Tz (of ) Tj 0.737838 0 Td 44.932432 Tz (that ) Tj 1.210811 0 Td 55.18018 Tz (produced ) Tj 2.8 0 Td 63.063063 Tz (when ) Tj 1.702703 0 Td 46.246246 Tz (the ) Tj 1.059459 0 Td 45.720721 Tz (H. ) Tj 51.428571 0 0 51.428571 0 2037.725067 Tm 25.2 0 Td 50.771605 Tz (evolution ) Tj 3.169444 0 Td 61.574074 Tz (was ) Tj 1.516667 0 Td 55.452675 Tz (conducted ) Tj 3.383333 0 Td 56.388889 Tz (under ) Tj 2.041667 0 Td 49.691358 Tz (Ar, ) Tj 1.302778 0 Td 51.851852 Tz (Suggesting ) Tj 3.480556 0 Td 93.981481 Tz (O ) Tj 1.244444 0 Td 55.092593 Tz (does ) Tj 51.428571 0 0 51.428571 0 1994 Tm 25.2 0 Td 45.37037 Tz (inhibit ) Tj 2.138889 0 Td 87.5 Tz (H ) Tj 0.972222 0 Td 48.935185 Tz (evolution. ) Tj 52.857143 0 0 52.857143 0 1955.36612 Tm 25.218919 0 Td 51.351351 Tz (Control ) Tj 2.345946 0 Td 52.457002 Tz (experiments ) Tj 3.651351 0 Td 51.801802 Tz (without ) Tj 2.345946 0 Td 48.873874 Tz (ascorbic ) Tj 2.535135 0 Td 44.774775 Tz (acid, ) Tj 1.816216 0 Td 56.306306 Tz (Ru\(bpy\) ) Tj 51.428571 0 0 51.428571 0 1913.123119 Tm 25.2 0 Td 53.472222 Tz (or ) Tj 0.913889 0 Td 59.259259 Tz (complex ) Tj 2.8 0 Td 55.092593 Tz (2 ) Tj 0.641667 0 Td 62.114198 Tz (showed ) Tj 2.566667 0 Td 56.712963 Tz (no ) Tj 0.991667 0 Td 53.472222 Tz (or ) Tj 0.894444 0 Td 53.472222 Tz (only ) Tj 1.594444 0 Td 47.800926 Tz (residual ) Tj 2.586111 0 Td 58.333333 Tz (amounts ) Tj 2.780556 0 Td 56.712963 Tz (of ) Tj 0.933333 0 Td 81.018519 Tz (H ) Tj 51.428571 0 0 51.428571 0 1876.054827 Tm 25.2 0 Td 50.378788 Tz (production, ) Tj 3.519444 0 Td 51.527778 Tz (Suggesting ) Tj 3.247222 0 Td 41.049383 Tz (all ) Tj 0.894444 0 Td 49.259259 Tz (three ) Tj 1.633333 0 Td 58.333333 Tz (components ) Tj 3.675 0 Td 49.691358 Tz (are ) Tj 1.05 0 Td 50.636574 Tz (required ) Tj 2.625 0 Td 47.530864 Tz (for ) Tj 51.428571 0 0 51.428571 0 1828 Tm 25.2 0 Td 87.5 Tz (H ) Tj 1.011111 0 Td 51.49177 Tz (evolution ) Tj 3.013889 0 Td 52.5 Tz (\(FIG. ) Tj 1.847222 0 Td 47.962963 Tz (10b\). ) Tj 51.428571 0 0 51.428571 0 1791.478723 Tm 25.919444 0 Td 72.106481 Tz (When ) Tj 2.119444 0 Td 49.583333 Tz (photolysis ) Tj 3.363889 0 Td 54.768519 Tz (experiment ) Tj 3.636111 0 Td 62.654321 Tz (was ) Tj 1.477778 0 Td 56.17284 Tz (conducted ) Tj 3.383333 0 Td 45.37037 Tz (at ) Tj 0.875 0 Td 53.472222 Tz (higher ) Tj 58.571429 0 0 58.571429 0 1746.980653 Tm 22.126829 0 Td 44.652908 Tz (concentration ) Tj 3.619512 0 Td 49.796748 Tz (of ) Tj 0.665854 0 Td 44.105691 Tz (ascorbic ) Tj 2.236585 0 Td 45.528455 Tz (acid ) Tj 1.212195 0 Td 41.971545 Tz (\(0.5 ) Tj 1.178049 0 Td 64.02439 Tz (M\) ) Tj 0.887805 0 Td 52.168022 Tz (and ) Tj 1.280488 0 Td 64.735772 Tz (Ru\(bpy\)" ) Tj 3.243902 0 Td 41.971545 Tz (\(2.0 ) Tj 51.428571 0 0 51.428571 0 1704.390836 Tm 25.2 0 Td 79.938272 Tz (mM\) ) Tj 1.75 0 Td 53.472222 Tz (with ) Tj 1.594444 0 Td 49.691358 Tz (5.0 ) Tj 1.575 0 Td 100.462963 Tz (M ) Tj 0.933333 0 Td 59.722222 Tz (complex ) Tj 2.8 0 Td 45.37037 Tz (2, ) Tj 0.836111 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 83.179012 Tz (TON ) Tj 1.808333 0 Td 50.771605 Tz (increased ) Tj 3.033333 0 Td 48.148148 Tz (further ) Tj 58.571429 0 0 58.571429 0 1663.522816 Tm 22.126829 0 Td 51.219512 Tz (from ) Tj 1.502439 0 Td 51.930894 Tz (1600 ) Tj 1.434146 0 Td 39.837398 Tz (to ) Tj 0.682927 0 Td 54.065041 Tz (2100 ) Tj 1.536585 0 Td 51.219512 Tz (mol ) Tj 1.195122 0 Td 35.094851 Tz (H., ) Tj 0.887805 0 Td 49.796748 Tz (\(mol ) Tj 1.4 0 Td 54.634146 Tz (cat\), ) Tj 1.843902 0 Td 47.060663 Tz (corresponding ) Tj 3.87561 0 Td 39.837398 Tz (to ) Tj 0.665854 0 Td 51.219512 Tz (a ) Tj 60 0 0 60 0 1620.129366 Tm 21.6 0 Td 64.814815 Tz (TOF ) Tj 1.35 0 Td 52.777778 Tz (of ) Tj 0.75 0 Td 53.888889 Tz (>1900 ) Tj 1.8 0 Td 53.703704 Tz (mol ) Tj 1.216667 0 Td 34.259259 Tz (H., ) Tj 0.883333 0 Td 47.916667 Tz (\(mol ) Tj 1.366667 0 Td 52.777778 Tz (cat\)'h' ) Tj 2.5 0 Td 44.907407 Tz (during ) Tj 1.833333 0 Td 42.592593 Tz (the ) Tj 0.966667 0 Td 32.222222 Tz (first ) Tj 1.166667 0 Td 48.611111 Tz (hour ) Tj 51.428571 0 0 51.428571 0 1578 Tm 25.2 0 Td 45.664983 Tz (irradiation ) Tj 3.286111 0 Td 52.5 Tz (\(FIG. ) Tj 1.886111 0 Td 46.180556 Tz (13\). ) Tj 1.361111 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 57.685185 Tz (above ) Tj 1.983333 0 Td 47.685185 Tz (studies ) Tj 2.294444 0 Td 54.282407 Tz (demonstrated ) Tj 4.180556 0 Td 45.37037 Tz (that ) Tj 51.428571 0 0 51.428571 0 1542.47343 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.069444 0 Td 49.608262 Tz (light-induced ) Tj 4.063889 0 Td 56.712963 Tz (H2 ) Tj 0.894444 0 Td 52.824074 Tz (production ) Tj 3.325 0 Td 51.131687 Tz (catalyzed ) Tj 2.877778 0 Td 61.574074 Tz (by ) Tj 0.933333 0 Td 59.259259 Tz (complex ) Tj 2.644444 0 Td 55.092593 Tz (2 ) Tj 0.505556 0 Td 47.800926 Tz (also ) Tj 51.428571 0 0 51.428571 0 1496.427083 Tm 25.2 0 Td 56.481481 Tz (depends ) Tj 2.761111 0 Td 58.333333 Tz (on ) Tj 1.069444 0 Td 50.771605 Tz (the ) Tj 1.283333 0 Td 50.462963 Tz (concentrations ) Tj 4.627778 0 Td 56.712963 Tz (of ) Tj 0.952778 0 Td 42.424242 Tz (sacrificial ) Tj 3.208333 0 Td 51.388889 Tz (reagent ) Tj 2.508333 0 Td 59.41358 Tz (and ) Tj 51.428571 0 0 51.428571 0 1456.5086 Tm 25.2 0 Td 49.259259 Tz (photosensitizer ) Tj 4.588889 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 45.37037 Tz (that ) Tj 1.283333 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 54.166667 Tz (reduced ) Tj 2.469444 0 Td 57.523148 Tz (form ) Tj 1.575 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 58.333333 Tz (2 ) Tj 0.544444 0 Td 46.990741 Tz (acts ) Tj 51.428571 0 0 51.428571 0 1414.455344 Tm 25.2 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 51.311728 Tz (highly ) Tj 2.1 0 Td 43.209877 Tz (efficient ) Tj 2.566667 0 Td 49.85755 Tz (photocatalyst ) Tj 4.102778 0 Td 48.611111 Tz (for ) Tj 1.147222 0 Td 77.777778 Tz (H ) Tj 0.952778 0 Td 48.935185 Tz (evolution. ) Tj 51.428571 0 0 51.428571 0 1339.04 Tm 32.355556 0 Td 61.111111 Tz (Example ) Tj 2.8 0 Td 58.333333 Tz (7 ) Tj 40 0 0 40 0 1257 Tm 39.075 0 Td 63.425926 Tz (Structure ) Tj 3.75 0 Td 69.230769 Tz (Determination ) Tj 51.428571 0 0 51.428571 0 1170.712925 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.497222 0 Td 47.395833 Tz (suitable ) Tj 2.605556 0 Td 46.585648 Tz (crystals ) Tj 2.625 0 Td 48.611111 Tz (for ) Tj 1.205556 0 Td 56.388889 Tz (X-ray ) Tj 2.061111 0 Td 49.907407 Tz (crystallography ) Tj 4.9 0 Td 56.712963 Tz (of ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 58.571429 0 0 58.571429 0 1126.743902 Tm 22.126829 0 Td 67.344173 Tz (Co' ) Tj 1.519512 0 Td 51.219512 Tz (form ) Tj 1.519512 0 Td 52.642276 Tz (of ) Tj 0.802439 0 Td 52.845528 Tz (complex ) Tj 2.543902 0 Td 31.300813 Tz (1 ) Tj 0.546341 0 Td 52.642276 Tz (were ) Tj 1.536585 0 Td 54.065041 Tz (grown ) Tj 1.912195 0 Td 51.219512 Tz (from ) Tj 1.502439 0 Td 51.219512 Tz (a ) Tj 0.563415 0 Td 43.394309 Tz (solution ) Tj 2.356098 0 Td 51.219512 Tz (of ) Tj 51.428571 0 0 51.428571 0 1085.383202 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.8 0 Td 38.888889 Tz (1 ) Tj 0.563889 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 83.899177 Tz (CHCN/CHCl ) Tj 5.036111 0 Td 46.666667 Tz (\(1:1\) ) Tj 1.652778 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 37.268519 Tz (air. ) Tj 1.127778 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 45.37037 Tz (crystal ) Tj 2.197222 0 Td 61.574074 Tz (was ) Tj 51.428571 0 0 51.428571 0 1043.271605 Tm 25.2 0 Td 44.722222 Tz (flash ) Tj 1.652778 0 Td 54.012346 Tz (cooled ) Tj 2.236111 0 Td 45.37037 Tz (to ) Tj 0.913889 0 Td 58.333333 Tz (100 ) Tj 1.322222 0 Td 87.5 Tz (K ) Tj 0.797222 0 Td 48.611111 Tz (for ) Tj 1.108333 0 Td 56.388889 Tz (X-ray ) Tj 2.002778 0 Td 48.611111 Tz (analysis ) Tj 2.605556 0 Td 59.953704 Tz (on ) Tj 1.030556 0 Td 51.851852 Tz (a ) Tj 0.661111 0 Td 55.092593 Tz (Bruker ) Tj 2.255556 0 Td 71.296296 Tz (D8 ) Tj 51.428571 0 0 51.428571 0 1000 Tm 25.2 0 Td 49.305556 Tz (diffractometer ) Tj 4.530556 0 Td 46.585648 Tz (3-circle ) Tj 2.663889 0 Td 49.074074 Tz (diffractometer ) Tj 4.55 0 Td 52.662037 Tz (with ) Tj 1.730556 0 Td 47.962963 Tz (fixed ) Tj 1.944444 0 Td 38.888889 Tz (X. ) Tj 0.913889 0 Td 63.734568 Tz (The ) Tj 51.428571 0 0 51.428571 0 959.853051 Tm 25.2 0 Td 45.833333 Tz (crystal ) Tj 2.138889 0 Td 62.654321 Tz (was ) Tj 1.302778 0 Td 50.378788 Tz (illuminated ) Tj 3.5 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 56.388889 Tz (X-ray ) Tj 1.886111 0 Td 65.625 Tz (beam ) Tj 1.769444 0 Td 58.333333 Tz (from ) Tj 1.613889 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 58.333333 Tz (FR-591 ) Tj 51.428571 0 0 51.428571 0 924.151358 Tm 25.2 0 Td 50.694444 Tz (rotating-anode ) Tj 4.647222 0 Td 56.388889 Tz (X-ray ) Tj 2.119444 0 Td 51.49177 Tz (generator ) Tj 3.15 0 Td 56.30787 Tz (equipped ) Tj 3.111111 0 Td 53.472222 Tz (with ) Tj 1.711111 0 Td 51.851852 Tz (a ) Tj 0.758333 0 Td 55.632716 Tz (copper ) Tj 51.428571 0 0 51.428571 0 878.753846 Tm 25.2 0 Td 58.333333 Tz (anode ) Tj 2.041667 0 Td 59.41358 Tz (and ) Tj 1.438889 0 Td 50.771605 Tz (Helios ) Tj 2.158333 0 Td 52.256944 Tz (focusing ) Tj 2.858333 0 Td 46.990741 Tz (mirrors. ) Tj 2.586111 0 Td 63.734568 Tz (The ) Tj 1.458333 0 Td 47.170782 Tz (resulting ) Tj 2.858333 0 Td 57.253086 Tz (images ) Tj 51.428571 0 0 51.428571 0 835.736842 Tm 25.180556 0 Td 59.953704 Tz (were ) Tj 1.711111 0 Td 48.611111 Tz (integrated ) Tj 3.208333 0 Td 51.851852 Tz (with ) Tj 1.536111 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 55.092593 Tz (Bruker ) Tj 2.236111 0 Td 71.296296 Tz (SAINT ) Tj 2.411111 0 Td 52.256944 Tz (software ) Tj 2.780556 0 Td 56.944444 Tz (package ) Tj 51.428571 0 0 51.428571 0 796.113786 Tm 25.180556 0 Td 53.148148 Tz (using ) Tj 1.808333 0 Td 58.333333 Tz (a ) Tj 0.641667 0 Td 55.092593 Tz (narrow-frame ) Tj 4.2 0 Td 49.583333 Tz (algorithm. ) Tj 40 0 0 40 0 758 Tm 33.325 0 Td 81.944444 Tz (The ) Tj 1.975 0 Td 60.648148 Tz (structure ) Tj 3.775 0 Td 80.555556 Tz (was ) Tj 2 0 Td 67.361111 Tz (solved ) Tj 2.925 0 Td 75 Tz (and ) Tj 1.85 0 Td 61.904762 Tz (refined ) Tj 3.125 0 Td 62.5 Tz (via ) Tj 1.625 0 Td 63.888889 Tz (the ) Tj 1.675 0 Td 72.916667 Tz (Bruker ) Tj 51.428571 0 0 51.428571 0 712.933248 Tm 25.219444 0 Td 75.925926 Tz (SHELXTL ) Tj 3.519444 0 Td 51.851852 Tz (software ) Tj 2.8 0 Td 53.472222 Tz (package, ) Tj 2.897222 0 Td 52.5 Tz (using ) Tj 1.886111 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 53.796296 Tz (space ) Tj 1.925 0 Td 56.388889 Tz (group ) Tj 2.061111 0 Td 46.990741 Tz (P-1, ) Tj 51.428571 0 0 51.428571 0 667 Tm 25.180556 0 Td 54.282407 Tz (with ) Tj 1.711111 0 Td 66.975309 Tz (Z-2 ) Tj 1.613889 0 Td 48.611111 Tz (for ) Tj 1.244444 0 Td 49.691358 Tz (the ) Tj 1.283333 0 Td 54.62963 Tz (formula ) Tj 2.683333 0 Td 42.777778 Tz (unit, ) Tj 1.691667 0 Td 75.347222 Tz (CassFH-47ClzCON. ) Tj 51.428571 0 0 51.428571 0 628.478736 Tm 25.219444 0 Td 59.953704 Tz (Hydrogen ) Tj 3.072222 0 Td 57.685185 Tz (atoms ) Tj 1.944444 0 Td 59.143519 Tz (were ) Tj 1.633333 0 Td 50 Tz (located ) Tj 2.294444 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 48.287037 Tz (difference ) Tj 3.052778 0 Td 49.016204 Tz (electron ) Tj 2.586111 0 Td 49.537037 Tz (density ) Tj 51.428571 0 0 51.428571 0 586.947368 Tm 25.2 0 Td 63.194444 Tz (maps ) Tj 1.769444 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 48.148148 Tz (refined ) Tj 2.255556 0 Td 46.450617 Tz (freely ) Tj 1.905556 0 Td 51.851852 Tz (as ) Tj 0.875 0 Td 46.8107 Tz (isotropic ) Tj 2.761111 0 Td 47.115385 Tz (contributors. ) Tj 3.908333 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 42.12963 Tz (final ) Tj 51.428571 0 0 51.428571 0 546.934132 Tm 25.2 0 Td 48.905724 Tz (anisotropic ) Tj 3.538889 0 Td 47.43266 Tz (full-matrix ) Tj 3.441667 0 Td 48.112536 Tz (least-squares ) Tj 4.083333 0 Td 51.527778 Tz (refinement ) Tj 3.402778 0 Td 56.17284 Tz (converged ) Tj 40 0 0 40 0 509 Tm 32.4 0 Td 58.333333 Tz (at ) Tj 0.95 0 Td 79.166667 Tz (R1 ) Tj 1.025 0 Td 81.25 Tz (=4.78% ) Tj 3.2 0 Td 61.111111 Tz (for ) Tj 1.325 0 Td 62.5 Tz (the ) Tj 1.35 0 Td 69.791667 Tz (observed ) Tj 3.6 0 Td 63.541667 Tz (data ) Tj 1.775 0 Td 73.611111 Tz (and ) Tj 1.6 0 Td 85.416667 Tz (wR2=12.36% ) Tj 5.4 0 Td 61.111111 Tz (for ) Tj 1.325 0 Td 50 Tz (all ) Tj 51.428571 0 0 51.428571 0 461.082603 Tm 25.2 0 Td 45.37037 Tz (data. ) Tj 1.594444 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 45.775463 Tz (crystals ) Tj 2.411111 0 Td 48.611111 Tz (also ) Tj 1.4 0 Td 50.462963 Tz (contain ) Tj 2.333333 0 Td 58.333333 Tz (a ) Tj 0.563889 0 Td 52.5 Tz (small ) Tj 1.808333 0 Td 51.311728 Tz (region ) Tj 2.080556 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 51.527778 Tz (disordered ) Tj 51.428571 0 0 51.428571 0 419.669211 Tm 25.219444 0 Td 50 Tz (solvent ) Tj 2.333333 0 Td 44.560185 Tz (that ) Tj 1.341667 0 Td 53.796296 Tz (could ) Tj 1.886111 0 Td 50.771605 Tz (not ) Tj 1.147222 0 Td 58.333333 Tz (be ) Tj 0.952778 0 Td 51.041667 Tz (well ) Tj 1.497222 0 Td 48.251029 Tz (resolved. ) Tj 2.838889 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 48.316498 Tz (disposition ) Tj 3.441667 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 380.740741 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.225 0 Td 49.016204 Tz (electron ) Tj 2.702778 0 Td 49.537037 Tz (density ) Tj 2.45 0 Td 43.75 Tz (in ) Tj 0.855556 0 Td 46.990741 Tz (that ) Tj 1.458333 0 Td 50.771605 Tz (region ) Tj 2.197222 0 Td 49.016204 Tz (strongly ) Tj 2.702778 0 Td 51.041667 Tz (suggests ) Tj 2.8 0 Td 59.41358 Tz (two ) Tj 51.428571 0 0 51.428571 0 337.698565 Tm 25.2 0 Td 49.826389 Tz (chlorine ) Tj 2.527778 0 Td 58.333333 Tz (atoms ) Tj 1.925 0 Td 58.333333 Tz (of ) Tj 0.758333 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 55.812757 Tz (methylene ) Tj 3.208333 0 Td 49.421296 Tz (chloride ) Tj 2.547222 0 Td 55.497685 Tz (molecule ) Tj 2.819444 0 Td 45.37037 Tz (at ) Tj 0.680556 0 Td 58.796296 Tz (approxi ) Tj 51.428571 0 0 51.428571 0 297.678877 Tm 25.2 0 Td 54.012346 Tz (mately ) Tj 2.197222 0 Td 72.376543 Tz (40% ) Tj 1.555556 0 Td 53.796296 Tz (occupancy, ) Tj 3.441667 0 Td 52.932099 Tz (but ) Tj 1.127778 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 53.098291 Tz (corresponding ) Tj 4.355556 0 Td 54.552469 Tz (carbon ) Tj 2.158333 0 Td 61.574074 Tz (atom ) Tj 51.428571 0 0 51.428571 0 251.922699 Tm 25.2 0 Td 53.796296 Tz (could ) Tj 1.827778 0 Td 49.691358 Tz (not ) Tj 1.05 0 Td 56.712963 Tz (be ) Tj 0.855556 0 Td 46.990741 Tz (located. ) Tj 2.411111 0 Td 64.814815 Tz (The ) Tj 1.341667 0 Td 50.555556 Tz (disordered ) Tj 3.227778 0 Td 50.771605 Tz (region ) Tj 2.022222 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 47.222222 Tz (treated ) Tj 2.177778 0 Td 53.472222 Tz (with ) Tj 51.428571 0 0 51.428571 0 211.992528 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 51.851852 Tz (help ) Tj 1.477778 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 76.851852 Tz (SQUEEZE ) Tj 3.441667 0 Td 55.092593 Tz (program, ) Tj 2.877778 0 Td 48.611111 Tz (therefore ) Tj 2.858333 0 Td 58.333333 Tz (no ) Tj 0.933333 0 Td 57.685185 Tz (atoms ) Tj 1.925 0 Td 51.851852 Tz (are ) Tj 51.428571 0 0 51.428571 0 168.507614 Tm 25.2 0 Td 59.722222 Tz (modeled ) Tj 2.819444 0 Td 44.830247 Tz (there. ) Tj 1.983333 0 Td 69.135802 Tz (SQUEEZEs ) Tj 4.063889 0 Td 50.636574 Tz (estimate ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 59.953704 Tz (32 ) Tj 1.030556 0 Td 48.611111 Tz (electrons ) Tj 2.955556 0 Td 54.012346 Tz (per ) Tj ET Q endstream endobj 286 0 obj << /Length 1 >> 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) Tj 2.547222 0 Td 46.990741 Tz (at ) Tj 0.738889 0 Td 72.376543 Tz (38% ) Tj 1.497222 0 Td 57.613169 Tz (occupancy ) Tj 3.305556 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 54.282407 Tz (formulae ) Tj 2.761111 0 Td 61.574074 Tz (and ) Tj 51.428571 0 0 51.428571 0 2834.432161 Tm 6.261111 0 Td 52.314815 Tz (derived ) Tj 2.488889 0 Td 53.148148 Tz (parameters ) Tj 3.558333 0 Td 49.826389 Tz (reported ) Tj 2.702778 0 Td 50.231481 Tz (herein ) Tj 2.158333 0 Td 43.055556 Tz (reflect ) Tj 2.138889 0 Td 45.37037 Tz (that ) Tj 1.419444 0 Td 49.907407 Tz (interpreta ) Tj 40 0 0 40 0 2786.363636 Tm 8.025 0 Td 55.833333 Tz (tion. ) Tj 26.175 0 Td 63.194444 Tz (Scheme ) Tj 2.475 0 Td 41.666667 Tz (3. ) Tj 0.725 0 Td 51.388889 Tz (Synthesis ) Tj 2.975 0 Td 56.25 Tz (of ) Tj 0.875 0 Td 86.904762 Tz (DIQ-Bpy ) Tj 3.925 0 Td 55.555556 Tz (Ligand ) Tj 2.175 0 Td 59.722222 Tz (and ) Tj 1.275 0 Td 55.769231 Tz (Ru-complexes. ) Tj 48.701299 0 0 48.701299 0 2755.726811 Tm 7.392 0 Td 66.162963 Tz (The ) Tj 1.3552 0 Td 48.888889 Tz (crystal ) Tj 2.238133 0 Td 49.432099 Tz (structure ) Tj 2.8336 0 Td 58.177778 Tz (has ) Tj 1.211467 0 Td 60.744444 Tz (been ) Tj 1.642667 0 Td 54.755556 Tz (deposited ) Tj 3.121067 0 Td 46.2 Tz (at ) Tj 0.7392 0 Td 52.474074 Tz (the ) Tj 1.1088 0 Td 63.501235 Tz (Cambridge ) Tj 4.045067 0 Td 41.066667 Tz (5 ) Tj 2.2176 0 Td 2628.266667 Tz (o ) Tj 51.428571 0 0 51.428571 0 2701 Tm 6.261111 0 Td 50.231481 Tz (Crystallographic ) Tj 5.152778 0 Td 55.902778 Tz (Data ) Tj 1.613889 0 Td 54.552469 Tz (Centre ) Tj 2.236111 0 Td 53.472222 Tz (with ) Tj 1.555556 0 Td 50.771605 Tz (the ) Tj 1.186111 0 Td 50.231481 Tz (deposition ) Tj 3.344444 0 Td 55.555556 Tz (number: ) Tj 51.428571 0 0 51.428571 0 2656.028571 Tm 6.261111 0 Td 83.449074 Tz (CCDC ) Tj 2.255556 0 Td 56.481481 Tz (860449, ) Tj 2.683333 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 54.282407 Tz (chemical ) Tj 2.877778 0 Td 60.493827 Tz (and ) Tj 1.361111 0 Td 45.833333 Tz (crystal ) Tj 2.236111 0 Td 49.421296 Tz (data ) Tj 1.477778 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 58.333333 Tz (which ) Tj 2.061111 0 Td 38.888889 Tz (is ) Tj 51.428571 0 0 51.428571 0 2618.070671 Tm 6.261111 0 Td 51.851852 Tz (presented ) Tj 3.052778 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 54.444444 Tz (Table ) Tj 1.827778 0 Td 45.37037 Tz (3: ) Tj 31.428571 0 0 31.428571 0 2720 Tm 48.395455 0 Td 76.893939 Tz (Br ) Tj 35.714286 0 0 35.714286 0 2537.012422 Tm 19.516 0 Td 109.2 Tz (TABLE ) Tj 3.64 0 Td 79.333333 Tz (3 ) Tj 11.704 0 Td 63 Tz (10 ) Tj 40 0 0 40 0 2464.577586 Tm 9.75 0 Td 57.8125 Tz (Chemical ) Tj 3 0 Td 59.722222 Tz (and ) Tj 1.325 0 Td 50 Tz (Crystal ) Tj 2.4 0 Td 54.166667 Tz (Data ) Tj 1.575 0 Td 56.25 Tz (of ) Tj 1.025 0 Td 59.722222 Tz (Co\(DPA-Bpy\)\(CI\) ) Tj 5.625 0 Td 75.925926 Tz (Cl2\(CHCN\) ) Tj 30 0 0 30 0 2435 Tm 22.766667 0 Td 109.722222 Tz (CCDC ) Tj 2.966667 0 Td 80.555556 Tz (86O449 ) Tj 34.285714 0 0 34.285714 0 2365.682505 Tm 16.858333 0 Td 69.444444 Tz (Formula ) Tj 9.7125 0 Td 61.426768 Tz (C25.38H24.76Cl3.76CoN6 ) Tj 29.079167 0 Td 82.638889 Tz (DIPEA ) Tj 36.666667 0 0 36.666667 0 2322.918033 Tm 33.954545 0 Td 59.090909 Tz (15 ) Tj 16.118182 0 Td 78.282828 Tz (CH3CN:THF ) Tj 4.472727 0 Td 47.727273 Tz (\(1:1\), ) Tj 27.857143 0 0 27.857143 0 2306.4375 Tm 20.712821 0 Td 80.769231 Tz (Mol. ) Tj 2.297436 0 Td 71.794872 Tz (wt. ) Tj 13.282051 0 Td 76.780627 Tz (606.OS ) Tj 36.005128 0 Td 53.846154 Tz (0 ) Tj 38.77551 0 0 38.77551 0 2277.463007 Tm 13.926316 0 Td 51.578947 Tz (Crystal ) Tj 2.398421 0 Td 58.026316 Tz (system ) Tj 9.464737 0 Td 47.280702 Tz (Triclinic ) Tj 22.178947 0 Td 37.251462 Tz (rt, ) Tj 0.876842 0 Td 60.175439 Tz (2 ) Tj 0.541579 0 Td 52.438596 Tz (days, ) Tj 1.753684 0 Td 77.368421 Tz (75% ) Tj 35.714286 0 0 35.714286 0 2240 Tm 15.54 0 Td 64.4 Tz (Space ) Tj 2.184 0 Td 63.466667 Tz (group ) Tj 11.144 0 Td 56 Tz (P-1 ) Tj 42.857143 0 0 42.857143 0 2201 Tm 13.906667 0 Td 50.555556 Tz (a ) Tj 0.56 0 Td 49.259259 Tz (\(A\) ) Tj 8.843333 0 Td 49.907407 Tz (9.2901 ) Tj 2.216667 0 Td 42.777778 Tz (\(2\) ) Tj 42.857143 0 0 42.857143 0 2168 Tm 13.883333 0 Td 54.444444 Tz (b ) Tj 0.583333 0 Td 50.555556 Tz (\(A\) ) Tj 8.563333 0 Td 50.555556 Tz (11.1802 ) Tj 2.473333 0 Td 44.074074 Tz (\(2\) ) Tj 40.285714 0 0 40.285714 0 2134.436893 Tm 14.794326 0 Td 53.782506 Tz (c ) Tj 0.595745 0 Td 52.403467 Tz (\(A\) ) Tj 9.085106 0 Td 54.964539 Tz (13.9726 ) Tj 2.680851 0 Td 45.508274 Tz (\(3\) ) Tj 3.698582 0 Td 59.98818 Tz (2O ) Tj 37.142857 0 0 37.142857 0 2101.745342 Tm 16.396154 0 Td 44.871795 Tz (Cu ) Tj 10.096154 0 Td 60.25641 Tz (70.0560 ) Tj 2.961538 0 Td 52.724359 Tz (\(10\) ) Tj 40 0 0 40 0 2068 Tm 15.3 0 Td 47.916667 Tz (B/ ) Tj 9.325 0 Td 55.357143 Tz (81.9510 ) Tj 2.725 0 Td 48.958333 Tz (\(10\) ) Tj 40.47619 0 0 40.47619 0 2035.901163 Tm 15.12 0 Td 63.823529 Tz (yo ) Tj 9.190588 0 Td 55.294118 Tz (74.7420 ) Tj 2.717647 0 Td 48.382353 Tz (\(10\) ) Tj 42.857143 0 0 42.857143 0 2002 Tm 13.58 0 Td 81.666667 Tz (V ) Tj 0.723333 0 Td 58.333333 Tz (\(A3\) ) Tj 8.703333 0 Td 51.111111 Tz (1314.12 ) Tj 2.496667 0 Td 44.074074 Tz (\(5\) ) Tj 30 0 0 30 0 1974 Tm 20.6 0 Td 52.777778 Tz (Z. ) Tj 14.033333 0 Td 77.777778 Tz (2 ) Tj 41.190476 0 0 41.190476 0 1938.61326 Tm 12.939884 0 Td 52.601156 Tz (Density ) Tj 2.427746 0 Td 60.019268 Tz (\(g/cm\) ) Tj 9.905202 0 Td 50.982659 Tz (1.532 ) Tj 9.079769 0 Td 194.219653 Tz (N ) Tj 3.957225 0 Td 93.063584 Tz (N ) Tj 4.442775 0 Td 194.219653 Tz (N ) Tj 39.428571 0 0 39.428571 0 1905.24 Tm 13.01087 0 Td 58.121981 Tz (Abs. ) Tj 1.648551 0 Td 45.793076 Tz (coeff. ) Tj 1.902174 0 Td 92.995169 Tz (\(mm\) ) Tj 9.815217 0 Td 54.10628 Tz (8.857 ) Tj 5.148551 0 Td 59.178744 Tz (25 ) Tj 31.428571 0 0 31.428571 0 1873.251462 Tm 17.054545 0 Td 71.590909 Tz (AbS. ) Tj 2.068182 0 Td 62.575758 Tz (correction ) Tj 12.313636 0 Td 65.757576 Tz (multi-scan ) Tj 15.081818 0 Td 121.969697 Tz (N ) Tj 7.35 0 Td 121.969697 Tz (N ) Tj 38.571429 0 0 38.571429 0 1838.66129 Tm 15.27037 0 Td 56.17284 Tz (F\(000\) ) Tj 10.940741 0 Td 60.493827 Tz (62O ) Tj 10.422222 0 Td 181.481481 Tz (2 ) Tj 8.996296 0 Td 110.185185 Tz (21 ) Tj 4.122222 0 Td 57.613169 Tz (RuCl3, ) Tj 2.307407 0 Td 63.08642 Tz (3H2O, ) Tj 2.125926 0 Td 73.45679 Tz (EtOH ) Tj 29.285714 0 0 29.285714 0 1813.28 Tm 17.004878 0 Td 66.01626 Tz (Total ) Tj 2.42439 0 Td 62.601626 Tz (no. ) Tj 1.536585 0 Td 79.674797 Tz (of ) Tj 1.160976 0 Td 62.601626 Tz (reflection ) Tj 11.439024 0 Td 79.674797 Tz (15946 ) Tj 31.790244 0 Td 392.682927 Tz (Hops ) Tj 37.792208 0 0 37.792208 0 1775.947589 Tm 13.230241 0 Td 50.715922 Tz (Reflections, ) Tj 3.916151 0 Td 44.100802 Tz (I ) Tj 0.608591 0 Td 57.331042 Tz (> ) Tj 0.635052 0 Td 63.946163 Tz (20 ) Tj 0.846735 0 Td 39.690722 Tz (\(I\) ) Tj 7.064948 0 Td 66.151203 Tz (4474 ) Tj 15.161856 0 Td 101.431844 Tz (N ) Tj 9.710997 0 Td 49.140893 Tz (reflux, ) Tj 2.328522 0 Td 57.331042 Tz (12 ) Tj 0.926117 0 Td 46.305842 Tz (h, ) Tj 0.767354 0 Td 76.44139 Tz (77% ) Tj 30.952381 0 0 30.952381 0 1742 Tm 18.350769 0 Td 79.423077 Tz (Max. ) Tj 2.261538 0 Td 59.230769 Tz (20. ) Tj 12.470769 0 Td 71.794872 Tz (71.540 ) Tj 34.714286 0 0 34.714286 0 1707.304054 Tm 15.353909 0 Td 67.215364 Tz (Ranges ) Tj 2.736626 0 Td 48.010974 Tz (\(h, ) Tj 1.152263 0 Td 52.812071 Tz (k, ) Tj 0.979424 0 Td 50.411523 Tz (1\) ) Tj 7.720165 0 Td 67.215364 Tz (-11 ) Tj 1.526749 0 Td 72.016461 Tz (s ) Tj 0.806584 0 Td 57.613169 Tz (h ) Tj 0.633745 0 Td 36.00823 Tz (is ) Tj 0.835391 0 Td 62.414266 Tz (10 ) Tj 4.061728 0 Td 69.615912 Tz (30 ) Tj 31.428571 0 0 31.428571 0 1676.916667 Tm 30.863636 0 Td 79.545455 Tz (-13 ) Tj 1.718182 0 Td 114.89899 Tz (sks ) Tj 2.513636 0 Td 60.984848 Tz (11 ) Tj 17.754545 0 Td 121.969697 Tz (N ) Tj 47.142857 0 0 47.142857 0 1639.222222 Tm 20.639394 0 Td 60.984848 Tz (-17s ) Tj 1.781818 0 Td 49.494949 Tz (is ) Tj 0.890909 0 Td 47.727273 Tz (17 ) Tj 10.563636 0 Td 70.707071 Tz (| ) Tj 1.69697 0 Td 127.272727 Tz (N ) Tj 38 0 0 38 0 1604.784615 Tm 13.394737 0 Td 61.951754 Tz (Complete ) Tj 3.184211 0 Td 52.631579 Tz (to ) Tj 0.894737 0 Td 63.596491 Tz (20 ) Tj 1.026316 0 Td 62.865497 Tz (\(%\) ) Tj 8.447368 0 Td 55.921053 Tz (95.0 ) Tj 35.714286 0 0 35.714286 0 1571.622912 Tm 13.328 0 Td 65.333333 Tz (Data ) Tj 1.736 0 Td 46.666667 Tz (restraints, ) Tj 3.22 0 Td 59.266667 Tz (parameters ) Tj 9.212 0 Td 57.866667 Tz (4874. ) Tj 1.876 0 Td 49 Tz (Of ) Tj 0.644 0 Td 66.888889 Tz (412 ) Tj 36.666667 0 0 36.666667 0 1537.16 Tm 15.490909 0 Td 71.590909 Tz (Goof ) Tj 1.909091 0 Td 55.681818 Tz (\(F2\) ) Tj 10.990909 0 Td 57.272727 Tz (1.OSO ) Tj 37.777778 0 0 37.777778 0 1510.284382 Tm 13.341176 0 Td 88.235294 Tz (R ) Tj 0.767647 0 Td 51.680672 Tz (indices ) Tj 2.726471 0 Td 39.705882 Tz (I ) Tj 0.741176 0 Td 30.882353 Tz (- ) Tj 0.45 0 Td 66.176471 Tz (20 ) Tj 0.873529 0 Td 39.705882 Tz (\(I\) ) Tj 8.602941 0 Td 49.789916 Tz (O.O.478 ) Tj 5.4 0 Td 61.764706 Tz (35 ) Tj 7.2 0 Td 92.647059 Tz (DIQ-Bpy ) Tj 38 0 0 38 0 1469.73913 Tm 13.526316 0 Td 87.719298 Tz (R ) Tj 0.763158 0 Td 51.378446 Tz (indices ) Tj 2.473684 0 Td 40.570175 Tz (\(all ) Tj 1.236842 0 Td 50 Tz (data\) ) Tj 9.342105 0 Td 58.479532 Tz (O.OS14 ) Tj 36.666667 0 0 36.666667 0 1437.246445 Tm 15.163636 0 Td 77.272727 Tz (wR2 ) Tj 1.663636 0 Td 52.597403 Tz (indices ) Tj 11.509091 0 Td 59.848485 Tz (O.1236 ) Tj 44.285714 0 0 44.285714 0 1287.314917 Tm 15.580645 0 Td 70.967742 Tz (Example ) Tj 3.229032 0 Td 71.505376 Tz (8 ) Tj 9.235484 0 Td 56.451613 Tz (40 ) Tj 51.428571 0 0 51.428571 0 1179.801835 Tm 8.905556 0 Td 62.654321 Tz (The ) Tj 1.380556 0 Td 51.851852 Tz (H. ) Tj 1.069444 0 Td 51.851852 Tz (Evolution ) Tj 3.013889 0 Td 49.421296 Tz (Activity ) Tj 2.625 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 63.425926 Tz (Complex ) Tj 2.897222 0 Td 55.092593 Tz (3 ) Tj 51.428571 0 0 51.428571 0 1089.288243 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 87.5 Tz (H ) Tj 0.991667 0 Td 50.771605 Tz (evolution ) Tj 2.955556 0 Td 45.775463 Tz (activity ) Tj 2.411111 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 60.185185 Tz (complex ) Tj 2.741667 0 Td 55.092593 Tz (3 ) Tj 0.583333 0 Td 62.654321 Tz (was ) Tj 1.361111 0 Td 48.881173 Tz (investigated ) Tj 3.927778 0 Td 46.990741 Tz (45 ) Tj 51.428571 0 0 51.428571 0 1043 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 55.092593 Tz (a ) Tj 0.719444 0 Td 59.62963 Tz (mixed ) Tj 2.119444 0 Td 50 Tz (solvent ) Tj 2.411111 0 Td 59.953704 Tz (of ) Tj 1.030556 0 Td 75.462963 Tz (EtOH/HO ) Tj 3.538889 0 Td 46.018519 Tz (\(1:1\) ) Tj 1.730556 0 Td 55.740741 Tz (under ) Tj 2.002778 0 Td 46.254209 Tz (irradiation ) Tj 51.428571 0 0 51.428571 0 1005.701643 Tm 6.280556 0 Td 68.055556 Tz (\(LED ) Tj 1.827778 0 Td 41.589506 Tz (light, ) Tj 1.691667 0 Td 61.574074 Tz (520 ) Tj 1.283333 0 Td 62.654321 Tz (nm\) ) Tj 1.302778 0 Td 51.527778 Tz (containing ) Tj 3.286111 0 Td 55.092593 Tz (5 ) Tj 0.544444 0 Td 81.018519 Tz (uM ) Tj 1.127778 0 Td 60.185185 Tz (complex ) Tj 2.683333 0 Td 46.990741 Tz (3, ) Tj 0.738889 0 Td 58.333333 Tz (2 ) Tj 0.583333 0 Td 98.842593 Tz (mM ) Tj 1.361111 0 Td 55.092593 Tz (FL, ) Tj 58.571429 0 0 58.571429 0 960 Tm 5.497561 0 Td 51.219512 Tz (and ) Tj 1.126829 0 Td 61.653117 Tz (10% ) Tj 1.229268 0 Td 58.333333 Tz (TEA, ) Tj 1.570732 0 Td 46.95122 Tz (with ) Tj 1.263415 0 Td 48.373984 Tz (a ) Tj 0.426829 0 Td 73.03523 Tz (TON ) Tj 1.468293 0 Td 49.796748 Tz (of ) Tj 0.665854 0 Td 54.065041 Tz (2000 ) Tj 1.45122 0 Td 54.065041 Tz (mol ) Tj 1.160976 0 Td 45.528455 Tz (H. ) Tj 0.836585 0 Td 48.373984 Tz (\(mol ) Tj 1.331707 0 Td 47.804878 Tz (cat\)' ) Tj 1.639024 0 Td 39.837398 Tz (after ) Tj 51.428571 0 0 51.428571 0 922.983979 Tm 6.261111 0 Td 61.574074 Tz (30 ) Tj 1.069444 0 Td 58.333333 Tz (h ) Tj 0.7 0 Td 48.021886 Tz (photolysis, ) Tj 3.538889 0 Td 71.296296 Tz (-25% ) Tj 2.080556 0 Td 61.574074 Tz (more ) Tj 1.808333 0 Td 51.851852 Tz (than ) Tj 1.594444 0 Td 46.180556 Tz (that ) Tj 1.419444 0 Td 56.712963 Tz (of ) Tj 1.166667 0 Td 61.868687 Tz (Ni\(DPA-Bpy\) ) Tj 47.857143 0 0 47.857143 0 877.293919 Tm 6.749254 0 Td 74.295191 Tz (\(H2O\)\(BF\) ) Tj 4.555224 0 Td 59.20398 Tz (under ) Tj 2.00597 0 Td 53.399668 Tz (the ) Tj 1.191045 0 Td 67.039801 Tz (same ) Tj 1.880597 0 Td 51.605608 Tz (conditions. ) Tj 9.591045 0 Td 50.497512 Tz (50 ) Tj 51.428571 0 0 51.428571 0 785.993377 Tm 13.416667 0 Td 61.111111 Tz (Example ) Tj 2.780556 0 Td 61.574074 Tz (9 ) Tj 48.367347 0 0 48.367347 0 678.309942 Tm 8.497468 0 Td 62.025316 Tz (Water ) Tj 2.088186 0 Td 57.047976 Tz (Oxidation ) Tj 3.349367 0 Td 63.748242 Tz (by ) Tj 1.033755 0 Td 55.133615 Tz (a ) Tj 0.620253 0 Td 62.651835 Tz (Mononuclear ) Tj 4.424473 0 Td 62.791061 Tz (Ruthenium ) Tj 5.685654 0 Td 48.241913 Tz (55 ) Tj 51.428571 0 0 51.428571 0 638.673171 Tm 10.636111 0 Td 63.425926 Tz (Complex ) Tj 2.916667 0 Td 52.662037 Tz (with ) Tj 1.497222 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 51.58179 Tz (Pentadentate ) Tj 51.428571 0 0 51.428571 0 602 Tm 10.519444 0 Td 50.378788 Tz (Isoquinoline-Bipyridyl ) Tj 6.941667 0 Td 56.712963 Tz (Ligand ) Tj 51.428571 0 0 51.428571 0 506.152174 Tm 7 0 Td 62.789352 Tz (Compared ) Tj 3.402778 0 Td 46.990741 Tz (to ) Tj 0.952778 0 Td 48.611111 Tz (pyridine, ) Tj 3.052778 0 Td 49.691358 Tz (isoquinoline ) Tj 3.986111 0 Td 37.268519 Tz (is ) Tj 0.875 0 Td 61.574074 Tz (more ) Tj 1.847222 0 Td 54.282407 Tz (electron ) Tj 51.428571 0 0 51.428571 0 463.988124 Tm 6.241667 0 Td 56.271044 Tz (withdrawing ) Tj 3.927778 0 Td 47.685185 Tz (ligand. ) Tj 2.236111 0 Td 61.574074 Tz (To ) Tj 0.991667 0 Td 53.240741 Tz (provide ) Tj 2.469444 0 Td 46.990741 Tz (insights ) Tj 2.508333 0 Td 46.180556 Tz (into ) Tj 1.361111 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 47.962963 Tz (electronic ) Tj 3.344444 0 Td 45.37037 Tz (60 ) Tj 51.428571 0 0 51.428571 0 420.977191 Tm 6.261111 0 Td 44.830247 Tz (effect ) Tj 1.769444 0 Td 49.96142 Tz (isoquinoline ) Tj 3.713889 0 Td 61.574074 Tz (on ) Tj 0.913889 0 Td 48.611111 Tz (the ) Tj 0.991667 0 Td 51.131687 Tz (oxidation ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 48.611111 Tz (water, ) Tj 1.905556 0 Td 71.296296 Tz (we ) Tj 1.030556 0 Td 50.636574 Tz (replaced ) Tj 2.586111 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 383.740741 Tm 6.261111 0 Td 50.636574 Tz (pyridine ) Tj 2.625 0 Td 55.092593 Tz (groups ) Tj 2.216667 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 50.605413 Tz (\(N.N-bis\(2-pyridinylmethyl\)-2,2'-bipyri ) Tj 51.428571 0 0 51.428571 0 337.392902 Tm 6.261111 0 Td 55.092593 Tz (dine-6-methanamine\) ) Tj 6.591667 0 Td 61.574074 Tz (\(DPA-Bpy\) ) Tj 3.616667 0 Td 46.990741 Tz (to ) Tj 0.894444 0 Td 48.070988 Tz (afford ) Tj 2.022222 0 Td 55.092593 Tz (a ) Tj 0.680556 0 Td 63.734568 Tz (new ) Tj 1.497222 0 Td 52.662037 Tz (type ) Tj 1.555556 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 301 Tm 6.261111 0 Td 51.311728 Tz (pentadentate ) Tj 4.141667 0 Td 47.222222 Tz (ligand, ) Tj 2.488889 0 Td 51.574074 Tz (N.N-bis\(isoquinolin-1-yl\)methyl\)\(6- ) Tj 51.428571 0 0 51.428571 0 258.036364 Tm 6.280556 0 Td 51.169591 Tz (\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 12.075 0 Td 56.388889 Tz (\(DIQ-Bpy\). ) Tj 3.811111 0 Td 51.851852 Tz (Here, ) Tj 2.041667 0 Td 42.12963 Tz (65 ) Tj 51.428571 0 0 51.428571 0 213.294675 Tm 6.241667 0 Td 72.916667 Tz (we ) Tj 1.030556 0 Td 48.611111 Tz (report ) Tj 1.886111 0 Td 50.771605 Tz (the ) Tj 1.05 0 Td 46.990741 Tz (synthesis, ) Tj 2.994444 0 Td 47.086057 Tz (characterization, ) Tj 4.977778 0 Td 58.333333 Tz (and ) Tj 1.166667 0 Td 45.775463 Tz (activity ) Tj 2.352778 0 Td 48.148148 Tz (studies ) Tj 51.428571 0 0 51.428571 0 174.907801 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 66.435185 Tz (Ru ) Tj 1.05 0 Td 57.253086 Tz (complexes ) Tj 3.363889 0 Td 52.572016 Tz (supported ) Tj 3.072222 0 Td 59.953704 Tz (by ) Tj 1.030556 0 Td 58.738426 Tz (DIQ-Bpy. ) Tj 1.428571 0 0 1.428571 0 1347 Tm 983.5 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 288 0 obj << /Length 1 >> stream q endstream endobj 289 0 obj << /Length 38800 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.113514 0 Td 77.252252 Tz (29 ) Tj 40 0 0 40 0 2913 Tm 17.35 0 Td 67.083333 Tz (-continued ) Tj 51.428571 0 0 51.428571 0 2238.561713 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 64.351852 Tz (DIQ-Bpy ) Tj 2.877778 0 Td 50.771605 Tz (ligand ) Tj 2.022222 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 51.262626 Tz (synthesized ) Tj 3.558333 0 Td 52.211934 Tz (following ) Tj 2.975 0 Td 56.712963 Tz (an ) Tj 0.875 0 Td 60.277778 Tz (analo ) Tj 51.428571 0 0 51.428571 0 2194.829091 Tm 6.261111 0 Td 55.902778 Tz (gous ) Tj 1.536111 0 Td 54.372428 Tz (procedure ) Tj 3.130556 0 Td 55.092593 Tz (used ) Tj 1.497222 0 Td 48.611111 Tz (for ) Tj 1.030556 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 48.611111 Tz (synthesis ) Tj 2.819444 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 66.203704 Tz (DPA-Bpy ) Tj 2.994444 0 Td 60.648148 Tz (\(Scheme ) Tj 51.428571 0 0 51.428571 0 2150.282927 Tm 6.261111 0 Td 43.209877 Tz (3\), ) Tj 1.05 0 Td 57.523148 Tz (from ) Tj 1.672222 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 48.206019 Tz (reaction ) Tj 2.566667 0 Td 61.574074 Tz (of ) Tj 0.933333 0 Td 52.692044 Tz (1-\(bromomethyl\)isoquinoline ) Tj 8.827778 0 Td 54.282407 Tz (with ) Tj 51.428571 0 0 51.428571 0 2109.294947 Tm 6.280556 0 Td 50.903342 Tz (\(6-\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 12.813889 0 Td 46.990741 Tz (in ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.186111 0 Td 53.472222 Tz (presence ) Tj 51.428571 0 0 51.428571 0 2060.329609 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.933333 0 Td 55.092593 Tz (base ) Tj 1.672222 0 Td 44.290123 Tz (\(Y. ) Tj 1.205556 0 Td 45.37037 Tz (Hirai, ) Tj 1.963889 0 Td 45.37037 Tz (T. ) Tj 0.952778 0 Td 55.092593 Tz (Kojima, ) Tj 2.644444 0 Td 46.990741 Tz (Y. ) Tj 0.952778 0 Td 51.49177 Tz (Mizutani, ) Tj 3.111111 0 Td 50.231481 Tz (Y. ) Tj 0.952778 0 Td 48.148148 Tz (Shiota, ) Tj 2.411111 0 Td 53.472222 Tz (K. ) Tj 51.428571 0 0 51.428571 0 2016.114428 Tm 6.261111 0 Td 55.740741 Tz (Yoshizawa, ) Tj 3.538889 0 Td 46.990741 Tz (S. ) Tj 0.797222 0 Td 57.613169 Tz (Fukuzumi, ) Tj 3.305556 0 Td 60.493827 Tz (Angew. ) Tj 2.411111 0 Td 68.703704 Tz (Chem. ) Tj 2.333333 0 Td 38.888889 Tz (Int. ) Tj 1.186111 0 Td 51.851852 Tz (Ed. ) Tj 1.166667 0 Td 53.796296 Tz (2008, ) Tj 1.808333 0 Td 49.691358 Tz (47. ) Tj 51.428571 0 0 51.428571 0 1972 Tm 6.280556 0 Td 53.619529 Tz (5772-5776\). ) Tj 3.811111 0 Td 61.574074 Tz (Slow ) Tj 1.75 0 Td 50.231481 Tz (addition ) Tj 2.663889 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 59.953704 Tz (an ) Tj 0.952778 0 Td 51.388889 Tz (ethanol ) Tj 2.430556 0 Td 49.016204 Tz (solution ) Tj 2.586111 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 84.259259 Tz (DIQ ) Tj 51.428571 0 0 51.428571 0 1928.57971 Tm 6.280556 0 Td 64.814815 Tz (Bpy ) Tj 1.341667 0 Td 45.37037 Tz (to ) Tj 0.719444 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 49.016204 Tz (refluxed ) Tj 2.508333 0 Td 48.206019 Tz (solution ) Tj 2.45 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 68.055556 Tz (RuC1.3H2O ) Tj 3.811111 0 Td 46.990741 Tz (in ) Tj 0.719444 0 Td 50.925926 Tz (ethanol ) Tj 2.313889 0 Td 48.206019 Tz (resulted ) Tj 51.428571 0 0 51.428571 0 1887.138614 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.816667 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 52.572016 Tz (formation ) Tj 3.072222 0 Td 59.953704 Tz (of ) Tj 1.088889 0 Td 60.430283 Tz (Ru\(DIQ-Bpy\)\(Cl\)C1 ) Tj 6.397222 0 Td 42.12963 Tz (\(6\). ) Tj 1.225 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 50.231481 Tz (addition ) Tj 52.857143 0 0 52.857143 0 1841.270166 Tm 6.091892 0 Td 56.756757 Tz (of ) Tj 0.851351 0 Td 47.297297 Tz (saturated ) Tj 2.8 0 Td 47.297297 Tz (solution ) Tj 2.516216 0 Td 56.756757 Tz (of ) Tj 0.832432 0 Td 87.5 Tz (NHPF ) Tj 2.610811 0 Td 44.144144 Tz (to ) Tj 0.775676 0 Td 56.756757 Tz (an ) Tj 0.908108 0 Td 55.855856 Tz (aqueous ) Tj 2.610811 0 Td 46.903153 Tz (solution ) Tj 2.497297 0 Td 56.756757 Tz (of ) Tj 51.428571 0 0 51.428571 0 1799.393617 Tm 6.261111 0 Td 59.722222 Tz (complex ) Tj 2.897222 0 Td 55.092593 Tz (7 ) Tj 0.719444 0 Td 49.691358 Tz (led ) Tj 1.244444 0 Td 46.990741 Tz (to ) Tj 0.933333 0 Td 44.444444 Tz (partial ) Tj 2.236111 0 Td 46.990741 Tz (substitution ) Tj 3.772222 0 Td 59.953704 Tz (of ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 52.441077 Tz (coordinated ) Tj 51.428571 0 0 51.428571 0 1754.291615 Tm 6.261111 0 Td 51.311728 Tz (Cl-ion ) Tj 2.022222 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 55.092593 Tz (6 ) Tj 0.505556 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 60.763889 Tz (H2O, ) Tj 1.652778 0 Td 46.450617 Tz (resulting ) Tj 2.702778 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 52.932099 Tz (formation ) Tj 3.013889 0 Td 58.333333 Tz (of ) Tj 0.777778 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 53.240741 Tz (mixture ) Tj 52.857143 0 0 52.857143 0 1713.452442 Tm 6.091892 0 Td 56.756757 Tz (of ) Tj 0.889189 0 Td 56.756757 Tz (complexes ) Tj 3.613514 0 Td 56.966967 Tz (Ru\(DIQ-Bpy\)\(Cl\) ) Tj 5.391892 0 Td 62.274775 Tz (\(PF\) ) Tj 1.835135 0 Td 44.144144 Tz (\(7\) ) Tj 1.135135 0 Td 56.756757 Tz (and ) Tj 1.589189 0 Td 70.42042 Tz (Ru\(DIQ ) Tj 51.428571 0 0 51.428571 0 1669.014634 Tm 6.280556 0 Td 68.055556 Tz (Bpy\)\(HO\) ) Tj 3.538889 0 Td 59.62963 Tz (\(PF\), ) Tj 2.022222 0 Td 42.12963 Tz (\(5\). ) Tj 1.263889 0 Td 56.481481 Tz (Because ) Tj 2.547222 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 45.37037 Tz (different ) Tj 2.625 0 Td 45.694444 Tz (solubility ) Tj 2.936111 0 Td 58.333333 Tz (of ) Tj 52.857143 0 0 52.857143 0 1625.951654 Tm 6.091892 0 Td 56.056056 Tz (complexes ) Tj 3.272973 0 Td 53.603604 Tz (7 ) Tj 0.548649 0 Td 56.756757 Tz (and ) Tj 1.286486 0 Td 53.603604 Tz (5 ) Tj 0.567568 0 Td 45.720721 Tz (in ) Tj 0.813514 0 Td 51.501502 Tz (methanol, ) Tj 2.989189 0 Td 49.399399 Tz (the ) Tj 1.135135 0 Td 59.90991 Tz (more ) Tj 1.664865 0 Td 49.099099 Tz (soluble ) Tj 2.27027 0 Td 58.558559 Tz (complex ) Tj 51.428571 0 0 51.428571 0 1584.183599 Tm 6.280556 0 Td 55.092593 Tz (5 ) Tj 0.544444 0 Td 60.493827 Tz (was ) Tj 1.283333 0 Td 51.131687 Tz (separated ) Tj 2.936111 0 Td 52.5 Tz (using ) Tj 1.711111 0 Td 58.333333 Tz (a ) Tj 0.544444 0 Td 66.666667 Tz (minimum ) Tj 2.994444 0 Td 61.574074 Tz (amount ) Tj 2.372222 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 55.902778 Tz (methanol ) Tj 2.897222 0 Td 58.333333 Tz (from ) Tj 58.571429 0 0 58.571429 0 1543.926413 Tm 5.497561 0 Td 52.439024 Tz (complex ) Tj 2.509756 0 Td 39.837398 Tz (7. ) Tj 0.853659 0 Td 93.902439 Tz (' ) Tj 0.904878 0 Td 66.869919 Tz (NMR, ) Tj 1.963415 0 Td 51.930894 Tz (mass ) Tj 1.570732 0 Td 44.434021 Tz (spectrometry, ) Tj 3.790244 0 Td 53.116531 Tz (and ) Tj 1.263415 0 Td 45.844625 Tz (elemental ) Tj 51.428571 0 0 51.428571 0 1503.678481 Tm 6.261111 0 Td 48.611111 Tz (analysis ) Tj 2.605556 0 Td 41.049383 Tz (all ) Tj 0.991667 0 Td 55.452675 Tz (confirmed ) Tj 3.266667 0 Td 48.611111 Tz (the ) Tj 1.147222 0 Td 45.775463 Tz (identity ) Tj 2.488889 0 Td 59.41358 Tz (and ) Tj 1.302778 0 Td 48.070988 Tz (purity ) Tj 2.041667 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 64.814815 Tz (DIQ-Bpy ) Tj 51.428571 0 0 51.428571 0 1461.972973 Tm 6.261111 0 Td 50.771605 Tz (ligand ) Tj 2.041667 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 66.435185 Tz (Ru ) Tj 1.05 0 Td 57.253086 Tz (complexes ) Tj 3.344444 0 Td 46.990741 Tz (5-7. ) Tj 51.428571 0 0 51.428571 0 1419.114883 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.361111 0 Td 64.814815 Tz (DIQ-Bpy ) Tj 2.975 0 Td 50.231481 Tz (ligand ) Tj 2.022222 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 68.055556 Tz (Ru ) Tj 1.011111 0 Td 57.973251 Tz (complexes ) Tj 3.363889 0 Td 57.523148 Tz (have ) Tj 1.594444 0 Td 56.712963 Tz (been ) Tj 1.594444 0 Td 61.574074 Tz (char ) Tj 58.571429 0 0 58.571429 0 1376.695312 Tm 5.497561 0 Td 42.682927 Tz (acterized ) Tj 2.526829 0 Td 54.065041 Tz (by ) Tj 0.921951 0 Td 62.601626 Tz (1D ) Tj 0.956098 0 Td 51.219512 Tz (and ) Tj 1.126829 0 Td 68.292683 Tz (2D ) Tj 1.041463 0 Td 79.674797 Tz (NMR ) Tj 1.656098 0 Td 45.528455 Tz (experiments. ) Tj 3.482927 0 Td 56.910569 Tz (The ) Tj 1.485366 0 Td 76.829268 Tz (H ) Tj 0.682927 0 Td 81.571816 Tz (NMR ) Tj 51.428571 0 0 51.428571 0 1337.445545 Tm 6.280556 0 Td 54.6875 Tz (spectrum ) Tj 2.858333 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 58.796296 Tz (complex ) Tj 2.722222 0 Td 55.092593 Tz (5 ) Tj 0.563889 0 Td 56.712963 Tz (\(shows ) Tj 2.275 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 59.41358 Tz (two ) Tj 1.322222 0 Td 49.96142 Tz (isoquinoline ) Tj 3.772222 0 Td 55.632716 Tz (groups ) Tj 52.857143 0 0 52.857143 0 1292.892989 Tm 6.072973 0 Td 52.815315 Tz (with ) Tj 1.475676 0 Td 48.348348 Tz (the ) Tj 1.059459 0 Td 60.698198 Tz (same ) Tj 1.664865 0 Td 87.237237 Tz (NMR ) Tj 1.778378 0 Td 44.494494 Tz (features, ) Tj 2.610811 0 Td 51.081081 Tz (suggesting ) Tj 3.216216 0 Td 49.399399 Tz (the ) Tj 1.059459 0 Td 52.027027 Tz (presence ) Tj 2.705405 0 Td 53.603604 Tz (of ) Tj 0.737838 0 Td 59.90991 Tz (C. ) Tj 51.428571 0 0 51.428571 0 1253.257888 Tm 6.280556 0 Td 59.953704 Tz (symmetry ) Tj 3.266667 0 Td 48.611111 Tz (for ) Tj 1.225 0 Td 55.092593 Tz (5 ) Tj 0.7 0 Td 46.990741 Tz (in ) Tj 0.952778 0 Td 48.206019 Tz (solution ) Tj 2.683333 0 Td 54.282407 Tz (with ) Tj 1.652778 0 Td 58.333333 Tz (a ) Tj 0.680556 0 Td 53.796296 Tz (plane ) Tj 1.983333 0 Td 50.87963 Tz (containing ) Tj 3.422222 0 Td 49.691358 Tz (the ) Tj 51.428571 0 0 51.428571 0 1211.744459 Tm 6.241667 0 Td 43.75 Tz (tertiary ) Tj 2.488889 0 Td 59.62963 Tz (amine ) Tj 2.119444 0 Td 60.493827 Tz (and ) Tj 1.419444 0 Td 50.771605 Tz (the ) Tj 1.263889 0 Td 50.231481 Tz (bipyridine ) Tj 3.363889 0 Td 51.851852 Tz (group. ) Tj 2.275 0 Td 59.143519 Tz (Such ) Tj 1.827778 0 Td 45.37037 Tz (structural ) Tj 51.428571 0 0 51.428571 0 1168.791403 Tm 6.261111 0 Td 48.148148 Tz (feature ) Tj 2.197222 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 55.092593 Tz (5 ) Tj 0.544444 0 Td 38.888889 Tz (is ) Tj 0.7 0 Td 48.611111 Tz (similar ) Tj 2.216667 0 Td 43.75 Tz (to ) Tj 0.758333 0 Td 46.180556 Tz (that ) Tj 1.263889 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 66.435185 Tz (Ru ) Tj 0.991667 0 Td 60.185185 Tz (complex ) Tj 2.722222 0 Td 53.472222 Tz (with ) Tj 1.516667 0 Td 67.592593 Tz (DPA-Bpy ) Tj 51.428571 0 0 51.428571 0 1126.358604 Tm 6.261111 0 Td 51.311728 Tz (ligand ) Tj 1.983333 0 Td 58.333333 Tz (and ) Tj 1.205556 0 Td 48.287037 Tz (consistent ) Tj 3.072222 0 Td 53.472222 Tz (with ) Tj 1.438889 0 Td 49.691358 Tz (the ) Tj 1.05 0 Td 54.012346 Tz (optimized ) Tj 3.072222 0 Td 47.170782 Tz (structure ) Tj 2.702778 0 Td 57.523148 Tz (from ) Tj 1.594444 0 Td 74.537037 Tz (DFT ) Tj 51.428571 0 0 51.428571 0 1083 Tm 6.261111 0 Td 48.316498 Tz (calculation ) Tj 3.655556 0 Td 51.851852 Tz (\(FIG. ) Tj 2.080556 0 Td 51.851852 Tz (19\) ) Tj 1.4 0 Td 47.530864 Tz (\(B. ) Tj 1.380556 0 Td 57.523148 Tz (Radaram, ) Tj 3.188889 0 Td 38.888889 Tz (J. ) Tj 0.894444 0 Td 56.712963 Tz (A. ) Tj 1.205556 0 Td 42.12963 Tz (Ivie, ) Tj 1.769444 0 Td 48.611111 Tz (R. ) Tj 1.088889 0 Td 64.814815 Tz (M. ) Tj 51.428571 0 0 51.428571 0 1043.78481 Tm 6.261111 0 Td 53.292181 Tz (Grudzien, ) Tj 3.091667 0 Td 35.648148 Tz (J. ) Tj 0.680556 0 Td 55.092593 Tz (H. ) Tj 0.913889 0 Td 50.771605 Tz (Reibenspies, ) Tj 3.85 0 Td 55.092593 Tz (C. ) Tj 0.913889 0 Td 46.990741 Tz (E. ) Tj 0.797222 0 Td 51.446759 Tz (Webster, ) Tj 2.683333 0 Td 58.333333 Tz (X. ) Tj 0.933333 0 Td 55.092593 Tz (Zhao, ) Tj 1.886111 0 Td 46.990741 Tz (Inorg. ) Tj 51.428571 0 0 51.428571 0 1000 Tm 6.261111 0 Td 63.518519 Tz (Chem. ) Tj 2.119444 0 Td 53.796296 Tz (2011, ) Tj 1.808333 0 Td 49.691358 Tz (50, ) Tj 1.166667 0 Td 55.902778 Tz (10564-10571; ) Tj 4.219444 0 Td 48.611111 Tz (a\) ) Tj 0.777778 0 Td 66.435185 Tz (M. ) Tj 1.05 0 Td 53.472222 Tz (B. ) Tj 0.913889 0 Td 45.37037 Tz (Hall, ) Tj 1.613889 0 Td 50.231481 Tz (R. ) Tj 0.855556 0 Td 38.888889 Tz (F. ) Tj 0.719444 0 Td 52.314815 Tz (Fenske, ) Tj 51.428571 0 0 51.428571 0 958.995804 Tm 6.261111 0 Td 48.070988 Tz (Inorg. ) Tj 2.041667 0 Td 64.814815 Tz (Chem. ) Tj 2.333333 0 Td 51.851852 Tz (1972, ) Tj 1.963889 0 Td 44.290123 Tz (11, ) Tj 1.108333 0 Td 54.6875 Tz (768-775; ) Tj 2.955556 0 Td 50.231481 Tz (b\) ) Tj 0.952778 0 Td 50.231481 Tz (B. ) Tj 0.972222 0 Td 50.231481 Tz (E. ) Tj 0.952778 0 Td 49.826389 Tz (Bursten, ) Tj 2.741667 0 Td 37.268519 Tz (J. ) Tj 0.816667 0 Td 50.231481 Tz (R. ) Tj 51.428571 0 0 51.428571 0 917.808989 Tm 6.261111 0 Td 50.462963 Tz (Jensen, ) Tj 2.352778 0 Td 50.231481 Tz (R. ) Tj 0.855556 0 Td 42.12963 Tz (F. ) Tj 0.738889 0 Td 52.777778 Tz (Fenske, ) Tj 2.411111 0 Td 37.268519 Tz (J. ) Tj 0.661111 0 Td 63.518519 Tz (Chem. ) Tj 2.138889 0 Td 52.5 Tz (Phys. ) Tj 1.866667 0 Td 51.851852 Tz (1978, ) Tj 1.769444 0 Td 55.324074 Tz (68,3320-3321\). ) Tj 40 0 0 40 0 883 Tm 8.05 0 Td 81.944444 Tz (The ) Tj 1.675 0 Td 65.277778 Tz (coordination ) Tj 4.95 0 Td 72.916667 Tz (of ) Tj 0.975 0 Td 89.583333 Tz (Ru ) Tj 1.3 0 Td 61.458333 Tz (resulted ) Tj 3.175 0 Td 58.333333 Tz (in ) Tj 0.95 0 Td 62.5 Tz (the ) Tj 1.35 0 Td 68.981481 Tz (downfield ) Tj 3.95 0 Td 54.861111 Tz (shifts ) Tj 2.225 0 Td 72.916667 Tz (of ) Tj 0.95 0 Td 52.777778 Tz (all ) Tj 51.428571 0 0 51.428571 0 837.014475 Tm 6.241667 0 Td 49.259259 Tz (three ) Tj 1.652778 0 Td 55.812757 Tz (methylene ) Tj 3.15 0 Td 54.552469 Tz (groups ) Tj 2.119444 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 61.033951 Tz (H12-15 ) Tj 2.372222 0 Td 45.37037 Tz (in ) Tj 0.680556 0 Td 54.282407 Tz (both ) Tj 1.438889 0 Td 57.613169 Tz (complexes ) Tj 3.305556 0 Td 55.092593 Tz (6 ) Tj 0.466667 0 Td 61.574074 Tz (and ) Tj 51.428571 0 0 51.428571 0 795.865839 Tm 6.280556 0 Td 55.092593 Tz (5 ) Tj 0.563889 0 Td 64.814815 Tz (when ) Tj 1.769444 0 Td 59.953704 Tz (compared ) Tj 3.111111 0 Td 43.75 Tz (to ) Tj 0.777778 0 Td 46.990741 Tz (free ) Tj 1.341667 0 Td 64.814815 Tz (DIQ-Bpy ) Tj 2.955556 0 Td 46.759259 Tz (ligand. ) Tj 2.197222 0 Td 62.654321 Tz (The ) Tj 1.341667 0 Td 47.530864 Tz (substitution ) Tj 51.428571 0 0 51.428571 0 752.592798 Tm 6.261111 0 Td 58.333333 Tz (of ) Tj 0.894444 0 Td 56.712963 Tz (Cl ) Tj 1.283333 0 Td 51.851852 Tz (ion ) Tj 1.225 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 60.185185 Tz (complex ) Tj 2.838889 0 Td 55.092593 Tz (6 ) Tj 0.622222 0 Td 53.472222 Tz (with ) Tj 1.555556 0 Td 58.333333 Tz (a ) Tj 0.661111 0 Td 108.564815 Tz (HO ) Tj 1.613889 0 Td 54.012346 Tz (molecular ) Tj 3.208333 0 Td 37.268519 Tz (is ) Tj 0.719444 0 Td 48.148148 Tz (clearly ) Tj 45.714286 0 0 45.714286 0 717 Tm 7.04375 0 Td 61.523438 Tz (observed ) Tj 3.171875 0 Td 63.802083 Tz (from ) Tj 1.75 0 Td 55.902778 Tz (the ) Tj 1.26875 0 Td 69.270833 Tz ("H ) Tj 1.05 0 Td 103.298611 Tz (NMR ) Tj 2.034375 0 Td 61.067708 Tz (chemical ) Tj 3.128125 0 Td 48.125 Tz (shift ) Tj 1.6625 0 Td 47.395833 Tz (at ) Tj 0.83125 0 Td 72.916667 Tz (H15 ) Tj 1.553125 0 Td 64.713542 Tz (from ) Tj 1.75 0 Td 60.15625 Tz (9.56 ) Tj 51.428571 0 0 51.428571 0 670.264798 Tm 6.261111 0 Td 71.296296 Tz (ppm ) Tj 1.536111 0 Td 47.530864 Tz (\(6\) ) Tj 1.088889 0 Td 46.990741 Tz (to ) Tj 0.797222 0 Td 54.282407 Tz (9.30 ) Tj 1.536111 0 Td 70.216049 Tz (ppm ) Tj 1.555556 0 Td 40.509259 Tz (\(5\). ) Tj 51.428571 0 0 51.428571 0 629.094891 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.516667 0 Td 56.712963 Tz (UV-vis ) Tj 2.430556 0 Td 48.611111 Tz (spectra ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.972222 0 Td 57.613169 Tz (complexes ) Tj 3.5 0 Td 51.851852 Tz (6 ) Tj 0.719444 0 Td 58.333333 Tz (and ) Tj 1.438889 0 Td 55.092593 Tz (5 ) Tj 0.719444 0 Td 45.37037 Tz (in ) Tj 0.933333 0 Td 57.253086 Tz (dichlo ) Tj 51.428571 0 0 51.428571 0 586.969617 Tm 6.261111 0 Td 57.253086 Tz (romethane ) Tj 3.363889 0 Td 49.691358 Tz (are ) Tj 1.186111 0 Td 62.87037 Tz (shown ) Tj 2.197222 0 Td 45.37037 Tz (in ) Tj 0.894444 0 Td 53.472222 Tz (FIG. ) Tj 1.594444 0 Td 49.691358 Tz (20. ) Tj 1.205556 0 Td 63.888889 Tz (Complex ) Tj 2.975 0 Td 55.092593 Tz (6 ) Tj 0.641667 0 Td 51.49177 Tz (displayed ) Tj 3.091667 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 544.684564 Tm 6.280556 0 Td 50.231481 Tz (strong ) Tj 2.061111 0 Td 50.87963 Tz (absorption ) Tj 3.325 0 Td 46.990741 Tz (at ) Tj 0.816667 0 Td 60.493827 Tz (497 ) Tj 1.380556 0 Td 74.537037 Tz (nm ) Tj 1.186111 0 Td 58.333333 Tz (and ) Tj 1.322222 0 Td 55.092593 Tz (a ) Tj 0.602778 0 Td 64.814815 Tz (weak ) Tj 1.769444 0 Td 59.953704 Tz (band ) Tj 1.691667 0 Td 46.990741 Tz (at ) Tj 0.797222 0 Td 60.493827 Tz (362 ) Tj 1.419444 0 Td 58.333333 Tz (nm, ) Tj 51.428571 0 0 51.428571 0 503.216495 Tm 6.241667 0 Td 55.092593 Tz (while ) Tj 1.925 0 Td 48.611111 Tz (the ) Tj 1.127778 0 Td 53.596866 Tz (corresponding ) Tj 4.433333 0 Td 56.388889 Tz (bands ) Tj 1.963889 0 Td 47.222222 Tz (shifted ) Tj 2.236111 0 Td 46.990741 Tz (to ) Tj 0.855556 0 Td 60.493827 Tz (457 ) Tj 1.361111 0 Td 74.537037 Tz (nm ) Tj 1.166667 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 60.493827 Tz (334 ) Tj 51.428571 0 0 51.428571 0 463.290999 Tm 6.261111 0 Td 61.574074 Tz (nm, ) Tj 1.341667 0 Td 46.367521 Tz (respectively, ) Tj 3.830556 0 Td 46.990741 Tz (in ) Tj 0.777778 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 43.75 Tz (5, ) Tj 0.738889 0 Td 48.611111 Tz (consistent ) Tj 3.111111 0 Td 53.472222 Tz (with ) Tj 1.497222 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 55.555556 Tz (replace ) Tj 40 0 0 40 0 426 Tm 8.1 0 Td 76.041667 Tz (ment ) Tj 2.125 0 Td 75 Tz (of ) Tj 1.1 0 Td 65.833333 Tz (weak-field ) Tj 4.225 0 Td 77.083333 Tz (Cl ) Tj 1.65 0 Td 63.888889 Tz (ion ) Tj 1.5 0 Td 67.708333 Tz (with ) Tj 1.95 0 Td 70.833333 Tz (water ) Tj 2.425 0 Td 66.666667 Tz (molecule. ) Tj 51.428571 0 0 51.428571 0 384 Tm 6.280556 0 Td 51.649306 Tz (Electrochemistry ) Tj 51.428571 0 0 51.428571 0 337.825316 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.322222 0 Td 50.987654 Tz (electrochemical ) Tj 4.802778 0 Td 48.611111 Tz (properties ) Tj 3.130556 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 59.722222 Tz (complex ) Tj 2.722222 0 Td 58.333333 Tz (5 ) Tj 0.583333 0 Td 58.333333 Tz (were ) Tj 1.594444 0 Td 58.981481 Tz (inves ) Tj 51.428571 0 0 51.428571 0 297.196547 Tm 6.241667 0 Td 47.685185 Tz (tigated ) Tj 2.197222 0 Td 46.990741 Tz (at ) Tj 0.758333 0 Td 54.282407 Tz (both ) Tj 1.536111 0 Td 74.537037 Tz (pH ) Tj 1.127778 0 Td 58.333333 Tz (7 ) Tj 0.544444 0 Td 60.493827 Tz (and ) Tj 1.302778 0 Td 74.537037 Tz (pH ) Tj 1.166667 0 Td 38.888889 Tz (1. ) Tj 0.758333 0 Td 45.37037 Tz (In ) Tj 0.777778 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 55.092593 Tz (phosphate ) Tj 3.188889 0 Td 49.151235 Tz (buffer ) Tj 1.963889 0 Td 46.990741 Tz (at ) Tj 0.719444 0 Td 76.157407 Tz (pH ) Tj 51.428571 0 0 51.428571 0 254.867485 Tm 6.261111 0 Td 43.75 Tz (7, ) Tj 0.719444 0 Td 59.722222 Tz (complex ) Tj 2.683333 0 Td 51.851852 Tz (5 ) Tj 0.505556 0 Td 49.421296 Tz (displays ) Tj 2.547222 0 Td 60.493827 Tz (two ) Tj 1.263889 0 Td 47.638889 Tz (reversible ) Tj 3.033333 0 Td 55.092593 Tz (redox ) Tj 1.808333 0 Td 51.49177 Tz (processes ) Tj 2.916667 0 Td 46.990741 Tz (at ) Tj 0.738889 0 Td 49.421296 Tz (0.61 ) Tj 58.571429 0 0 58.571429 0 211.874005 Tm 5.497561 0 Td 76.829268 Tz (V ) Tj 0.682927 0 Td 50.271003 Tz (and ) Tj 1.160976 0 Td 46.239837 Tz (0.80 ) Tj 1.331707 0 Td 71.138211 Tz (V ) Tj 0.64878 0 Td 42.682927 Tz (\(vs ) Tj 1.007317 0 Td 51.788618 Tz (SHE\), ) Tj 1.809756 0 Td 44.674797 Tz (assignable ) Tj 2.902439 0 Td 38.414634 Tz (to ) Tj 0.734146 0 Td 90.108401 Tz (Ru' ) Tj 1.895122 0 Td 51.219512 Tz (and ) Tj 1.178049 0 Td 65.447154 Tz (Ru'', ) Tj 25.714286 0 0 25.714286 0 192 Tm 46.472222 0 Td 19.444444 Tz (s ) Tj 51.428571 0 0 51.428571 0 171.544715 Tm 6.261111 0 Td 48.611111 Tz (respectively ) Tj 3.752778 0 Td 52.5 Tz (\(FIG. ) Tj 1.847222 0 Td 46.180556 Tz (21\). ) Tj 1.361111 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 54.444444 Tz (redox ) Tj 1.847222 0 Td 47.638889 Tz (potentials ) Tj 3.111111 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 66.435185 Tz (Ru ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 77.252252 Tz (30 ) Tj 60 0 0 60 0 2915.84148 Tm 21.6 0 Td 50 Tz (and ) Tj 1.166667 0 Td 97.222222 Tz (Ru' ) Tj 2.016667 0 Td 45.634921 Tz (couples ) Tj 2.133333 0 Td 52.777778 Tz (of ) Tj 0.783333 0 Td 47.222222 Tz (5 ) Tj 0.533333 0 Td 44.444444 Tz (are ) Tj 1.033333 0 Td 42.063492 Tz (similar ) Tj 1.983333 0 Td 37.5 Tz (to ) Tj 0.733333 0 Td 43.333333 Tz (those ) Tj 1.55 0 Td 43.055556 Tz (reported ) Tj 2.316667 0 Td 41.666667 Tz (for ) Tj 51.428571 0 0 51.428571 0 2871.392713 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 87.5 Tz (A ) Tj 0.719444 0 Td 48.611111 Tz (\(B. ) Tj 1.205556 0 Td 57.523148 Tz (Radaram, ) Tj 3.013889 0 Td 37.268519 Tz (J. ) Tj 0.680556 0 Td 56.712963 Tz (A. ) Tj 0.991667 0 Td 42.777778 Tz (Ivie, ) Tj 1.594444 0 Td 48.611111 Tz (R. ) Tj 0.855556 0 Td 68.055556 Tz (M. ) Tj 1.088889 0 Td 52.932099 Tz (Grudzien, ) Tj 3.15 0 Td 35.648148 Tz (J. ) Tj 0.758333 0 Td 53.472222 Tz (H. ) Tj 51.428571 0 0 51.428571 0 2828.716049 Tm 25.219444 0 Td 51.041667 Tz (Reibenspies, ) Tj 3.830556 0 Td 53.472222 Tz (C. ) Tj 0.855556 0 Td 46.990741 Tz (E. ) Tj 0.758333 0 Td 51.851852 Tz (Webster, ) Tj 2.644444 0 Td 58.333333 Tz (X. ) Tj 0.875 0 Td 55.740741 Tz (Zhao, ) Tj 1.866667 0 Td 46.450617 Tz (Inorg. ) Tj 1.866667 0 Td 62.87037 Tz (Chem. ) Tj 2.080556 0 Td 52.5 Tz (2011, ) Tj 1.769444 0 Td 48.611111 Tz (50. ) Tj 51.428571 0 0 51.428571 0 2784.658858 Tm 25.277778 0 Td 55.092593 Tz (10564-10571, ) Tj 4.219444 0 Td 51.311728 Tz (incorporated ) Tj 3.908333 0 Td 50.771605 Tz (herein ) Tj 2.080556 0 Td 59.953704 Tz (by ) Tj 0.991667 0 Td 46.548822 Tz (reference\). ) Tj 51.428571 0 0 51.428571 0 2196.690909 Tm 25.919444 0 Td 63.888889 Tz (Complex ) Tj 2.897222 0 Td 87.5 Tz (A ) Tj 51.428571 0 0 51.428571 0 2146 Tm 25.919444 0 Td 51.851852 Tz (In ) Tj 0.913889 0 Td 46.450617 Tz (0.1 ) Tj 1.225 0 Td 100.462963 Tz (M ) Tj 0.952778 0 Td 82.638889 Tz (HNO, ) Tj 2.333333 0 Td 47.962963 Tz (three ) Tj 1.75 0 Td 54.444444 Tz (redox ) Tj 1.905556 0 Td 51.851852 Tz (events ) Tj 2.177778 0 Td 58.333333 Tz (were ) Tj 1.711111 0 Td 54.282407 Tz (observed ) Tj 2.936111 0 Td 48.611111 Tz (for ) Tj 51.428571 0 0 51.428571 0 2104.744681 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 2.761111 0 Td 51.851852 Tz (5 ) Tj 0.583333 0 Td 43.75 Tz (at ) Tj 0.758333 0 Td 47.962963 Tz (0.87, ) Tj 1.769444 0 Td 45.37037 Tz (1.26, ) Tj 1.594444 0 Td 59.41358 Tz (and ) Tj 1.361111 0 Td 50.231481 Tz (1.87 ) Tj 1.419444 0 Td 84.259259 Tz (V ) Tj 0.777778 0 Td 47.530864 Tz (\(vs ) Tj 1.108333 0 Td 59.62963 Tz (SHE\), ) Tj 2.022222 0 Td 52.256944 Tz (assigned ) Tj 2.741667 0 Td 45.37037 Tz (to ) Tj 58.571429 0 0 58.571429 0 2062.496815 Tm 22.126829 0 Td 61.463415 Tz (Ru'', ) Tj 2.168293 0 Td 65.447154 Tz (Ru'', ) Tj 2.236585 0 Td 53.116531 Tz (and ) Tj 1.212195 0 Td 59.186992 Tz (Ru'', ) Tj 2.065854 0 Td 42.920054 Tz (respectively ) Tj 3.363415 0 Td 44.105691 Tz (\(Figures ) Tj 2.390244 0 Td 59.756098 Tz (Ca ) Tj 0.973171 0 Td 52.168022 Tz (and ) Tj 60 0 0 60 0 2016.809917 Tm 21.6 0 Td 44.444444 Tz (Cb\). ) Tj 1.433333 0 Td 51.666667 Tz (While ) Tj 1.916667 0 Td 41.666667 Tz (the ) Tj 1.083333 0 Td 47.222222 Tz (redox ) Tj 1.766667 0 Td 40.555556 Tz (potentials ) Tj 2.8 0 Td 50 Tz (of ) Tj 0.9 0 Td 90.740741 Tz (Ru' ) Tj 2 0 Td 50 Tz (and ) Tj 1.3 0 Td 72.916667 Tz (Ru'' ) Tj 52.857143 0 0 52.857143 0 1975.427861 Tm 24.518919 0 Td 51.801802 Tz (couples ) Tj 2.308108 0 Td 56.756757 Tz (of ) Tj 0.775676 0 Td 53.603604 Tz (5 ) Tj 0.491892 0 Td 48.348348 Tz (are ) Tj 1.021622 0 Td 48.558559 Tz (close ) Tj 1.608108 0 Td 44.144144 Tz (to ) Tj 0.7 0 Td 49.81982 Tz (those ) Tj 1.645946 0 Td 55.18018 Tz (of ) Tj 0.737838 0 Td 58.108108 Tz (complex ) Tj 2.572973 0 Td 81.981982 Tz (A ) Tj 0.605405 0 Td 47.297297 Tz (in ) Tj 0.737838 0 Td 44.144144 Tz (0.1 ) Tj 1.040541 0 Td 90.810811 Tz (MHNO. ) Tj 60 0 0 60 0 1936.38101 Tm 21.583333 0 Td 42.222222 Tz (there ) Tj 1.383333 0 Td 36.111111 Tz (is ) Tj 0.533333 0 Td 47.222222 Tz (a ) Tj 0.433333 0 Td 39.393939 Tz (significant ) Tj 2.716667 0 Td 43.055556 Tz (increase ) Tj 2.183333 0 Td 41.666667 Tz (for ) Tj 0.85 0 Td 42.592593 Tz (the ) Tj 0.883333 0 Td 86.111111 Tz (Ru' ) Tj 1.75 0 Td 46.296296 Tz (couple ) Tj 1.783333 0 Td 51.736111 Tz (compared ) Tj 51.428571 0 0 51.428571 0 1891.301387 Tm 25.180556 0 Td 46.990741 Tz (to ) Tj 0.758333 0 Td 43.75 Tz (that ) Tj 1.205556 0 Td 49.259259 Tz (\(1.75 ) Tj 1.672222 0 Td 84.259259 Tz (V ) Tj 0.641667 0 Td 51.851852 Tz (vs ) Tj 0.777778 0 Td 68.055556 Tz (SHE\) ) Tj 1.769444 0 Td 55.092593 Tz (of ) Tj 0.738889 0 Td 59.722222 Tz (complex ) Tj 2.663889 0 Td 55.092593 Tz (5 ) Tj 0.525 0 Td 49.691358 Tz (\(B. ) Tj 1.069444 0 Td 57.928241 Tz (Radaram, ) Tj 2.916667 0 Td 37.268519 Tz (J. ) Tj 0.602778 0 Td 56.712963 Tz (A. ) Tj 0.855556 0 Td 42.12963 Tz (Ivie, ) Tj 51.428571 0 0 51.428571 0 1850.938144 Tm 25.219444 0 Td 51.851852 Tz (R. ) Tj 0.855556 0 Td 64.814815 Tz (M. ) Tj 1.011111 0 Td 53.652263 Tz (Grudzien, ) Tj 3.111111 0 Td 35.648148 Tz (J. ) Tj 0.680556 0 Td 55.092593 Tz (H. ) Tj 0.933333 0 Td 50.771605 Tz (Reibenspies, ) Tj 3.85 0 Td 53.472222 Tz (C. ) Tj 0.913889 0 Td 46.990741 Tz (E. ) Tj 0.777778 0 Td 51.851852 Tz (Webster, ) Tj 2.702778 0 Td 58.333333 Tz (X. ) Tj 0.933333 0 Td 55.092593 Tz (Zhao, ) Tj 51.428571 0 0 51.428571 0 1809.270968 Tm 25.2 0 Td 48.070988 Tz (Inorg. ) Tj 2.041667 0 Td 63.518519 Tz (Chem. ) Tj 2.197222 0 Td 53.796296 Tz (2011, ) Tj 1.905556 0 Td 49.691358 Tz (50, ) Tj 1.263889 0 Td 54.344729 Tz (10564-10571\). ) Tj 4.55 0 Td 48.611111 Tz (In ) Tj 0.894444 0 Td 47.530864 Tz (the ) Tj 1.166667 0 Td 53.06713 Tz (presence ) Tj 2.838889 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 1768.829932 Tm 25.2 0 Td 59.259259 Tz (complex ) Tj 2.858333 0 Td 45.37037 Tz (5, ) Tj 0.894444 0 Td 49.691358 Tz (the ) Tj 1.263889 0 Td 49.421296 Tz (increase ) Tj 2.722222 0 Td 43.75 Tz (in ) Tj 0.894444 0 Td 54.012346 Tz (anodic ) Tj 2.313889 0 Td 49.537037 Tz (current ) Tj 2.391667 0 Td 46.990741 Tz (at ) Tj 0.894444 0 Td 51.851852 Tz (a ) Tj 0.661111 0 Td 47.530864 Tz (potential ) Tj 58.571429 0 0 58.571429 0 1727.095178 Tm 22.109756 0 Td 46.95122 Tz (higher ) Tj 1.878049 0 Td 45.528455 Tz (than ) Tj 1.34878 0 Td 41.734417 Tz (1.5 ) Tj 0.990244 0 Td 76.829268 Tz (V ) Tj 0.682927 0 Td 43.631436 Tz (indicated ) Tj 2.543902 0 Td 41.260163 Tz (that ) Tj 1.178049 0 Td 51.219512 Tz (a ) Tj 0.512195 0 Td 44.493718 Tz (high-valent ) Tj 3.158537 0 Td 64.02439 Tz (Ru?'O ) Tj 2.526829 0 Td 46.95122 Tz (or ) Tj 51.428571 0 0 51.428571 0 1687.598742 Tm 25.180556 0 Td 52.932099 Tz (higher ) Tj 2.158333 0 Td 50.411523 Tz (oxidation ) Tj 2.994444 0 Td 44.074074 Tz (state ) Tj 1.594444 0 Td 68.055556 Tz (may ) Tj 1.497222 0 Td 58.333333 Tz (be ) Tj 0.972222 0 Td 50.084175 Tz (responsible ) Tj 3.538889 0 Td 49.691358 Tz (for ) Tj 1.088889 0 Td 51.851852 Tz (the ) Tj 1.186111 0 Td 45.37037 Tz (catalytic ) Tj 40 0 0 40 0 1649 Tm 32.4 0 Td 65.277778 Tz (oxidation ) Tj 3.875 0 Td 70.833333 Tz (of ) Tj 1.05 0 Td 61.805556 Tz (water. ) Tj 51.428571 0 0 51.428571 0 1599.51436 Tm 25.919444 0 Td 50.084175 Tz (Theoretical ) Tj 3.577778 0 Td 48.070988 Tz (calculations ) Tj 3.772222 0 Td 58.333333 Tz (of ) Tj 0.913889 0 Td 53.796296 Tz (redox ) Tj 1.886111 0 Td 46.990741 Tz (potentials ) Tj 3.091667 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 64.814815 Tz (Ru ) Tj 1.069444 0 Td 83.179012 Tz (com ) Tj 51.428571 0 0 51.428571 0 1560.463479 Tm 25.2 0 Td 51.311728 Tz (plexes ) Tj 2.177778 0 Td 57.523148 Tz (have ) Tj 1.672222 0 Td 57.523148 Tz (been ) Tj 1.711111 0 Td 48.148148 Tz (carried ) Tj 2.352778 0 Td 50.771605 Tz (out ) Tj 1.205556 0 Td 46.990741 Tz (to ) Tj 0.894444 0 Td 53.240741 Tz (provide ) Tj 2.527778 0 Td 46.990741 Tz (insights ) Tj 2.586111 0 Td 46.990741 Tz (into ) Tj 1.438889 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 1516.139601 Tm 25.2 0 Td 47.638889 Tz (electronic ) Tj 3.266667 0 Td 45.37037 Tz (effects ) Tj 2.352778 0 Td 58.333333 Tz (of ) Tj 1.05 0 Td 46.296296 Tz (ligand. ) Tj 2.372222 0 Td 64.814815 Tz (As ) Tj 1.225 0 Td 62.87037 Tz (shown ) Tj 2.333333 0 Td 45.37037 Tz (in ) Tj 0.952778 0 Td 54.444444 Tz (Table ) Tj 2.1 0 Td 40.509259 Tz (1, ) Tj 0.913889 0 Td 50.771605 Tz (the ) Tj 58.571429 0 0 58.571429 0 1477.339623 Tm 22.126829 0 Td 52.997967 Tz (computed ) Tj 2.765854 0 Td 48.373984 Tz (redox ) Tj 1.673171 0 Td 41.544715 Tz (potentials ) Tj 2.731707 0 Td 42.682927 Tz (for ) Tj 1.007317 0 Td 61.463415 Tz (Ru'', ) Tj 2.117073 0 Td 66.01626 Tz (Ru'', ) Tj 2.219512 0 Td 51.219512 Tz (and ) Tj 1.178049 0 Td 65.447154 Tz (Ru'' ) Tj 51.428571 0 0 51.428571 0 1435.796117 Tm 25.2 0 Td 52.777778 Tz (couples ) Tj 2.411111 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 55.092593 Tz (5 ) Tj 0.525 0 Td 49.691358 Tz (are ) Tj 1.069444 0 Td 52.777778 Tz (underestimated ) Tj 4.627778 0 Td 64.00463 Tz (when ) Tj 1.730556 0 Td 59.953704 Tz (compared ) Tj 3.052778 0 Td 45.37037 Tz (to ) Tj 51.428571 0 0 51.428571 0 1395.521739 Tm 25.180556 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 52.662037 Tz (experimental ) Tj 4.063889 0 Td 47.685185 Tz (values. ) Tj 38.571429 0 0 38.571429 0 1311 Tm 43.322222 0 Td 101.111111 Tz (TABLE ) Tj 3.448148 0 Td 25.925926 Tz (1. ) Tj 41.428571 0 0 41.428571 0 1240.465969 Tm 31.451724 0 Td 52.6341 Tz (Experimental ) Tj 4.031034 0 Td 54.980843 Tz (and ) Tj 1.206897 0 Td 61.350575 Tz (Computed ) Tj 3.234483 0 Td 59.54023 Tz (Redox ) Tj 2.051724 0 Td 45.862069 Tz (Potentials ) Tj 2.993103 0 Td 54.310345 Tz (of ) Tj 0.844828 0 Td 48.275862 Tz (5 ) Tj 0.555172 0 Td 44.252874 Tz (at ) Tj 0.724138 0 Td 70.402299 Tz (pH ) Tj 1.158621 0 Td 36.206897 Tz (1 ) Tj 0.555172 0 Td 56.321839 Tz (\(0.1M ) Tj 2.003448 0 Td 81.465517 Tz (HNO\) ) Tj 40 0 0 40 0 1207.050314 Tm 36.725 0 Td 58.333333 Tz (and ) Tj 1.3 0 Td 70.833333 Tz (pH ) Tj 1.175 0 Td 50 Tz (7 ) Tj 0.575 0 Td 53.75 Tz (\(Phosphate ) Tj 3.475 0 Td 46.875 Tz (Bufler\), ) Tj 2.55 0 Td 54.166667 Tz (EL\). ) Tj 1.525 0 Td 79.166667 Tz (VVS ) Tj 1.65 0 Td 63.541667 Tz (SHE. ) Tj 37.142857 0 0 37.142857 0 1145 Tm 43.669231 0 Td 103.205128 Tz (RHA ) Tj 5.788462 0 Td 76.282051 Tz (RVIII ) Tj 5.976923 0 Td 61.698718 Tz (Ru7 ) Tj 34.285714 0 0 34.285714 0 1083.232227 Tm 40.3375 0 Td 89.930556 Tz (pH ) Tj 1.341667 0 Td 77.777778 Tz (= ) Tj 0.7875 0 Td 53.472222 Tz (1 ) Tj 5.191667 0 Td 61.979167 Tz (O.87 ) Tj 6.445833 0 Td 58.333333 Tz (1.26 ) Tj 6.358333 0 Td 58.333333 Tz (1.87 ) Tj 34.285714 0 0 34.285714 0 1049.130435 Tm 40.3375 0 Td 89.930556 Tz (pH ) Tj 1.341667 0 Td 77.777778 Tz (= ) Tj 0.758333 0 Td 68.055556 Tz (7 ) Tj 5.220833 0 Td 59.548611 Tz (O.61 ) Tj 6.3875 0 Td 60.763889 Tz (O.80 ) Tj 6.504167 0 Td 99.652778 Tz (NA ) Tj 32.5 0 0 32.5 0 1015.403941 Tm 42.923077 0 Td 138.461538 Tz (HO ) Tj 7.353846 0 Td 66.666667 Tz (O.24 ) Tj 6.738462 0 Td 64.102564 Tz (O.47 ) Tj 6.769231 0 Td 60.25641 Tz (1.13 ) Tj 35.714286 0 0 35.714286 0 952.888889 Tm 36.568 0 Td 60.666667 Tz (Computed ) Tj 3.164 0 Td 52.266667 Tz (redox ) Tj 1.792 0 Td 42.933333 Tz (potential. ) Tj 40 0 0 40 0 883 Tm 32.4 0 Td 75 Tz (Water ) Tj 2.525 0 Td 68.981481 Tz (Oxidation ) Tj 4.075 0 Td 64.880952 Tz (Studies ) Tj 51.428571 0 0 51.428571 0 836.606218 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 58.873457 Tz (oxygen ) Tj 2.352778 0 Td 50.771605 Tz (evolution ) Tj 2.975 0 Td 44.965278 Tz (activity ) Tj 2.391667 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 58.333333 Tz (5 ) Tj 0.583333 0 Td 62.654321 Tz (was ) Tj 1.361111 0 Td 51.388889 Tz (investi ) Tj 51.428571 0 0 51.428571 0 793.582418 Tm 25.2 0 Td 52.5 Tz (gated ) Tj 1.75 0 Td 52.5 Tz (using ) Tj 1.769444 0 Td 55.092593 Tz (cerium ) Tj 2.158333 0 Td 69.270833 Tz (ammonium ) Tj 3.558333 0 Td 43.518519 Tz (nitrate ) Tj 2.002778 0 Td 66.759259 Tz (\(CAN\) ) Tj 2.197222 0 Td 48.611111 Tz (as ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.088889 0 Td 51.851852 Tz (oxidant ) Tj 58.571429 0 0 58.571429 0 750 Tm 22.143902 0 Td 59.163279 Tz (\(2H2O+4Ce'->O+4H"+4Ce'\). ) Tj 8.707317 0 Td 56.910569 Tz (As ) Tj 0.904878 0 Td 55.203252 Tz (shown ) Tj 1.843902 0 Td 41.260163 Tz (in ) Tj 0.734146 0 Td 47.662602 Tz (FIG. ) Tj 1.34878 0 Td 43.631436 Tz (22, ) Tj 0.990244 0 Td 43.631436 Tz (the ) Tj 57.142857 0 0 57.142857 0 710.306329 Tm 22.68 0 Td 44.84375 Tz (addition ) Tj 2.345 0 Td 52.5 Tz (of ) Tj 0.735 0 Td 47.152778 Tz (excess ) Tj 1.89 0 Td 63.194444 Tz (Ce' ) Tj 1.435 0 Td 43.75 Tz (solution ) Tj 2.2925 0 Td 40.833333 Tz (to ) Tj 0.6825 0 Td 49.583333 Tz (a ) Tj 0.5075 0 Td 44.479167 Tz (solution ) Tj 2.2925 0 Td 53.958333 Tz (of ) Tj 0.7525 0 Td 53.75 Tz (complex ) Tj 2.4675 0 Td 46.666667 Tz (5 ) Tj 51.428571 0 0 51.428571 0 668.218065 Tm 25.2 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 47.530864 Tz (1.0 ) Tj 1.030556 0 Td 102.083333 Tz (MHNO ) Tj 2.936111 0 Td 45.37037 Tz (\(3 ) Tj 0.816667 0 Td 68.055556 Tz (mL\) ) Tj 1.438889 0 Td 47.395833 Tz (resulted ) Tj 2.488889 0 Td 45.37037 Tz (in ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.05 0 Td 50.771605 Tz (evolution ) Tj 2.955556 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 54.62963 Tz (oxygen, ) Tj 51.428571 0 0 51.428571 0 629.571995 Tm 25.180556 0 Td 59.62963 Tz (which ) Tj 2.177778 0 Td 52.932099 Tz (has ) Tj 1.361111 0 Td 55.902778 Tz (been ) Tj 1.769444 0 Td 54.372428 Tz (confirmed ) Tj 3.286111 0 Td 59.953704 Tz (by ) Tj 1.108333 0 Td 55.092593 Tz (gas ) Tj 1.4 0 Td 54.012346 Tz (chromatography. ) Tj 5.25 0 Td 62.654321 Tz (The ) Tj 51.428571 0 0 51.428571 0 585.151832 Tm 25.2 0 Td 50.771605 Tz (evolution ) Tj 3.052778 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 59.41358 Tz (oxygen ) Tj 2.469444 0 Td 54.012346 Tz (ceased ) Tj 2.216667 0 Td 46.018519 Tz (after ) Tj 1.672222 0 Td 61.574074 Tz (30 ) Tj 1.05 0 Td 59.41358 Tz (min ) Tj 1.419444 0 Td 53.472222 Tz (with ) Tj 1.575 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 52.256944 Tz (turnover ) Tj 51.428571 0 0 51.428571 0 544.656753 Tm 25.2 0 Td 62.654321 Tz (number ) Tj 2.430556 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 44.560185 Tz (2.8. ) Tj 1.283333 0 Td 63.599537 Tz (Compared ) Tj 3.286111 0 Td 43.75 Tz (to ) Tj 0.777778 0 Td 48.611111 Tz (the ) Tj 1.108333 0 Td 53.148148 Tz (water ) Tj 1.788889 0 Td 50.771605 Tz (oxidation ) Tj 2.975 0 Td 44.965278 Tz (activity ) Tj 2.391667 0 Td 58.333333 Tz (of ) Tj 51.428571 0 0 51.428571 0 504.975093 Tm 25.2 0 Td 59.259259 Tz (complex ) Tj 2.722222 0 Td 56.712963 Tz (A, ) Tj 0.894444 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 48.881173 Tz (introduction ) Tj 3.772222 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 49.96142 Tz (isoquinoline ) Tj 3.85 0 Td 55.740741 Tz (group ) Tj 1.925 0 Td 45.37037 Tz (in ) Tj 0.797222 0 Td 83.179012 Tz (com ) Tj 51.428571 0 0 51.428571 0 460.745993 Tm 25.2 0 Td 52.662037 Tz (plex ) Tj 1.438889 0 Td 55.092593 Tz (5 ) Tj 0.525 0 Td 47.800926 Tz (resulted ) Tj 2.469444 0 Td 43.75 Tz (in ) Tj 0.719444 0 Td 55.740741 Tz (lower ) Tj 1.808333 0 Td 45.37037 Tz (activity ) Tj 2.372222 0 Td 46.990741 Tz (in ) Tj 0.719444 0 Td 54.444444 Tz (water ) Tj 1.75 0 Td 48.935185 Tz (oxidation. ) Tj 3.111111 0 Td 53.472222 Tz (This ) Tj 1.458333 0 Td 60.493827 Tz (low ) Tj 51.428571 0 0 51.428571 0 422.465374 Tm 25.2 0 Td 44.965278 Tz (activity ) Tj 2.625 0 Td 68.055556 Tz (may ) Tj 1.711111 0 Td 44.290123 Tz (result ) Tj 2.022222 0 Td 57.523148 Tz (from ) Tj 1.827778 0 Td 49.691358 Tz (the ) Tj 1.302778 0 Td 52.932099 Tz (higher ) Tj 2.333333 0 Td 54.444444 Tz (redox ) Tj 2.041667 0 Td 47.170782 Tz (potential ) Tj 2.994444 0 Td 58.333333 Tz (of ) Tj 60 0 0 60 0 379.20437 Tm 21.6 0 Td 51.190476 Tz (complex ) Tj 2.35 0 Td 47.222222 Tz (5 ) Tj 0.5 0 Td 43.333333 Tz (\(1.87 ) Tj 1.466667 0 Td 72.222222 Tz (V ) Tj 0.65 0 Td 45.833333 Tz (vs ) Tj 0.716667 0 Td 65.740741 Tz (SHE ) Tj 1.383333 0 Td 42.592593 Tz (for ) Tj 0.933333 0 Td 75.694444 Tz (Ru'\) ) Tj 2 0 Td 51.388889 Tz (compared ) Tj 2.666667 0 Td 37.5 Tz (to ) Tj 0.65 0 Td 40.277778 Tz (that ) Tj 1.133333 0 Td 50 Tz (of ) Tj 58.571429 0 0 58.571429 0 337.211132 Tm 22.126829 0 Td 52.03252 Tz (complex ) Tj 2.373171 0 Td 76.829268 Tz (A ) Tj 0.64878 0 Td 43.252033 Tz (\(1.75 ) Tj 1.519512 0 Td 73.98374 Tz (V ) Tj 0.682927 0 Td 45.528455 Tz (vs ) Tj 0.768293 0 Td 67.344173 Tz (SHE ) Tj 1.417073 0 Td 42.682927 Tz (for ) Tj 0.990244 0 Td 55.01355 Tz (Ru''\). ) Tj 51.428571 0 0 51.428571 0 295.983957 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.477778 0 Td 52.572016 Tz (formation ) Tj 3.169444 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 50.378788 Tz (high-valent ) Tj 3.675 0 Td 85.87963 Tz (Ru=O ) Tj 2.391667 0 Td 50 Tz (species ) Tj 2.411111 0 Td 54.012346 Tz (has ) Tj 1.322222 0 Td 57.523148 Tz (been ) Tj 51.428571 0 0 51.428571 0 252.970443 Tm 25.219444 0 Td 52.932099 Tz (Suggested ) Tj 3.013889 0 Td 50.231481 Tz (as ) Tj 0.777778 0 Td 55.092593 Tz (a ) Tj 0.486111 0 Td 57.253086 Tz (key ) Tj 1.205556 0 Td 50.771605 Tz (intermediate ) Tj 3.830556 0 Td 43.75 Tz (in ) Tj 0.7 0 Td 48.611111 Tz (the ) Tj 1.069444 0 Td 50.411523 Tz (oxidation ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 48.070988 Tz (water. ) Tj 1.905556 0 Td 64.814815 Tz (As ) Tj 51.428571 0 0 51.428571 0 212.235294 Tm 25.219444 0 Td 62.222222 Tz (shown ) Tj 2.041667 0 Td 46.990741 Tz (in ) Tj 0.758333 0 Td 54.282407 Tz (FIG. ) Tj 1.516667 0 Td 51.851852 Tz (21b, ) Tj 1.438889 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 46.180556 Tz (electrocatalytic ) Tj 4.627778 0 Td 50.411523 Tz (oxidation ) Tj 2.916667 0 Td 56.712963 Tz (of ) Tj 0.777778 0 Td 54.444444 Tz (water ) Tj 1.769444 0 Td 45.37037 Tz (to ) Tj 51.428571 0 0 51.428571 0 170.414894 Tm 25.2 0 Td 51.851852 Tz (O. ) Tj 1.011111 0 Td 52.391975 Tz (occurs ) Tj 2.080556 0 Td 45.37037 Tz (at ) Tj 0.738889 0 Td 51.851852 Tz (a ) Tj 0.525 0 Td 46.450617 Tz (potential ) Tj 2.722222 0 Td 52.932099 Tz (higher ) Tj 2.080556 0 Td 50.231481 Tz (than ) Tj 1.516667 0 Td 44.290123 Tz (1.5 ) Tj 1.030556 0 Td 84.259259 Tz (V ) Tj 0.719444 0 Td 49.259259 Tz (\(1.84 ) Tj 1.711111 0 Td 81.018519 Tz (V ) Tj 0.7 0 Td 51.851852 Tz (vs ) Tj 0.855556 0 Td 58.333333 Tz (SHE\), ) Tj 1.428571 0 0 1.428571 0 2703 Tm 1064.7 0 Td 116.666667 Tz ( ) Tj ET Q endstream endobj 290 0 obj << /Length 1 >> stream q endstream endobj 291 0 obj << /Length 42580 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.113514 0 Td 74.099099 Tz (31 ) Tj 51.428571 0 0 51.428571 0 2917.216749 Tm 6.280556 0 Td 51.527778 Tz (Suggesting ) Tj 3.325 0 Td 46.990741 Tz (that ) Tj 1.341667 0 Td 58.333333 Tz (a ) Tj 0.602778 0 Td 50.378788 Tz (high-valent ) Tj 3.616667 0 Td 86.203704 Tz (RuV=O ) Tj 2.838889 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 52.932099 Tz (higher ) Tj 2.158333 0 Td 51.131687 Tz (oxidation ) Tj 51.428571 0 0 51.428571 0 2874.38342 Tm 6.280556 0 Td 44.074074 Tz (state ) Tj 1.652778 0 Td 65.895062 Tz (may ) Tj 1.477778 0 Td 59.953704 Tz (be ) Tj 1.030556 0 Td 49.789562 Tz (responsible ) Tj 3.577778 0 Td 48.611111 Tz (for ) Tj 1.147222 0 Td 54.444444 Tz (water ) Tj 1.905556 0 Td 50.411523 Tz (oxidation ) Tj 3.052778 0 Td 60.185185 Tz (\(Scheme ) Tj 2.838889 0 Td 41.049383 Tz (4\). ) Tj 51.428571 0 0 51.428571 0 2834.576923 Tm 6.280556 0 Td 57.407407 Tz (Because ) Tj 2.625 0 Td 56.712963 Tz (of ) Tj 0.758333 0 Td 50.771605 Tz (the ) Tj 1.108333 0 Td 48.611111 Tz (electron ) Tj 2.547222 0 Td 55.681818 Tz (withdrawing ) Tj 3.869444 0 Td 49.96142 Tz (isoquinoline ) Tj 3.791667 0 Td 55.092593 Tz (groups ) Tj 2.197222 0 Td 48.611111 Tz (in ) Tj 58.571429 0 0 58.571429 0 2793.23203 Tm 5.497561 0 Td 52.439024 Tz (complex ) Tj 2.407317 0 Td 36.99187 Tz (5, ) Tj 0.64878 0 Td 42.682927 Tz (the ) Tj 0.921951 0 Td 46.95122 Tz (higher ) Tj 1.843902 0 Td 48.373984 Tz (redox ) Tj 1.604878 0 Td 41.734417 Tz (potential ) Tj 2.42439 0 Td 54.065041 Tz (of ) Tj 0.75122 0 Td 66.158537 Tz (Ruf' ) Tj 1.843902 0 Td 47.899729 Tz (couple ) Tj 1.895122 0 Td 39.837398 Tz (in ) Tj 0.682927 0 Td 48.373984 Tz (3 ) Tj 57.142857 0 0 57.142857 0 2747.393094 Tm 5.635 0 Td 55.416667 Tz (makes ) Tj 1.925 0 Td 43.75 Tz (the ) Tj 1.015 0 Td 45.37037 Tz (oxidation ) Tj 2.6775 0 Td 53.958333 Tz (of ) Tj 0.8225 0 Td 63.194444 Tz (Ru' ) Tj 1.4525 0 Td 40.833333 Tz (to ) Tj 0.7525 0 Td 49.583333 Tz (Ru? ) Tj 1.2775 0 Td 40.833333 Tz (less ) Tj 1.2075 0 Td 39.212963 Tz (efficient ) Tj 2.3275 0 Td 53.958333 Tz (by ) Tj 0.875 0 Td 56.875 Tz (Ce'. ) Tj 51.428571 0 0 51.428571 0 2706.365617 Tm 6.261111 0 Td 57.118056 Tz (Although ) Tj 2.975 0 Td 34.027778 Tz (it ) Tj 0.622222 0 Td 54.012346 Tz (has ) Tj 1.225 0 Td 56.712963 Tz (been ) Tj 1.594444 0 Td 54.552469 Tz (demonstrated ) Tj 4.161111 0 Td 45.37037 Tz (that ) Tj 1.322222 0 Td 54.520697 Tz (electron-withdraw ) Tj 51.428571 0 0 51.428571 0 2669.26853 Tm 6.261111 0 Td 50.771605 Tz (ing ) Tj 1.108333 0 Td 54.552469 Tz (groups ) Tj 2.177778 0 Td 54.282407 Tz (such ) Tj 1.497222 0 Td 48.611111 Tz (as ) Tj 0.797222 0 Td 49.691358 Tz (isoquinoline ) Tj 3.752778 0 Td 54.444444 Tz (could ) Tj 1.808333 0 Td 54.012346 Tz (induce ) Tj 2.1 0 Td 52.391975 Tz (higher ) Tj 2.041667 0 Td 45.775463 Tz (activity ) Tj 51.428571 0 0 51.428571 0 2624.604891 Tm 6.261111 0 Td 49.691358 Tz (for ) Tj 1.186111 0 Td 54.444444 Tz (water ) Tj 1.905556 0 Td 48.935185 Tz (oxidation, ) Tj 3.266667 0 Td 49.691358 Tz (the ) Tj 1.205556 0 Td 45.37037 Tz (relatively ) Tj 3.033333 0 Td 45.775463 Tz (activity ) Tj 2.508333 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 53.148148 Tz (metal ) Tj 1.886111 0 Td 84.259259 Tz (com ) Tj 51.428571 0 0 51.428571 0 2584.695431 Tm 6.261111 0 Td 51.311728 Tz (plexes ) Tj 2.1 0 Td 49.421296 Tz (also ) Tj 1.419444 0 Td 56.944444 Tz (depends ) Tj 2.625 0 Td 59.953704 Tz (on ) Tj 0.972222 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 55.740741 Tz (redox ) Tj 1.886111 0 Td 47.314815 Tz (potentials ) Tj 3.091667 0 Td 58.333333 Tz (and ) Tj 1.302778 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 60.925926 Tz (acces ) Tj 51.428571 0 0 51.428571 0 2542.910644 Tm 6.280556 0 Td 41.724537 Tz (sibility ) Tj 2.411111 0 Td 59.953704 Tz (of ) Tj 0.991667 0 Td 53.472222 Tz (higher ) Tj 2.255556 0 Td 51.131687 Tz (oxidation ) Tj 3.188889 0 Td 44.290123 Tz (states ) Tj 2.041667 0 Td 50.084175 Tz (responsible ) Tj 3.713889 0 Td 47.530864 Tz (for ) Tj 1.244444 0 Td 54.444444 Tz (water ) Tj 40 0 0 40 0 2505 Tm 8.05 0 Td 62.083333 Tz (oxidation. ) Tj 31.428571 0 0 31.428571 0 2384 Tm 22.590909 0 Td 80.429293 Tz (Scheme ) Tj 3.086364 0 Td 58.333333 Tz (4. ) Tj 40 0 0 40 0 2345.877347 Tm 8.475 0 Td 56.25 Tz (Proposed ) Tj 2.925 0 Td 62.5 Tz (Mechanism ) Tj 3.6 0 Td 47.222222 Tz (for ) Tj 0.975 0 Td 60.833333 Tz (Water ) Tj 1.95 0 Td 54.62963 Tz (Oxidation ) Tj 3.125 0 Td 60.416667 Tz (by ) Tj 0.925 0 Td 59.469697 Tz (Mononuclear ) Tj 4.1 0 Td 66.666667 Tz (Ru ) Tj 1 0 Td 58.854167 Tz (Complex. ) Tj 40 0 0 40 0 2276 Tm 12.875 0 Td 55.555556 Tz (Cei ) Tj 2.1 0 Td 44.444444 Tz (Hit ) Tj 6.1 0 Td 55.555556 Tz (Cei ) Tj 2.1 0 Td 44.444444 Tz (Hit ) Tj 51.142857 0 0 51.142857 0 2223.230769 Tm 7.821229 0 Td 57.572936 Tz (QH2 ) Tj 2.463687 0 Td 83.6437 Tz (\\u? ) Tj 3.773743 0 Td 68.435754 Tz (OH ) Tj 2.639665 0 Td 130.353818 Tz (NJ ) Tj 3.773743 0 Td 68.435754 Tz (O ) Tj 38.571429 0 0 38.571429 0 2168 Tm 10.37037 0 Td 59.053498 Tz (Rut ) Tj 8.27037 0 Td 69.135802 Tz (Rui ) Tj 8.503704 0 Td 59.053498 Tz (Rui ) Tj 40 0 0 40 0 2077 Tm 8.275 0 Td 91.666667 Tz (O ) Tj 88.095238 0 0 88.095238 0 2022.564516 Tm 4.336216 0 Td 71.891892 Tz (D ) Tj 8.048108 0 Td 56.756757 Tz (1 ) Tj 0.533514 0 Td 35.315315 Tz (cer ) Tj 38.571429 0 0 38.571429 0 1996 Tm 8.322222 0 Td 114.506173 Tz (HO ) Tj 31.428571 0 0 31.428571 0 1955.666667 Tm 14.636364 0 Td 111.363636 Tz (O ) Tj 9.672727 0 Td 111.363636 Tz (OH ) Tj 47.619048 0 0 47.619048 0 1923 Tm 8.4 0 Td 96.25 Tz (oa ) Tj 6.426 0 Td 91 Tz (o1 ) Tj 7.182 0 Td 73.5 Tz (O ) Tj 53.142857 0 0 53.142857 0 1850.057851 Tm 7.526882 0 Td 42.86141 Tz (Rui ) Tj 2.860215 0 Td 127.016129 Tz (rN ) Tj 2.897849 0 Td 50.179211 Tz (Rui ) Tj 4.215054 0 Td 122.311828 Tz (N ) Tj 2.22043 0 Td 51.747312 Tz (Ru ) Tj 42.857143 0 0 42.857143 0 1808.296296 Tm 12.693333 0 Td 40.185185 Tz (Hit ) Tj 1.586667 0 Td 60.277778 Tz (Ce ) Tj 6.253333 0 Td 81.666667 Tz (H ) Tj 1.82 0 Td 101.111111 Tz (HO ) Tj 40 0 0 40 0 1707 Tm 8.05 0 Td 70.075758 Tz (Conclusions ) Tj 51.428571 0 0 51.428571 0 1659.774398 Tm 7 0 Td 79.398148 Tz (We ) Tj 1.186111 0 Td 57.523148 Tz (have ) Tj 1.613889 0 Td 51.557239 Tz (synthesized ) Tj 3.616667 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 50.106838 Tz (characterized ) Tj 4.161111 0 Td 57.744108 Tz (mononuclear ) Tj 4.063889 0 Td 68.055556 Tz (Ru ) Tj 52.857143 0 0 52.857143 0 1622.214371 Tm 6.091892 0 Td 56.056056 Tz (complexes ) Tj 3.216216 0 Td 52.027027 Tz (with ) Tj 1.437838 0 Td 50.45045 Tz (a ) Tj 0.510811 0 Td 49.662162 Tz (pentadentate ) Tj 3.783784 0 Td 45.045045 Tz (ligand, ) Tj 2.118919 0 Td 57.545045 Tz (DIO-Bpy. ) Tj 2.97027 0 Td 62.274775 Tz (Compared ) Tj 51.428571 0 0 51.428571 0 1577.158025 Tm 6.241667 0 Td 45.37037 Tz (to ) Tj 0.855556 0 Td 64.814815 Tz (Ru ) Tj 0.991667 0 Td 60.185185 Tz (complex ) Tj 2.722222 0 Td 53.472222 Tz (with ) Tj 1.516667 0 Td 61.574074 Tz (DPA-Bpy, ) Tj 3.169444 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 46.990741 Tz (substitution ) Tj 3.597222 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 50.05144 Tz (pyridines ) Tj 51.428571 0 0 51.428571 0 1537.619753 Tm 6.261111 0 Td 45.37037 Tz (in ) Tj 0.836111 0 Td 66.203704 Tz (DPA-Bpy ) Tj 3.033333 0 Td 52.662037 Tz (with ) Tj 1.497222 0 Td 50.231481 Tz (isoquinoline ) Tj 3.830556 0 Td 54.552469 Tz (groups ) Tj 2.216667 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 64.351852 Tz (DIQ-Bpy ) Tj 2.955556 0 Td 48.206019 Tz (resulted ) Tj 58.571429 0 0 58.571429 0 1492.291557 Tm 5.497561 0 Td 41.260163 Tz (in ) Tj 0.785366 0 Td 49.512195 Tz (lower ) Tj 1.707317 0 Td 40.193089 Tz (activity ) Tj 2.185366 0 Td 42.682927 Tz (for ) Tj 1.007317 0 Td 48.373984 Tz (water ) Tj 1.673171 0 Td 44.896116 Tz (oxidation ) Tj 2.697561 0 Td 57.621951 Tz (when ) Tj 1.673171 0 Td 45.528455 Tz (using ) Tj 1.621951 0 Td 61.653117 Tz (Ce' ) Tj 1.45122 0 Td 44.105691 Tz (as ) Tj 51.428571 0 0 51.428571 0 1450.103448 Tm 6.261111 0 Td 54.282407 Tz (chemical ) Tj 2.819444 0 Td 49.421296 Tz (oxidant. ) Tj 2.586111 0 Td 63.734568 Tz (The ) Tj 1.380556 0 Td 44.965278 Tz (relative ) Tj 2.372222 0 Td 57.037037 Tz (lower ) Tj 1.866667 0 Td 45.37037 Tz (activity ) Tj 2.411111 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 61.574074 Tz (oxida ) Tj 51.428571 0 0 51.428571 0 1409.348052 Tm 6.241667 0 Td 47.800926 Tz (tion ) Tj 1.4 0 Td 59.953704 Tz (of ) Tj 0.894444 0 Td 55.092593 Tz (water ) Tj 1.886111 0 Td 53.148148 Tz (could ) Tj 1.905556 0 Td 44.830247 Tz (result ) Tj 1.886111 0 Td 56.712963 Tz (from ) Tj 1.652778 0 Td 49.691358 Tz (the ) Tj 1.166667 0 Td 52.391975 Tz (higher ) Tj 2.119444 0 Td 46.450617 Tz (potential ) Tj 2.819444 0 Td 58.333333 Tz (of ) Tj 0.875 0 Td 49.691358 Tz (the ) Tj 57.142857 0 0 57.142857 0 1370.523741 Tm 5.635 0 Td 70 Tz (Ru/ ) Tj 2.2575 0 Td 45.833333 Tz (couple, ) Tj 2.4675 0 Td 54.444444 Tz (making ) Tj 2.5025 0 Td 44.722222 Tz (the ) Tj 1.3125 0 Td 47.962963 Tz (formation ) Tj 3.115 0 Td 52.5 Tz (of ) Tj 1.085 0 Td 45.340909 Tz (high-valent ) Tj 58.571429 0 0 58.571429 0 1326.31746 Tm 5.497561 0 Td 76.260163 Tz (RuV=O ) Tj 2.509756 0 Td 44.308943 Tz (species ) Tj 2.082927 0 Td 39.837398 Tz (less ) Tj 1.143902 0 Td 43.821138 Tz (accessible ) Tj 2.817073 0 Td 52.642276 Tz (by ) Tj 0.853659 0 Td 54.776423 Tz (Ce'. ) Tj 51.428571 0 0 51.428571 0 1250.263158 Tm 11.9 0 Td 54.012346 Tz (Experimental ) Tj 4.180556 0 Td 48.148148 Tz (Details ) Tj 51.428571 0 0 51.428571 0 1165.351032 Tm 6.261111 0 Td 50.771605 Tz (Materials ) Tj 2.975 0 Td 60.493827 Tz (and ) Tj 1.322222 0 Td 51.131687 Tz (Synthesis ) Tj 51.428571 0 0 51.428571 0 1123.885714 Tm 7 0 Td 50.771605 Tz (All ) Tj 1.186111 0 Td 54.012346 Tz (chemicals ) Tj 3.247222 0 Td 58.333333 Tz (were ) Tj 1.672222 0 Td 55.092593 Tz (purchased ) Tj 3.266667 0 Td 57.523148 Tz (from ) Tj 1.711111 0 Td 55.092593 Tz (Sigma-Aldrich ) Tj 4.588889 0 Td 60.493827 Tz (and ) Tj 51.428571 0 0 51.428571 0 1082.553325 Tm 6.261111 0 Td 54.768519 Tz (Alfa-Aesar ) Tj 3.5 0 Td 52.932099 Tz (except ) Tj 2.197222 0 Td 48.611111 Tz (noted. ) Tj 2.041667 0 Td 56.388889 Tz (Other ) Tj 1.925 0 Td 50.231481 Tz (reagents ) Tj 2.722222 0 Td 54.282407 Tz (such ) Tj 1.575 0 Td 48.611111 Tz (as ) Tj 0.933333 0 Td 53.472222 Tz (1-methyl ) Tj 51.428571 0 0 51.428571 0 1039 Tm 6.261111 0 Td 48.361823 Tz (isoquinoline, ) Tj 4.394444 0 Td 63.842593 Tz (RuC1.3H2O, ) Tj 4.413889 0 Td 78.367003 Tz (\(NH\)Ce\(NO\), ) Tj 5.736111 0 Td 58.333333 Tz (and ) Tj 1.652778 0 Td 42.12963 Tz (2,2'- ) Tj 51.428571 0 0 51.428571 0 999.056287 Tm 6.261111 0 Td 49.331276 Tz (dipyridyl ) Tj 2.838889 0 Td 59.953704 Tz (were ) Tj 1.613889 0 Td 55.092593 Tz (used ) Tj 1.477778 0 Td 51.851852 Tz (as ) Tj 0.816667 0 Td 51.041667 Tz (received ) Tj 2.644444 0 Td 52.777778 Tz (without ) Tj 2.411111 0 Td 47.222222 Tz (further ) Tj 2.1 0 Td 45.37037 Tz (purification. ) Tj 51.428571 0 0 51.428571 0 956.148252 Tm 6.261111 0 Td 52.777778 Tz (Milli-Q ) Tj 2.702778 0 Td 106.944444 Tz (HO ) Tj 1.711111 0 Td 50.555556 Tz (\(18.2 ) Tj 1.963889 0 Td 59.953704 Tz (MS2\) ) Tj 1.886111 0 Td 61.574074 Tz (was ) Tj 1.536111 0 Td 55.902778 Tz (used ) Tj 1.788889 0 Td 45.37037 Tz (in ) Tj 0.972222 0 Td 39.969136 Tz (all ) Tj 1.147222 0 Td 51.851852 Tz (experiments. ) Tj 51.428571 0 0 51.428571 0 917.278772 Tm 6.280556 0 Td 53.292181 Tz (Syntheses ) Tj 3.344444 0 Td 58.333333 Tz (of ) Tj 1.05 0 Td 59.511785 Tz (bromomethyl ) Tj 4.394444 0 Td 48.905724 Tz (isoquinline ) Tj 3.675 0 Td 58.333333 Tz (and ) Tj 1.555556 0 Td 63.374486 Tz (6-\(aminom ) Tj 51.428571 0 0 51.428571 0 875.503632 Tm 6.261111 0 Td 47.138047 Tz (ethyl\)-2,2'-bipyridine ) Tj 6.513889 0 Td 58.333333 Tz (were ) Tj 1.672222 0 Td 48.148148 Tz (carried ) Tj 2.313889 0 Td 52.932099 Tz (out ) Tj 1.244444 0 Td 52.211934 Tz (following ) Tj 3.091667 0 Td 44.074074 Tz (literature ) Tj 51.428571 0 0 51.428571 0 830.367232 Tm 6.261111 0 Td 57.87037 Tz (methods ) Tj 2.8 0 Td 43.75 Tz (\(\(a\) ) Tj 1.4 0 Td 48.611111 Tz (Z. ) Tj 0.933333 0 Td 49.016204 Tz (Tyeklar, ) Tj 2.741667 0 Td 50.231481 Tz (R. ) Tj 1.011111 0 Td 48.611111 Tz (R. ) Tj 0.952778 0 Td 52.572016 Tz (Jacobson, ) Tj 3.208333 0 Td 55.092593 Tz (N. ) Tj 0.991667 0 Td 55.902778 Tz (Wei, ) Tj 1.691667 0 Td 55.092593 Tz (N. ) Tj 1.05 0 Td 55.092593 Tz (N. ) Tj 51.428571 0 0 51.428571 0 789.245383 Tm 6.261111 0 Td 54.62963 Tz (Murthy, ) Tj 2.547222 0 Td 37.268519 Tz (J. ) Tj 0.719444 0 Td 49.016204 Tz (Zubieta, ) Tj 2.644444 0 Td 53.472222 Tz (K. ) Tj 0.933333 0 Td 53.472222 Tz (D. ) Tj 0.952778 0 Td 47.222222 Tz (Karlin, ) Tj 2.216667 0 Td 37.268519 Tz (J. ) Tj 0.680556 0 Td 68.055556 Tz (Am. ) Tj 1.458333 0 Td 64.166667 Tz (Chem. ) Tj 2.177778 0 Td 51.851852 Tz (Soc. ) Tj 1.575 0 Td 51.203704 Tz (1993, ) Tj 51.428571 0 0 51.428571 0 747.302096 Tm 6.319444 0 Td 49.421296 Tz (115, ) Tj 1.361111 0 Td 55.740741 Tz (2677-2689; ) Tj 3.558333 0 Td 50.231481 Tz (b\) ) Tj 0.758333 0 Td 50.231481 Tz (Y. ) Tj 0.797222 0 Td 52.662037 Tz (Gultneh, ) Tj 2.683333 0 Td 46.990741 Tz (T. ) Tj 0.816667 0 Td 51.851852 Tz (B. ) Tj 0.777778 0 Td 53.472222 Tz (Yisgedu, ) Tj 2.722222 0 Td 56.712963 Tz (Y.T. ) Tj 1.516667 0 Td 56.944444 Tz (Tesema, ) Tj 51.428571 0 0 51.428571 0 705.965706 Tm 6.261111 0 Td 53.472222 Tz (R. ) Tj 1.011111 0 Td 37.268519 Tz (J. ) Tj 0.875 0 Td 50.231481 Tz (Butcher, ) Tj 2.8 0 Td 47.530864 Tz (Inorg. ) Tj 2.041667 0 Td 64.814815 Tz (Chem. ) Tj 2.294444 0 Td 54.444444 Tz (2003, ) Tj 1.983333 0 Td 50.771605 Tz (42, ) Tj 1.322222 0 Td 55.092593 Tz (1857-1867; ) Tj 3.636111 0 Td 50.231481 Tz (c\) ) Tj 0.913889 0 Td 46.990741 Tz (T. ) Tj 51.428571 0 0 51.428571 0 666.693878 Tm 6.261111 0 Td 58.333333 Tz (Murashima, ) Tj 3.713889 0 Td 45.37037 Tz (S. ) Tj 0.777778 0 Td 55.416667 Tz (Tsukiyama, ) Tj 3.558333 0 Td 46.990741 Tz (S. ) Tj 0.836111 0 Td 42.12963 Tz (Fujii, ) Tj 1.769444 0 Td 53.472222 Tz (K. ) Tj 0.913889 0 Td 52.314815 Tz (Hayata, ) Tj 2.45 0 Td 51.851852 Tz (H. ) Tj 0.894444 0 Td 49.151235 Tz (Sakai, ) Tj 1.963889 0 Td 46.990741 Tz (T. ) Tj 51.428571 0 0 51.428571 0 623.297542 Tm 6.261111 0 Td 59.41358 Tz (Miyazawa, ) Tj 3.461111 0 Td 46.990741 Tz (T. ) Tj 0.875 0 Td 59.722222 Tz (Yamada, ) Tj 2.8 0 Td 61.574074 Tz (Org ) Tj 1.458333 0 Td 58.873457 Tz (Biomol ) Tj 2.411111 0 Td 71.296296 Tz (Chem ) Tj 2.041667 0 Td 52.5 Tz (2005, ) Tj 1.886111 0 Td 45.37037 Tz (3, ) Tj 0.836111 0 Td 70.486111 Tz (4060 ) Tj 51.428571 0 0 51.428571 0 580 Tm 6.261111 0 Td 50 Tz (4064\)\). ) Tj 51.428571 0 0 51.428571 0 508.598372 Tm 7.641667 0 Td 51.131687 Tz (Synthesis ) Tj 2.994444 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 50.231481 Tz (N,N-bis\(\(isoquinolin-1-yl\)methyl\)\(6- ) Tj 51.428571 0 0 51.428571 0 467 Tm 7.447222 0 Td 51.169591 Tz (\(pyridin-2-yl\)pyridin-2-yl\)methanamine ) Tj 11.919444 0 Td 59.053498 Tz (\(DIQ-Bpy\) ) Tj 51.428571 0 0 51.428571 0 381.821935 Tm 7 0 Td 61.574074 Tz (To ) Tj 1.186111 0 Td 51.851852 Tz (a ) Tj 0.758333 0 Td 48.206019 Tz (solution ) Tj 2.741667 0 Td 61.574074 Tz (of ) Tj 1.069444 0 Td 50.771605 Tz (\(6-\(pyridin-2-yl\)pyridin-2-yl\)methan ) Tj 51.428571 0 0 51.428571 0 339.198511 Tm 6.261111 0 Td 59.62963 Tz (amine ) Tj 2.041667 0 Td 49.259259 Tz (\(0.25 ) Tj 1.788889 0 Td 45.37037 Tz (g, ) Tj 0.875 0 Td 49.421296 Tz (1.35 ) Tj 1.497222 0 Td 63.518519 Tz (mmol\) ) Tj 2.158333 0 Td 60.493827 Tz (and ) Tj 1.419444 0 Td 55.6562 Tz (1-\(bromomethyl\)isoquino ) Tj 51.428571 0 0 51.428571 0 293.276215 Tm 6.261111 0 Td 46.180556 Tz (line ) Tj 1.322222 0 Td 49.907407 Tz (\(0.75 ) Tj 1.711111 0 Td 43.75 Tz (g, ) Tj 0.777778 0 Td 52.662037 Tz (3.37 ) Tj 1.497222 0 Td 64.814815 Tz (mmol\) ) Tj 2.158333 0 Td 43.75 Tz (in ) Tj 0.777778 0 Td 45.37037 Tz (acetonitrile ) Tj 3.5 0 Td 54.012346 Tz (\(10 ) Tj 1.186111 0 Td 68.055556 Tz (mL\) ) Tj 1.458333 0 Td 61.574074 Tz (was ) Tj 1.341667 0 Td 58.981481 Tz (added ) Tj 51.428571 0 0 51.428571 0 253.72679 Tm 6.261111 0 Td 49.151235 Tz (di-isopropyl ) Tj 3.888889 0 Td 48.611111 Tz (ethyl ) Tj 1.769444 0 Td 60.277778 Tz (amine ) Tj 2.158333 0 Td 49.259259 Tz (\(0.69 ) Tj 1.866667 0 Td 63.734568 Tz (mL, ) Tj 1.497222 0 Td 51.851852 Tz (3.98 ) Tj 1.633333 0 Td 64.166667 Tz (mmol\) ) Tj 2.255556 0 Td 43.75 Tz (at ) Tj 0.875 0 Td 64.00463 Tz (room ) Tj 51.428571 0 0 51.428571 0 212.032432 Tm 6.241667 0 Td 50.771605 Tz (temperature. ) Tj 4.083333 0 Td 63.734568 Tz (The ) Tj 1.575 0 Td 48.611111 Tz (reaction ) Tj 2.819444 0 Td 53.240741 Tz (mixture ) Tj 2.683333 0 Td 60.493827 Tz (was ) Tj 1.555556 0 Td 43.981481 Tz (stirred ) Tj 2.275 0 Td 45.37037 Tz (at ) Tj 0.952778 0 Td 64.00463 Tz (room ) Tj 51.428571 0 0 51.428571 0 171.628025 Tm 6.241667 0 Td 51.041667 Tz (temperature, ) Tj 3.986111 0 Td 59.41358 Tz (and ) Tj 1.380556 0 Td 49.691358 Tz (the ) Tj 1.225 0 Td 47.800926 Tz (reaction ) Tj 2.625 0 Td 51.851852 Tz (progress ) Tj 2.780556 0 Td 62.654321 Tz (was ) Tj 1.497222 0 Td 54.73251 Tz (monitored ) Tj 3.247222 0 Td 63.194444 Tz (by ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 75.675676 Tz (32 ) Tj 51.428571 0 0 51.428571 0 2916.373134 Tm 25.2 0 Td 64.00463 Tz (TLC. ) Tj 1.769444 0 Td 66.435185 Tz (Upon ) Tj 1.808333 0 Td 54.444444 Tz (completion ) Tj 3.480556 0 Td 59.953704 Tz (of ) Tj 0.816667 0 Td 49.691358 Tz (the ) Tj 1.108333 0 Td 48.206019 Tz (reaction ) Tj 2.527778 0 Td 55.092593 Tz (\(-2 ) Tj 1.225 0 Td 48.070988 Tz (days\), ) Tj 1.944444 0 Td 54.444444 Tz (water ) Tj 1.827778 0 Td 52.932099 Tz (\(50 ) Tj 51.428571 0 0 51.428571 0 2875.846902 Tm 25.2 0 Td 70.216049 Tz (mL\) ) Tj 1.419444 0 Td 61.574074 Tz (was ) Tj 1.283333 0 Td 52.391975 Tz (added. ) Tj 2.061111 0 Td 62.654321 Tz (The ) Tj 1.283333 0 Td 53.240741 Tz (product ) Tj 2.411111 0 Td 60.493827 Tz (was ) Tj 1.263889 0 Td 49.331276 Tz (extracted ) Tj 2.838889 0 Td 46.180556 Tz (into ) Tj 1.263889 0 Td 48.611111 Tz (ethyl ) Tj 1.594444 0 Td 49.074074 Tz (acetate ) Tj 51.428571 0 0 51.428571 0 2834 Tm 25.219444 0 Td 57.685185 Tz (\(3x50 ) Tj 2.022222 0 Td 69.135802 Tz (mL\) ) Tj 1.536111 0 Td 58.333333 Tz (and ) Tj 1.361111 0 Td 60.493827 Tz (washed ) Tj 2.469444 0 Td 53.472222 Tz (with ) Tj 1.575 0 Td 50.555556 Tz (brine ) Tj 1.827778 0 Td 57.685185 Tz (\(2x30 ) Tj 2.022222 0 Td 58.333333 Tz (mL\). ) Tj 1.691667 0 Td 63.734568 Tz (The ) Tj 1.419444 0 Td 84.259259 Tz (com ) Tj 52.857143 0 0 52.857143 0 2797.616858 Tm 24.5 0 Td 52.972973 Tz (bined ) Tj 1.910811 0 Td 49.54955 Tz (organic ) Tj 2.421622 0 Td 46.246246 Tz (layers ) Tj 1.967568 0 Td 57.545045 Tz (were ) Tj 1.683784 0 Td 48.558559 Tz (dried ) Tj 1.778378 0 Td 52.027027 Tz (over ) Tj 1.532432 0 Td 54.654655 Tz (anhydrous ) Tj 3.254054 0 Td 81.351351 Tz (NaSO, ) Tj 51.428571 0 0 51.428571 0 2758.665025 Tm 25.2 0 Td 41.049383 Tz (filtered, ) Tj 2.488889 0 Td 53.472222 Tz (evaporated ) Tj 3.441667 0 Td 56.388889 Tz (under ) Tj 1.905556 0 Td 55.092593 Tz (reduced ) Tj 2.527778 0 Td 48.251029 Tz (pressure, ) Tj 2.877778 0 Td 60.493827 Tz (and ) Tj 1.302778 0 Td 51.851852 Tz (then ) Tj 1.497222 0 Td 59.143519 Tz (puri ) Tj 51.428571 0 0 51.428571 0 2719.53715 Tm 25.2 0 Td 45.37037 Tz (fied ) Tj 1.283333 0 Td 61.574074 Tz (by ) Tj 0.952778 0 Td 60.493827 Tz (column ) Tj 2.391667 0 Td 56.481481 Tz (chromatography ) Tj 4.977778 0 Td 48.070988 Tz (\(basic ) Tj 1.925 0 Td 54.282407 Tz (alumina\) ) Tj 2.819444 0 Td 52.5 Tz (using ) Tj 1.808333 0 Td 72.376543 Tz (60% ) Tj 51.428571 0 0 51.428571 0 2679.340768 Tm 25.2 0 Td 48.341049 Tz (ethylacetate ) Tj 3.694444 0 Td 45.37037 Tz (in ) Tj 0.738889 0 Td 56.018519 Tz (hexanes ) Tj 2.547222 0 Td 50.231481 Tz (as ) Tj 0.797222 0 Td 50.771605 Tz (eluent ) Tj 2.002778 0 Td 46.990741 Tz (to ) Tj 0.777778 0 Td 48.070988 Tz (afford ) Tj 1.905556 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 64.00463 Tz (compound ) Tj 3.266667 0 Td 50.231481 Tz (as ) Tj 51.428571 0 0 51.428571 0 2642.432225 Tm 25.2 0 Td 44.722222 Tz (light ) Tj 1.613889 0 Td 54.012346 Tz (yellow ) Tj 2.255556 0 Td 43.75 Tz (solid. ) Tj 1.905556 0 Td 47.848584 Tz (Recrystallization ) Tj 5.191667 0 Td 42.12963 Tz (in ) Tj 0.816667 0 Td 52.932099 Tz (hot ) Tj 1.186111 0 Td 50.555556 Tz (ether ) Tj 1.730556 0 Td 51.388889 Tz (yielded ) Tj 2.45 0 Td 55.092593 Tz (a ) Tj 58.571429 0 0 58.571429 0 2597.328125 Tm 22.109756 0 Td 47.804878 Tz (white ) Tj 1.639024 0 Td 41.544715 Tz (solid ) Tj 1.468293 0 Td 43.252033 Tz (\(0.47 ) Tj 1.502439 0 Td 39.837398 Tz (g, ) Tj 0.717073 0 Td 50.650407 Tz (75%\). ) Tj 1.77561 0 Td 55.487805 Tz ("H ) Tj 0.887805 0 Td 81.571816 Tz (NMR ) Tj 1.656098 0 Td 58.333333 Tz (\(CDC1, ) Tj 2.321951 0 Td 53.116531 Tz (500 ) Tj 1.160976 0 Td 55.772358 Tz (MHz\): ) Tj 1.946341 0 Td 45.528455 Tz (8 ) Tj 51.428571 0 0 51.428571 0 2562.785894 Tm 25.2 0 Td 52.662037 Tz (3.99 ) Tj 1.477778 0 Td 37.808642 Tz (\(s. ) Tj 0.913889 0 Td 56.17284 Tz (2H, ) Tj 1.205556 0 Td 49.691358 Tz (bipyridyl ) Tj 2.936111 0 Td 53.935185 Tz (methylene-H8\), ) Tj 4.763889 0 Td 48.611111 Tz (6 ) Tj 0.525 0 Td 49.421296 Tz (4.41 ) Tj 1.458333 0 Td 38.888889 Tz (\(s, ) Tj 0.894444 0 Td 59.41358 Tz (4H, ) Tj 1.263889 0 Td 56.17284 Tz (isoqui ) Tj 51.428571 0 0 51.428571 0 2521.077707 Tm 25.219444 0 Td 50.231481 Tz (noline ) Tj 2.002778 0 Td 53.472222 Tz (methylene, ) Tj 3.461111 0 Td 51.851852 Tz (H1\), ) Tj 1.458333 0 Td 52.662037 Tz (7.08 ) Tj 1.497222 0 Td 38.888889 Tz (\(d. ) Tj 0.952778 0 Td 53.148148 Tz (J=6.7 ) Tj 1.847222 0 Td 55.092593 Tz (Hz, ) Tj 1.283333 0 Td 54.012346 Tz (1H, ) Tj 1.166667 0 Td 55.497685 Tz (bpy-H9\), ) Tj 2.877778 0 Td 45.37037 Tz (7.1 ) Tj 51.428571 0 0 51.428571 0 2480.283804 Tm 25.219444 0 Td 33.487654 Tz (\(t, ) Tj 0.991667 0 Td 52.5 Tz (J=7.3 ) Tj 2.061111 0 Td 52.932099 Tz (Hz, ) Tj 1.438889 0 Td 55.092593 Tz (1H, ) Tj 1.4 0 Td 50 Tz (iq-H3\), ) Tj 2.527778 0 Td 52.662037 Tz (7.29 ) Tj 1.672222 0 Td 40.509259 Tz (\(td, ) Tj 1.361111 0 Td 49.151235 Tz (J4.6, ) Tj 2.216667 0 Td 49.691358 Tz (5.9 ) Tj 1.322222 0 Td 54.012346 Tz (HZ, ) Tj 1.438889 0 Td 55.092593 Tz (1H, ) Tj 51.428571 0 0 51.428571 0 2441.704225 Tm 25.180556 0 Td 55.812757 Tz (bpy-H14\), ) Tj 3.227778 0 Td 52.662037 Tz (7.54 ) Tj 1.497222 0 Td 38.888889 Tz (\(d. ) Tj 0.952778 0 Td 53.796296 Tz (J=5.6 ) Tj 1.866667 0 Td 55.092593 Tz (Hz, ) Tj 1.166667 0 Td 60.493827 Tz (2H, ) Tj 1.302778 0 Td 50.462963 Tz (iq-H6\), ) Tj 2.333333 0 Td 51.851852 Tz (7.56 ) Tj 1.477778 0 Td 32.407407 Tz (\(t, ) Tj 0.816667 0 Td 53.796296 Tz (J=7.7 ) Tj 1.866667 0 Td 52.932099 Tz (Hz, ) Tj 51.428571 0 0 51.428571 0 2402.690722 Tm 25.258333 0 Td 55.092593 Tz (1H, ) Tj 1.225 0 Td 49.537037 Tz (iq-H4\), ) Tj 2.333333 0 Td 51.851852 Tz (7.64 ) Tj 1.438889 0 Td 34.567901 Tz (\(t, ) Tj 0.816667 0 Td 54.444444 Tz (J7.7 ) Tj 1.847222 0 Td 55.092593 Tz (Hz, ) Tj 1.263889 0 Td 55.092593 Tz (1H, ) Tj 1.186111 0 Td 55.452675 Tz (bpy-H10\), ) Tj 3.247222 0 Td 51.851852 Tz (7.75 ) Tj 1.477778 0 Td 39.969136 Tz (\(d. ) Tj 0.972222 0 Td 52.5 Tz (J=8.2 ) Tj 51.428571 0 0 51.428571 0 2362.801061 Tm 25.2 0 Td 57.253086 Tz (Hz, ) Tj 1.283333 0 Td 59.41358 Tz (2H, ) Tj 1.322222 0 Td 50.462963 Tz (iq-H5\), ) Tj 2.411111 0 Td 51.041667 Tz (7.78 ) Tj 1.516667 0 Td 33.487654 Tz (\(t, ) Tj 0.855556 0 Td 53.148148 Tz (J7.7 ) Tj 1.886111 0 Td 56.17284 Tz (Hz, ) Tj 1.341667 0 Td 55.092593 Tz (1H, ) Tj 1.244444 0 Td 55.812757 Tz (bpy-H13\), ) Tj 3.286111 0 Td 52.662037 Tz (7.89 ) Tj 1.555556 0 Td 41.049383 Tz (\(d. ) Tj 51.428571 0 0 51.428571 0 2323.623441 Tm 25.2 0 Td 53.796296 Tz (J=8.4 ) Tj 1.808333 0 Td 54.012346 Tz (Hz, ) Tj 1.147222 0 Td 58.333333 Tz (2H, ) Tj 1.225 0 Td 50.462963 Tz (iq-H2\), ) Tj 2.294444 0 Td 51.851852 Tz (8.23 ) Tj 1.438889 0 Td 41.049383 Tz (\(d. ) Tj 0.913889 0 Td 53.796296 Tz (J=7.7 ) Tj 1.847222 0 Td 54.012346 Tz (Hz, ) Tj 1.186111 0 Td 56.17284 Tz (1H, ) Tj 1.166667 0 Td 55.452675 Tz (bpy-H11\), ) Tj 3.15 0 Td 52.662037 Tz (8.39 ) Tj 51.428571 0 0 51.428571 0 2283.715215 Tm 25.219444 0 Td 39.969136 Tz (\(d. ) Tj 0.972222 0 Td 53.796296 Tz (J=8.0 ) Tj 1.866667 0 Td 52.932099 Tz (Hz, ) Tj 1.263889 0 Td 54.012346 Tz (1H, ) Tj 1.205556 0 Td 55.452675 Tz (bpy-H12\), ) Tj 3.188889 0 Td 53.472222 Tz (8.45 ) Tj 1.497222 0 Td 41.049383 Tz (\(d. ) Tj 0.991667 0 Td 53.796296 Tz (J=5.6 ) Tj 1.886111 0 Td 51.851852 Tz (Hz, ) Tj 1.166667 0 Td 58.333333 Tz (2H, ) Tj 1.302778 0 Td 49.537037 Tz (iq-H7\), ) Tj 51.428571 0 0 51.428571 0 2243.710345 Tm 25.219444 0 Td 52.662037 Tz (8.66 ) Tj 1.652778 0 Td 39.969136 Tz (\(d. ) Tj 1.127778 0 Td 54.444444 Tz (J4.6 ) Tj 2.061111 0 Td 54.012346 Tz (Hz, ) Tj 1.419444 0 Td 56.17284 Tz (1H, ) Tj 1.380556 0 Td 55.812757 Tz (bpy-H15\). ) Tj 3.422222 0 Td 60.185185 Tz (ESI-MS: ) Tj 2.975 0 Td 56.712963 Tz (m/z" ) Tj 1.769444 0 Td 53.148148 Tz (468.3 ) Tj 52.857143 0 0 52.857143 0 2202 Tm 24.537838 0 Td 47.822823 Tz (\(calcd ) Tj 2.572973 0 Td 47.927928 Tz (m/z-- ) Tj 2.289189 0 Td 47.297297 Tz (for ) Tj 1.872973 0 Td 68.318318 Tz (M+1468.2. ) Tj 4.540541 0 Td 49.81982 Tz (Anal. ) Tj 2.364865 0 Td 55.495495 Tz (Calcd ) Tj 2.516216 0 Td 47.297297 Tz (for ) Tj 52.857143 0 0 52.857143 0 2162 Tm 24.518919 0 Td 117.717718 Tz (CHNOs: ) Tj 4.635135 0 Td 55.18018 Tz (C, ) Tj 1.059459 0 Td 48.348348 Tz (78.13; ) Tj 2.175676 0 Td 55.18018 Tz (H, ) Tj 1.059459 0 Td 46.036036 Tz (5.50; ) Tj 1.816216 0 Td 53.603604 Tz (N, ) Tj 1.135135 0 Td 46.771772 Tz (14.70. ) Tj 2.1 0 Td 54.129129 Tz (Found: ) Tj 2.364865 0 Td 52.027027 Tz (C, ) Tj 47.142857 0 0 47.142857 0 2125 Tm 27.490909 0 Td 54.79798 Tz (78.37; ) Tj 2.269697 0 Td 63.636364 Tz (H, ) Tj 1.060606 0 Td 51.616162 Tz (5.41; ) Tj 1.845455 0 Td 61.868687 Tz (N, ) Tj 1.10303 0 Td 52.441077 Tz (14.68. ) Tj 51.428571 0 0 51.428571 0 2051.547619 Tm 26.930556 0 Td 51.131687 Tz (Synthesis ) Tj 2.975 0 Td 59.953704 Tz (of ) Tj 1.088889 0 Td 58.333333 Tz (Ru\(DIQ-Bpy\)\(Cl\)Cl. ) Tj 6.397222 0 Td 82.314815 Tz (\(HO\)s ) Tj 2.741667 0 Td 45.37037 Tz (\(6\) ) Tj 51.428571 0 0 51.428571 0 1968.777778 Tm 25.919444 0 Td 87.5 Tz (A ) Tj 0.719444 0 Td 48.206019 Tz (solution ) Tj 2.527778 0 Td 61.574074 Tz (of ) Tj 0.894444 0 Td 63.888889 Tz (DIQ-Bpy ) Tj 2.916667 0 Td 51.203704 Tz (\(0.30 ) Tj 1.730556 0 Td 45.37037 Tz (g, ) Tj 0.777778 0 Td 51.851852 Tz (0.64 ) Tj 1.516667 0 Td 64.166667 Tz (mmol\) ) Tj 2.119444 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 61.574074 Tz (50 ) Tj 0.952778 0 Td 82.638889 Tz (mL ) Tj 1.166667 0 Td 59.953704 Tz (of ) Tj 51.428571 0 0 51.428571 0 1929.403329 Tm 25.2 0 Td 50.462963 Tz (ethanol ) Tj 2.45 0 Td 60.493827 Tz (was ) Tj 1.380556 0 Td 58.333333 Tz (added ) Tj 2.041667 0 Td 55.497685 Tz (dropwise ) Tj 2.936111 0 Td 45.37037 Tz (to ) Tj 0.816667 0 Td 55.092593 Tz (a ) Tj 0.622222 0 Td 48.611111 Tz (solution ) Tj 2.625 0 Td 59.953704 Tz (of ) Tj 0.952778 0 Td 67.335391 Tz (RuC1.3H2O ) Tj 51.428571 0 0 51.428571 0 1888.297521 Tm 25.219444 0 Td 51.851852 Tz (\(0.167 ) Tj 2.158333 0 Td 43.75 Tz (g. ) Tj 0.875 0 Td 51.851852 Tz (0.64 ) Tj 1.594444 0 Td 64.166667 Tz (mmol\) ) Tj 2.236111 0 Td 43.75 Tz (in ) Tj 0.836111 0 Td 63.194444 Tz (80 ) Tj 1.088889 0 Td 81.018519 Tz (mL ) Tj 1.244444 0 Td 59.953704 Tz (of ) Tj 0.913889 0 Td 50.925926 Tz (ethanol ) Tj 2.45 0 Td 45.37037 Tz (that ) Tj 1.4 0 Td 52.932099 Tz (has ) Tj 1.263889 0 Td 58.333333 Tz (been ) Tj 51.428571 0 0 51.428571 0 1850.948856 Tm 25.2 0 Td 49.826389 Tz (refluxed ) Tj 2.683333 0 Td 47.530864 Tz (for ) Tj 1.108333 0 Td 63.194444 Tz (30 ) Tj 1.05 0 Td 59.41358 Tz (min ) Tj 1.380556 0 Td 55.092593 Tz (over ) Tj 1.575 0 Td 51.851852 Tz (a ) Tj 0.622222 0 Td 51.851852 Tz (period ) Tj 2.119444 0 Td 61.574074 Tz (of ) Tj 0.913889 0 Td 61.574074 Tz (30 ) Tj 1.05 0 Td 59.41358 Tz (min ) Tj 1.380556 0 Td 55.740741 Tz (under ) Tj 1.944444 0 Td 55.092593 Tz (argon ) Tj 51.428571 0 0 51.428571 0 1810.82048 Tm 25.2 0 Td 53.030303 Tz (atmosphere. ) Tj 3.733333 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 47.800926 Tz (reaction ) Tj 2.566667 0 Td 53.240741 Tz (mixture ) Tj 2.488889 0 Td 61.574074 Tz (was ) Tj 1.361111 0 Td 51.041667 Tz (then ) Tj 1.497222 0 Td 49.016204 Tz (refluxed ) Tj 2.586111 0 Td 48.611111 Tz (for ) Tj 1.166667 0 Td 51.851852 Tz (12 ) Tj 51.428571 0 0 51.428571 0 1772.757946 Tm 25.180556 0 Td 45.37037 Tz (h. ) Tj 0.719444 0 Td 52.5 Tz (After ) Tj 1.75 0 Td 41.481481 Tz (filtration ) Tj 2.702778 0 Td 53.703704 Tz (through ) Tj 2.469444 0 Td 45.37037 Tz (Celite, ) Tj 2.119444 0 Td 49.691358 Tz (the ) Tj 1.088889 0 Td 39.293981 Tz (filtrate ) Tj 2.1 0 Td 62.654321 Tz (was ) Tj 1.341667 0 Td 53.796296 Tz (evaporated ) Tj 51.428571 0 0 51.428571 0 1731.433155 Tm 25.180556 0 Td 57.037037 Tz (under ) Tj 2.080556 0 Td 54.62963 Tz (reduced ) Tj 2.605556 0 Td 48.251029 Tz (pressure. ) Tj 2.975 0 Td 63.734568 Tz (The ) Tj 1.536111 0 Td 49.074074 Tz (residue ) Tj 2.430556 0 Td 61.574074 Tz (was ) Tj 1.497222 0 Td 50.771605 Tz (dissolved ) Tj 3.111111 0 Td 45.37037 Tz (in ) Tj 0.913889 0 Td 55.092593 Tz (a ) Tj 40 0 0 40 0 1699 Tm 32.4 0 Td 85.714286 Tz (minimum ) Tj 4.125 0 Td 63.690476 Tz (soluble ) Tj 3.1 0 Td 79.166667 Tz (amount ) Tj 3.325 0 Td 72.916667 Tz (of ) Tj 1.275 0 Td 71.354167 Tz (methanol ) Tj 3.85 0 Td 77.777778 Tz (and ) Tj 1.875 0 Td 77.083333 Tz (washed ) Tj 3.25 0 Td 68.75 Tz (with ) Tj 51.428571 0 0 51.428571 0 1653.563204 Tm 25.2 0 Td 48.611111 Tz (diethylether ) Tj 3.675 0 Td 57.523148 Tz (\(-70 ) Tj 1.575 0 Td 68.055556 Tz (mL\) ) Tj 1.380556 0 Td 50.771605 Tz (for ) Tj 1.030556 0 Td 55.092593 Tz (3-4 ) Tj 1.166667 0 Td 51.203704 Tz (times ) Tj 1.75 0 Td 45.37037 Tz (to ) Tj 0.738889 0 Td 49.259259 Tz (yield ) Tj 1.633333 0 Td 55.092593 Tz (a ) Tj 0.525 0 Td 54.282407 Tz (dark ) Tj 1.477778 0 Td 50.771605 Tz (red ) Tj 1.108333 0 Td 47.314815 Tz (solid ) Tj 58.571429 0 0 58.571429 0 1612.310127 Tm 22.143902 0 Td 46.747967 Tz (\(0.34g, ) Tj 2.134146 0 Td 42.682927 Tz (Yield, ) Tj 1.72439 0 Td 51.219512 Tz (77%\). ) Tj 1.980488 0 Td 73.98374 Tz (H ) Tj 0.64878 0 Td 80.623306 Tz (NMR ) Tj 1.639024 0 Td 65.921409 Tz (\(CDCN, ) Tj 2.578049 0 Td 52.168022 Tz (500 ) Tj 1.109756 0 Td 56.341463 Tz (MHz\): ) Tj 1.929268 0 Td 51.788618 Tz (85.08 ) Tj 51.428571 0 0 51.428571 0 1574.880052 Tm 25.219444 0 Td 35.648148 Tz (\(s. ) Tj 0.972222 0 Td 58.333333 Tz (2H, ) Tj 1.341667 0 Td 49.691358 Tz (bipyridyl ) Tj 2.994444 0 Td 54.166667 Tz (methylene-H8\), ) Tj 4.880556 0 Td 51.851852 Tz (5.59 ) Tj 1.536111 0 Td 41.049383 Tz (\(d. ) Tj 1.05 0 Td 55.092593 Tz (J=15.6 ) Tj 2.333333 0 Td 54.012346 Tz (Hz, ) Tj 1.263889 0 Td 58.333333 Tz (2H, ) Tj 51.428571 0 0 51.428571 0 1536.204744 Tm 25.2 0 Td 46.666667 Tz (axial ) Tj 1.652778 0 Td 50.231481 Tz (isoquinoline ) Tj 3.869444 0 Td 54.398148 Tz (methylene-H1\), ) Tj 4.841667 0 Td 51.851852 Tz (5.96 ) Tj 1.497222 0 Td 39.969136 Tz (\(d. ) Tj 1.030556 0 Td 54.552469 Tz (J=15.6 ) Tj 2.236111 0 Td 56.17284 Tz (Hz, ) Tj 1.263889 0 Td 58.333333 Tz (2H, ) Tj 51.428571 0 0 51.428571 0 1495.62406 Tm 25.2 0 Td 46.018519 Tz (equitorial ) Tj 3.091667 0 Td 49.96142 Tz (isoquinoline ) Tj 3.927778 0 Td 54.166667 Tz (methylene-H1\), ) Tj 4.880556 0 Td 51.041667 Tz (7.06 ) Tj 1.536111 0 Td 43.209877 Tz (\(d. ) Tj 1.069444 0 Td 53.796296 Tz (J=6.4 ) Tj 1.944444 0 Td 55.092593 Tz (Hz, ) Tj 51.428571 0 0 51.428571 0 1451.558322 Tm 25.2 0 Td 59.41358 Tz (2H, ) Tj 1.302778 0 Td 50 Tz (iq-H6\), ) Tj 2.352778 0 Td 47.800926 Tz (7.11 ) Tj 1.438889 0 Td 42.12963 Tz (\(d. ) Tj 1.011111 0 Td 53.796296 Tz (J=8.0 ) Tj 1.886111 0 Td 54.012346 Tz (Hz, ) Tj 1.283333 0 Td 54.012346 Tz (1H, ) Tj 1.186111 0 Td 55.092593 Tz (bpy-H9\), ) Tj 2.897222 0 Td 52.662037 Tz (7.42 ) Tj 1.516667 0 Td 38.888889 Tz (\(d. ) Tj 0.972222 0 Td 53.148148 Tz (J6.4 ) Tj 51.428571 0 0 51.428571 0 1409.715026 Tm 25.2 0 Td 57.253086 Tz (Hz, ) Tj 1.263889 0 Td 57.253086 Tz (2H, ) Tj 1.302778 0 Td 49.537037 Tz (iq-H7\), ) Tj 2.313889 0 Td 52.662037 Tz (7.55 ) Tj 1.497222 0 Td 34.567901 Tz (\(t, ) Tj 0.836111 0 Td 53.148148 Tz (J=8.0 ) Tj 1.847222 0 Td 56.17284 Tz (Hz, ) Tj 1.283333 0 Td 55.092593 Tz (1H, ) Tj 1.225 0 Td 55.812757 Tz (bpy-H10\), ) Tj 3.266667 0 Td 52.662037 Tz (7.77 ) Tj 1.497222 0 Td 46.180556 Tz (\(dd, ) Tj 51.428571 0 0 51.428571 0 1367.211781 Tm 25.2 0 Td 49.151235 Tz (J=1.8, ) Tj 2.119444 0 Td 50.771605 Tz (4.0 ) Tj 1.302778 0 Td 51.851852 Tz (Hz, ) Tj 1.302778 0 Td 58.333333 Tz (2H, ) Tj 1.4 0 Td 50 Tz (iq-H5\), ) Tj 2.45 0 Td 52.662037 Tz (7.78 ) Tj 1.633333 0 Td 46.990741 Tz (\(dd, ) Tj 1.438889 0 Td 50.231481 Tz (J=1.4, ) Tj 2.138889 0 Td 50.771605 Tz (3.8 ) Tj 1.302778 0 Td 51.851852 Tz (Hz, ) Tj 1.302778 0 Td 58.333333 Tz (2H, ) Tj 51.428571 0 0 51.428571 0 1326.22108 Tm 25.2 0 Td 50.462963 Tz (iq-H2\), ) Tj 2.294444 0 Td 52.662037 Tz (7.86 ) Tj 1.477778 0 Td 32.407407 Tz (\(t, ) Tj 0.797222 0 Td 53.148148 Tz (J=6.2 ) Tj 1.827778 0 Td 54.012346 Tz (Hz, ) Tj 1.147222 0 Td 60.493827 Tz (2H, ) Tj 1.283333 0 Td 49.537037 Tz (iq-H3\), ) Tj 2.313889 0 Td 52.662037 Tz (7.87 ) Tj 1.438889 0 Td 34.567901 Tz (\(t, ) Tj 0.797222 0 Td 53.148148 Tz (J=5.5 ) Tj 1.847222 0 Td 54.012346 Tz (Hz, ) Tj 1.244444 0 Td 54.012346 Tz (1H, ) Tj 51.428571 0 0 51.428571 0 1285.204161 Tm 25.180556 0 Td 55.812757 Tz (bpy-H14\), ) Tj 3.247222 0 Td 54.282407 Tz (8.14 ) Tj 1.555556 0 Td 41.049383 Tz (\(d. ) Tj 1.011111 0 Td 52.5 Tz (J5.5 ) Tj 1.925 0 Td 51.851852 Tz (Hz, ) Tj 1.283333 0 Td 55.092593 Tz (1H, ) Tj 1.225 0 Td 55.092593 Tz (bpy-H11\), ) Tj 3.247222 0 Td 51.851852 Tz (8.15 ) Tj 1.516667 0 Td 34.567901 Tz (\(t, ) Tj 0.875 0 Td 51.851852 Tz (J=6.5 ) Tj 51.428571 0 0 51.428571 0 1243.772908 Tm 25.2 0 Td 57.253086 Tz (Hz, ) Tj 1.263889 0 Td 60.493827 Tz (2H, ) Tj 1.361111 0 Td 49.537037 Tz (iq-H4\), ) Tj 2.352778 0 Td 52.662037 Tz (8.19 ) Tj 1.536111 0 Td 34.567901 Tz (\(t, ) Tj 0.894444 0 Td 52.5 Tz (J=8.2 ) Tj 1.886111 0 Td 55.092593 Tz (Hz, ) Tj 1.341667 0 Td 52.932099 Tz (1H, ) Tj 1.225 0 Td 55.452675 Tz (bpy-H13\), ) Tj 3.266667 0 Td 54.282407 Tz (8.50 ) Tj 1.575 0 Td 41.049383 Tz (\(d. ) Tj 51.428571 0 0 51.428571 0 1202.183569 Tm 25.2 0 Td 52.5 Tz (J=8.2 ) Tj 1.886111 0 Td 52.932099 Tz (Hz, ) Tj 1.244444 0 Td 55.092593 Tz (1H, ) Tj 1.225 0 Td 55.812757 Tz (bpy-H12\), ) Tj 3.208333 0 Td 54.282407 Tz (9.56 ) Tj 1.516667 0 Td 41.049383 Tz (\(d. ) Tj 1.011111 0 Td 53.148148 Tz (J=5.5 ) Tj 1.866667 0 Td 54.012346 Tz (Hz, ) Tj 1.283333 0 Td 55.092593 Tz (1H, ) Tj 1.186111 0 Td 55.812757 Tz (bpy-H15\). ) Tj 51.428571 0 0 51.428571 0 1158 Tm 25.2 0 Td 61.111111 Tz (ESI-MS: ) Tj 2.975 0 Td 60.493827 Tz (m/z ) Tj 1.808333 0 Td 51.203704 Tz (604.1 ) Tj 2.022222 0 Td 49.151235 Tz (\(calcd ) Tj 2.158333 0 Td 57.523148 Tz (m/z" ) Tj 1.788889 0 Td 47.530864 Tz (for ) Tj 1.458333 0 Td 80.37037 Tz (M-Clt ) Tj 2.838889 0 Td 49.826389 Tz (604.08\). ) Tj 51.428571 0 0 51.428571 0 1116 Tm 25.2 0 Td 52.5 Tz (Anal. ) Tj 1.827778 0 Td 57.037037 Tz (Calcd ) Tj 1.983333 0 Td 46.450617 Tz (for ) Tj 1.05 0 Td 95.601852 Tz (CHClNORu:C, ) Tj 7.136111 0 Td 50.231481 Tz (54.39; ) Tj 2.119444 0 Td 53.472222 Tz (H, ) Tj 0.933333 0 Td 47.962963 Tz (4.42; ) Tj 1.730556 0 Td 55.092593 Tz (N. ) Tj 51.428571 0 0 51.428571 0 1076.866667 Tm 25.258333 0 Td 48.611111 Tz (10.23. ) Tj 2.177778 0 Td 55.632716 Tz (Found: ) Tj 2.430556 0 Td 55.092593 Tz (C, ) Tj 1.069444 0 Td 50.231481 Tz (54.70; ) Tj 2.275 0 Td 51.851852 Tz (H, ) Tj 1.011111 0 Td 49.259259 Tz (4.34; ) Tj 1.925 0 Td 56.712963 Tz (N, ) Tj 1.147222 0 Td 48.070988 Tz (10.24. ) Tj 2.119444 0 Td 54.444444 Tz (Absorption ) Tj 51.428571 0 0 51.428571 0 1033 Tm 25.2 0 Td 65.354938 Tz (maxima ) Tj 2.586111 0 Td 57.118056 Tz (\(CH2Cl2\) ) Tj 3.013889 0 Td 82.638889 Tz (\(W\): ) Tj 2.236111 0 Td 60.493827 Tz (497 ) Tj 1.380556 0 Td 59.41358 Tz (nm, ) Tj 1.322222 0 Td 59.41358 Tz (362 ) Tj 1.361111 0 Td 58.333333 Tz (nm. ) Tj 51.428571 0 0 51.428571 0 961.033233 Tm 27.047222 0 Td 50.771605 Tz (Synthesis ) Tj 2.994444 0 Td 59.953704 Tz (of ) Tj 1.127778 0 Td 64.962121 Tz (Ru\(DIQ-Bpy\)\(Cl\)\(PF\).HO ) Tj 8.808333 0 Td 46.450617 Tz (\(7\) ) Tj 51.428571 0 0 51.428571 0 871.297477 Tm 25.919444 0 Td 87.5 Tz (A ) Tj 0.680556 0 Td 48.206019 Tz (solution ) Tj 2.508333 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 55.092593 Tz (6 ) Tj 0.525 0 Td 51.203704 Tz (\(0.30 ) Tj 1.691667 0 Td 45.37037 Tz (g, ) Tj 0.719444 0 Td 51.851852 Tz (0.13 ) Tj 1.497222 0 Td 63.518519 Tz (mmol\) ) Tj 2.080556 0 Td 45.37037 Tz (in ) Tj 0.758333 0 Td 55.092593 Tz (water ) Tj 1.788889 0 Td 55.092593 Tz (\(50 ) Tj 1.147222 0 Td 69.135802 Tz (mL\) ) Tj 1.419444 0 Td 61.574074 Tz (was ) Tj 40 0 0 40 0 837 Tm 32.425 0 Td 56.547619 Tz (stirred ) Tj 2.7 0 Td 61.111111 Tz (for ) Tj 1.475 0 Td 41.666667 Tz (1 ) Tj 0.675 0 Td 79.166667 Tz (h ) Tj 0.8 0 Td 75 Tz (and ) Tj 1.65 0 Td 63.888889 Tz (the ) Tj 1.475 0 Td 61.979167 Tz (solution ) Tj 3.325 0 Td 79.166667 Tz (was ) Tj 1.725 0 Td 70.833333 Tz (cooled ) Tj 2.875 0 Td 56.25 Tz (to ) Tj 1 0 Td 68.75 Tz (0 ) Tj 1.15 0 Td 70.833333 Tz (C. ) Tj 1.15 0 Td 67.361111 Tz (before ) Tj 52.857143 0 0 52.857143 0 787 Tm 24.518919 0 Td 48.47973 Tz (addition ) Tj 2.478378 0 Td 58.333333 Tz (of ) Tj 0.794595 0 Td 56.756757 Tz (a ) Tj 0.52973 0 Td 46.946947 Tz (saturated ) Tj 2.724324 0 Td 47.297297 Tz (solution ) Tj 2.478378 0 Td 55.18018 Tz (of ) Tj 0.737838 0 Td 88.288288 Tz (NHPF ) Tj 2.572973 0 Td 47.297297 Tz (in ) Tj 0.718919 0 Td 54.234234 Tz (water ) Tj 1.797297 0 Td 45.720721 Tz (\(5 ) Tj 0.775676 0 Td 56.756757 Tz (mL\). ) Tj 51.428571 0 0 51.428571 0 748.874845 Tm 25.2 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 47.170782 Tz (resulting ) Tj 2.741667 0 Td 46.843434 Tz (precipitate ) Tj 3.305556 0 Td 62.654321 Tz (was ) Tj 1.380556 0 Td 40.6893 Tz (filtered, ) Tj 2.430556 0 Td 61.033951 Tz (washed ) Tj 2.430556 0 Td 52.662037 Tz (with ) Tj 1.497222 0 Td 47.530864 Tz (ice ) Tj 1.069444 0 Td 52.662037 Tz (cold ) Tj 51.428571 0 0 51.428571 0 705.876574 Tm 25.180556 0 Td 49.691358 Tz (water, ) Tj 1.944444 0 Td 58.333333 Tz (and ) Tj 1.186111 0 Td 49.907407 Tz (dried ) Tj 1.672222 0 Td 43.75 Tz (to ) Tj 0.680556 0 Td 50.771605 Tz (get ) Tj 1.05 0 Td 51.851852 Tz (a ) Tj 0.505556 0 Td 49.691358 Tz (red ) Tj 1.05 0 Td 47.314815 Tz (solid ) Tj 1.555556 0 Td 49.907407 Tz (\(0.32 ) Tj 1.652778 0 Td 43.209877 Tz (g\). ) Tj 0.933333 0 Td 63.734568 Tz (The ) Tj 1.302778 0 Td 50.771605 Tz (red ) Tj 1.069444 0 Td 46.666667 Tz (solid ) Tj 1.575 0 Td 54.282407 Tz (\(100 ) Tj 51.428571 0 0 51.428571 0 663.615385 Tm 25.2 0 Td 65.895062 Tz (mg\) ) Tj 1.4 0 Td 59.41358 Tz (was ) Tj 1.322222 0 Td 50.771605 Tz (dissolved ) Tj 2.936111 0 Td 46.990741 Tz (in ) Tj 0.797222 0 Td 66.203704 Tz (minimum ) Tj 3.013889 0 Td 60.925926 Tz (amont ) Tj 2.022222 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 55.497685 Tz (methanol ) Tj 2.897222 0 Td 40.509259 Tz (\(1 ) Tj 0.816667 0 Td 57.523148 Tz (mL\), ) Tj 51.428571 0 0 51.428571 0 624.227384 Tm 25.219444 0 Td 50.771605 Tz (Sonicated ) Tj 2.936111 0 Td 46.990741 Tz (\(5 ) Tj 0.797222 0 Td 50.555556 Tz (min\), ) Tj 1.691667 0 Td 59.41358 Tz (and ) Tj 1.263889 0 Td 50.084175 Tz (centrifuged ) Tj 3.480556 0 Td 54.012346 Tz (\(15 ) Tj 1.205556 0 Td 49.259259 Tz (min\). ) Tj 1.672222 0 Td 63.734568 Tz (The ) Tj 1.302778 0 Td 47.138047 Tz (precipitate ) Tj 51.428571 0 0 51.428571 0 582.151088 Tm 25.2 0 Td 52.256944 Tz (obtained ) Tj 2.877778 0 Td 57.523148 Tz (from ) Tj 1.75 0 Td 48.611111 Tz (centrifugation ) Tj 4.472222 0 Td 60.493827 Tz (was ) Tj 1.458333 0 Td 60.493827 Tz (washed ) Tj 2.547222 0 Td 53.472222 Tz (with ) Tj 1.691667 0 Td 55.497685 Tz (methanol ) Tj 51.428571 0 0 51.428571 0 543.674534 Tm 25.2 0 Td 51.851852 Tz (again ) Tj 1.788889 0 Td 58.333333 Tz (and ) Tj 1.283333 0 Td 49.907407 Tz (dried ) Tj 1.711111 0 Td 45.37037 Tz (to ) Tj 0.777778 0 Td 48.611111 Tz (yield ) Tj 1.925 0 Td 64.197531 Tz (Ru\(DIQ-Bpy\)Cl\(PF\).H2O ) Tj 8.302778 0 Td 47.530864 Tz (\(7\) ) Tj 1.069444 0 Td 50.231481 Tz (as ) Tj 51.428571 0 0 51.428571 0 497.289406 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 55.092593 Tz (dark ) Tj 1.516667 0 Td 50.771605 Tz (red ) Tj 1.147222 0 Td 46.666667 Tz (solid ) Tj 1.633333 0 Td 51.851852 Tz (\(0.047 ) Tj 2.1 0 Td 30.246914 Tz (g., ) Tj 0.777778 0 Td 58.333333 Tz (42%\). ) Tj 2.022222 0 Td 60.185185 Tz (ESI-MS: ) Tj 2.780556 0 Td 59.41358 Tz (m/z ) Tj 1.322222 0 Td 51.203704 Tz (604.1 ) Tj 1.847222 0 Td 49.691358 Tz (\(calcd ) Tj 52.857143 0 0 52.857143 0 455 Tm 24.518919 0 Td 55.968468 Tz (m/z" ) Tj 2.232432 0 Td 47.297297 Tz (for ) Tj 1.910811 0 Td 107.207207 Tz (M ) Tj 1.494595 0 Td 84.084084 Tz (Cl" ) Tj 2.421622 0 Td 48.085586 Tz (604.09\). ) Tj 3.178378 0 Td 50.45045 Tz (Anal. ) Tj 2.402703 0 Td 55.495495 Tz (Calcd ) Tj 2.535135 0 Td 47.297297 Tz (for ) Tj 52.857143 0 0 52.857143 0 413 Tm 24.518919 0 Td 78.101178 Tz (C.H.CIFNOPRu: ) Tj 6.3 0 Td 55.18018 Tz (C, ) Tj 0.87027 0 Td 48.873874 Tz (48.54; ) Tj 2.024324 0 Td 53.603604 Tz (H, ) Tj 0.832432 0 Td 47.297297 Tz (3.38; ) Tj 1.645946 0 Td 53.603604 Tz (N, ) Tj 0.851351 0 Td 47.297297 Tz (9.13. ) Tj 1.645946 0 Td 54.129129 Tz (Found: ) Tj 2.175676 0 Td 52.027027 Tz (C, ) Tj 47.142857 0 0 47.142857 0 374 Tm 27.490909 0 Td 54.79798 Tz (48.70; ) Tj 2.269697 0 Td 63.636364 Tz (H, ) Tj 1.018182 0 Td 53.030303 Tz (3.38: ) Tj 1.887879 0 Td 61.868687 Tz (N, ) Tj 1.039394 0 Td 51.616162 Tz (9.28. ) Tj 51.428571 0 0 51.428571 0 299.985737 Tm 27.377778 0 Td 51.131687 Tz (Synthesis ) Tj 2.975 0 Td 59.953704 Tz (of ) Tj 1.088889 0 Td 63.117284 Tz (Ru\(DIQ-Bpy\)\(H2O\)\(PF\), ) Tj 8.225 0 Td 46.450617 Tz (\(5\) ) Tj 51.428571 0 0 51.428571 0 213.309973 Tm 25.919444 0 Td 63.734568 Tz (The ) Tj 1.536111 0 Td 55.902778 Tz (methanol ) Tj 3.072222 0 Td 48.611111 Tz (Solution ) Tj 2.722222 0 Td 57.523148 Tz (from ) Tj 1.788889 0 Td 48.37963 Tz (centrifugation ) Tj 4.452778 0 Td 52.932099 Tz (during ) Tj 2.275 0 Td 50.771605 Tz (the ) Tj 51.428571 0 0 51.428571 0 170.653266 Tm 25.219444 0 Td 48.971193 Tz (synthesis ) Tj 2.916667 0 Td 55.092593 Tz (of ) Tj 0.836111 0 Td 59.259259 Tz (complex ) Tj 2.741667 0 Td 58.333333 Tz (7 ) Tj 0.622222 0 Td 61.574074 Tz (was ) Tj 1.380556 0 Td 51.311728 Tz (concentrated ) Tj 3.927778 0 Td 59.41358 Tz (and ) Tj 1.322222 0 Td 59.953704 Tz (washed ) Tj 2.411111 0 Td 54.282407 Tz (with ) Tj ET Q endstream endobj 292 0 obj << /Length 1 >> stream q endstream endobj 293 0 obj << /Length 51759 >> stream Q q 0.24 0 0 0.24 0 0 cm BT /F1 1 Tf 3 Tr 62.857143 0 0 62.857143 0 3023 Tm 17.181818 0 Td 83.522727 Tz (US ) Tj 1.288636 0 Td 58.922559 Tz (9,566,576 ) Tj 3.468182 0 Td 74.242424 Tz (B2 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 14.113514 0 Td 75.675676 Tz (33 ) Tj 51.428571 0 0 51.428571 0 2916.053942 Tm 6.261111 0 Td 48.148148 Tz (diethyl ) Tj 2.45 0 Td 44.830247 Tz (ether, ) Tj 2.041667 0 Td 58.333333 Tz (and ) Tj 1.477778 0 Td 49.907407 Tz (dried ) Tj 1.925 0 Td 57.037037 Tz (under ) Tj 2.138889 0 Td 54.166667 Tz (reduced ) Tj 2.683333 0 Td 50.636574 Tz (pressure ) Tj 2.877778 0 Td 45.37037 Tz (to ) Tj 0.972222 0 Td 50.771605 Tz (get ) Tj 52.857143 0 0 52.857143 0 2874.2554 Tm 6.337838 0 Td 70.085995 Tz (Ru\(DIQ-Bpy\)\(HO\)\(PF\).HO ) Tj 9.572973 0 Td 46.246246 Tz (\(5\) ) Tj 1.154054 0 Td 49.924925 Tz (\(0.045 ) Tj 2.118919 0 Td 44.144144 Tz (g, ) Tj 0.832432 0 Td 64.63964 Tz (35%\) ) Tj 1.835135 0 Td 50.45045 Tz (as ) Tj 0.927027 0 Td 53.603604 Tz (a ) Tj 57.142857 0 0 57.142857 0 2827.278296 Tm 5.635 0 Td 46.666667 Tz (red ) Tj 1.05 0 Td 50 Tz (powder. ) Tj 2.3975 0 Td 53.958333 Tz ("H ) Tj 0.91 0 Td 83.611111 Tz (NMR ) Tj 1.715 0 Td 67.569444 Tz (\(CDCN, ) Tj 2.7125 0 Td 53.472222 Tz (500 ) Tj 1.19 0 Td 57.166667 Tz (MHz\): ) Tj 2.0125 0 Td 46.666667 Tz (8 ) Tj 0.525 0 Td 48.125 Tz (5.14 ) Tj 1.4 0 Td 32.083333 Tz (\(s. ) Tj 0.8575 0 Td 51.527778 Tz (2H, ) Tj 51.428571 0 0 51.428571 0 2785.941722 Tm 6.241667 0 Td 49.691358 Tz (bipyridyl ) Tj 3.091667 0 Td 54.166667 Tz (methylene-H8\), ) Tj 4.938889 0 Td 52.662037 Tz (5.45 ) Tj 1.672222 0 Td 42.12963 Tz (\(d. ) Tj 1.166667 0 Td 54.012346 Tz (J=16.2 ) Tj 2.352778 0 Td 56.17284 Tz (Hz, ) Tj 1.419444 0 Td 58.333333 Tz (2H, ) Tj 1.419444 0 Td 47.314815 Tz (axial ) Tj 51.428571 0 0 51.428571 0 2744.19802 Tm 6.261111 0 Td 50.231481 Tz (isoquinoline ) Tj 3.85 0 Td 53.935185 Tz (methylene-H1\), ) Tj 4.783333 0 Td 43.209877 Tz (6.1 ) Tj 1.108333 0 Td 41.049383 Tz (\(d. ) Tj 0.972222 0 Td 54.012346 Tz (J=16.2 ) Tj 2.197222 0 Td 55.092593 Tz (Hz, ) Tj 1.225 0 Td 58.333333 Tz (2H, ) Tj 1.263889 0 Td 57.253086 Tz (equito ) Tj 51.428571 0 0 51.428571 0 2699.404731 Tm 6.261111 0 Td 40.509259 Tz (rial ) Tj 1.341667 0 Td 49.96142 Tz (isoquinoline ) Tj 3.966667 0 Td 54.166667 Tz (methylene-H1\), ) Tj 4.938889 0 Td 52.662037 Tz (7.14 ) Tj 1.652778 0 Td 39.969136 Tz (\(d. ) Tj 1.127778 0 Td 54.444444 Tz (J=6.0 ) Tj 1.983333 0 Td 56.17284 Tz (Hz, ) Tj 1.380556 0 Td 58.333333 Tz (2H, ) Tj 51.428571 0 0 51.428571 0 2653.561265 Tm 6.261111 0 Td 50.462963 Tz (iq-H6\), ) Tj 2.372222 0 Td 48.611111 Tz (7.21 ) Tj 1.497222 0 Td 39.969136 Tz (\(d. ) Tj 0.972222 0 Td 53.796296 Tz (J7.8 ) Tj 1.886111 0 Td 54.012346 Tz (Hz, ) Tj 1.263889 0 Td 56.17284 Tz (1H, ) Tj 1.244444 0 Td 54.282407 Tz (bpy-H9\), ) Tj 2.858333 0 Td 51.851852 Tz (7.55 ) Tj 1.497222 0 Td 41.049383 Tz (\(d. ) Tj 1.011111 0 Td 53.796296 Tz (J=6.0 ) Tj 1.886111 0 Td 52.932099 Tz (Hz, ) Tj 51.428571 0 0 51.428571 0 2610.587361 Tm 6.261111 0 Td 59.41358 Tz (2H, ) Tj 1.244444 0 Td 49.537037 Tz (iq-H7\), ) Tj 2.275 0 Td 52.662037 Tz (7.76 ) Tj 1.419444 0 Td 33.487654 Tz (\(t, ) Tj 0.758333 0 Td 53.148148 Tz (J=7.8 ) Tj 1.769444 0 Td 56.17284 Tz (Hz, ) Tj 1.225 0 Td 56.17284 Tz (1H, ) Tj 1.147222 0 Td 55.452675 Tz (bpy-H10\), ) Tj 3.188889 0 Td 51.851852 Tz (7.87 ) Tj 1.438889 0 Td 50.771605 Tz (\(J=4.0 ) Tj 1.983333 0 Td 55.092593 Tz (Hz, ) Tj 51.428571 0 0 51.428571 0 2566.246719 Tm 6.261111 0 Td 59.41358 Tz (2H, ) Tj 1.341667 0 Td 49.537037 Tz (iq-H2\), ) Tj 2.333333 0 Td 52.662037 Tz (7.85 ) Tj 1.516667 0 Td 51.311728 Tz (\(J=4.0 ) Tj 2.119444 0 Td 55.092593 Tz (Hz, ) Tj 1.225 0 Td 59.41358 Tz (2H, ) Tj 1.322222 0 Td 49.537037 Tz (iq-H5\), ) Tj 2.352778 0 Td 50.231481 Tz (7.91 ) Tj 1.516667 0 Td 34.567901 Tz (\(t, ) Tj 0.836111 0 Td 54.444444 Tz (J7.8 ) Tj 1.925 0 Td 52.932099 Tz (Hz, ) Tj 51.428571 0 0 51.428571 0 2522.670064 Tm 6.319444 0 Td 55.092593 Tz (1H, ) Tj 1.205556 0 Td 55.452675 Tz (bpy-H14\), ) Tj 3.188889 0 Td 52.662037 Tz (7.94 ) Tj 1.477778 0 Td 32.407407 Tz (\(t, ) Tj 0.797222 0 Td 53.796296 Tz (J=2.8 ) Tj 1.827778 0 Td 55.092593 Tz (Hz, ) Tj 1.166667 0 Td 60.493827 Tz (2H, ) Tj 1.283333 0 Td 50 Tz (iq-H3\), ) Tj 2.294444 0 Td 50.231481 Tz (8.21 ) Tj 1.477778 0 Td 41.049383 Tz (\(d. ) Tj 0.972222 0 Td 56.388889 Tz (J=Hz, ) Tj 51.428571 0 0 51.428571 0 2479.653113 Tm 6.261111 0 Td 59.41358 Tz (2H, ) Tj 1.302778 0 Td 49.537037 Tz (iq-H4\), ) Tj 2.275 0 Td 54.282407 Tz (8.28 ) Tj 1.497222 0 Td 41.049383 Tz (\(d. ) Tj 0.972222 0 Td 54.444444 Tz (J7.8 ) Tj 1.866667 0 Td 54.012346 Tz (Hz, ) Tj 1.244444 0 Td 56.17284 Tz (1H, ) Tj 1.186111 0 Td 55.452675 Tz (bpy-H11\), ) Tj 3.208333 0 Td 53.472222 Tz (8.30 ) Tj 1.477778 0 Td 34.567901 Tz (\(t, ) Tj 0.816667 0 Td 53.148148 Tz (J7.8 ) Tj 51.428571 0 0 51.428571 0 2436.076923 Tm 6.261111 0 Td 57.253086 Tz (HZ, ) Tj 1.244444 0 Td 56.17284 Tz (1H, ) Tj 1.147222 0 Td 55.812757 Tz (bpy-H13\), ) Tj 3.169444 0 Td 52.662037 Tz (8.60 ) Tj 1.458333 0 Td 39.969136 Tz (\(d. ) Tj 0.894444 0 Td 54.444444 Tz (J8.0 ) Tj 1.827778 0 Td 54.012346 Tz (Hz, ) Tj 1.186111 0 Td 56.17284 Tz (1H, ) Tj 1.147222 0 Td 55.812757 Tz (bpy-H12\), ) Tj 3.169444 0 Td 52.662037 Tz (9.30 ) Tj 1.458333 0 Td 41.049383 Tz (\(d. ) Tj 52.857143 0 0 52.857143 0 2390.559748 Tm 6.091892 0 Td 52.342342 Tz (J=4.7 ) Tj 1.854054 0 Td 51.501502 Tz (Hz, ) Tj 1.267568 0 Td 53.603604 Tz (1H, ) Tj 1.210811 0 Td 54.304304 Tz (bpy-H15\). ) Tj 3.216216 0 Td 58.558559 Tz (ESI-MS: ) Tj 2.724324 0 Td 52.027027 Tz (m/z"713.6, ) Tj 3.405405 0 Td 47.297297 Tz (\(calcd ) Tj 1.948649 0 Td 56.756757 Tz (m/z" ) Tj 52.857143 0 0 52.857143 0 2345 Tm 6.091892 0 Td 47.297297 Tz (for ) Tj 2.156757 0 Td 92.623874 Tz (M-HO-PF" ) Tj 5.581081 0 Td 47.297297 Tz (713.6\). ) Tj 3.045946 0 Td 51.081081 Tz (Anal. ) Tj 2.648649 0 Td 54.864865 Tz (Calcd ) Tj 2.743243 0 Td 47.297297 Tz (for ) Tj 51.428571 0 0 51.428571 0 2302 Tm 6.261111 0 Td 114.146091 Tz (CHFNOPRu: ) Tj 6.377778 0 Td 55.092593 Tz (C, ) Tj 0.894444 0 Td 50.771605 Tz (42.48; ) Tj 2.119444 0 Td 53.472222 Tz (H, ) Tj 0.836111 0 Td 49.259259 Tz (3.10: ) Tj 1.730556 0 Td 56.712963 Tz (N, ) Tj 0.913889 0 Td 47.314815 Tz (7.99. ) Tj 1.672222 0 Td 55.632716 Tz (Found: ) Tj 2.236111 0 Td 55.092593 Tz (C, ) Tj 51.428571 0 0 51.428571 0 2259.809264 Tm 6.261111 0 Td 50.231481 Tz (42.32; ) Tj 2.294444 0 Td 55.092593 Tz (H, ) Tj 1.088889 0 Td 47.962963 Tz (3.29; ) Tj 1.925 0 Td 56.712963 Tz (N, ) Tj 1.108333 0 Td 47.314815 Tz (8.04. ) Tj 1.866667 0 Td 53.796296 Tz (Absorption ) Tj 3.694444 0 Td 64.274691 Tz (maxima ) Tj 2.761111 0 Td 75.617284 Tz (\(CHCI\) ) Tj 52.857143 0 0 52.857143 0 2214 Tm 6.110811 0 Td 106.156156 Tz (\(\): ) Tj 2.194595 0 Td 58.858859 Tz (457 ) Tj 1.305405 0 Td 57.807808 Tz (nm, ) Tj 1.305405 0 Td 59.90991 Tz (334 ) Tj 1.324324 0 Td 56.756757 Tz (nm. ) Tj 40 0 0 40 0 2179 Tm 8.05 0 Td 64.322917 Tz (Characterization ) Tj 6.525 0 Td 76.785714 Tz (Methods ) Tj 51.428571 0 0 51.428571 0 2129.938547 Tm 7 0 Td 57.253086 Tz (UV-vis ) Tj 2.488889 0 Td 51.527778 Tz (absorption ) Tj 3.577778 0 Td 48.148148 Tz (spectra ) Tj 2.508333 0 Td 58.333333 Tz (were ) Tj 1.886111 0 Td 57.523148 Tz (measured ) Tj 3.208333 0 Td 43.75 Tz (in ) Tj 0.991667 0 Td 57.253086 Tz (dichlo ) Tj 51.428571 0 0 51.428571 0 2086.659873 Tm 6.261111 0 Td 57.253086 Tz (romethane ) Tj 3.383333 0 Td 45.37037 Tz (at ) Tj 0.894444 0 Td 61.574074 Tz (room ) Tj 1.808333 0 Td 53.030303 Tz (temperature ) Tj 3.791667 0 Td 52.5 Tz (using ) Tj 1.905556 0 Td 55.092593 Tz (a ) Tj 0.661111 0 Td 65.219907 Tz (HP-8452A ) Tj 3.422222 0 Td 53.796296 Tz (diode ) Tj 58.571429 0 0 58.571429 0 2045.243574 Tm 5.497561 0 Td 43.252033 Tz (array ) Tj 1.536585 0 Td 44.215134 Tz (spectrometer. ) Tj 3.721951 0 Td 55.487805 Tz ("H ) Tj 0.921951 0 Td 82.520325 Tz (NMR ) Tj 1.690244 0 Td 46.95122 Tz (spectroscopy ) Tj 3.585366 0 Td 56.910569 Tz (was ) Tj 1.263415 0 Td 49.006323 Tz (conducted ) Tj 51.428571 0 0 51.428571 0 1999.125828 Tm 6.261111 0 Td 61.574074 Tz (on ) Tj 1.069444 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 52.932099 Tz (Varian ) Tj 2.275 0 Td 49.691358 Tz (Direct ) Tj 2.138889 0 Td 54.444444 Tz (Drive ) Tj 1.983333 0 Td 58.333333 Tz (500 ) Tj 1.4 0 Td 83.179012 Tz (MHz ) Tj 1.847222 0 Td 49.358974 Tz (spectrometer. ) Tj 4.219444 0 Td 52.391975 Tz (Cyclic ) Tj 51.428571 0 0 51.428571 0 1955.00995 Tm 6.261111 0 Td 53.472222 Tz (voltammetric ) Tj 4.122222 0 Td 56.983025 Tz (measurements ) Tj 4.336111 0 Td 58.333333 Tz (were ) Tj 1.575 0 Td 56.532922 Tz (performed ) Tj 3.266667 0 Td 43.75 Tz (in ) Tj 0.836111 0 Td 47.530864 Tz (1.0 ) Tj 1.030556 0 Td 106.944444 Tz (M ) Tj 0.855556 0 Td 72.916667 Tz (pH ) Tj 1.108333 0 Td 55.092593 Tz (7 ) Tj 51.428571 0 0 51.428571 0 1914.497326 Tm 6.261111 0 Td 54.73251 Tz (phosphate ) Tj 3.247222 0 Td 48.611111 Tz (buffer ) Tj 2.022222 0 Td 58.333333 Tz (and ) Tj 1.341667 0 Td 46.450617 Tz (0.1 ) Tj 1.205556 0 Td 103.703704 Tz (M ) Tj 0.952778 0 Td 87.5 Tz (HNO ) Tj 2.119444 0 Td 53.148148 Tz (using ) Tj 1.847222 0 Td 55.092593 Tz (a ) Tj 0.641667 0 Td 50.231481 Tz (glassy ) Tj 2.080556 0 Td 56.17284 Tz (carbon ) Tj 51.428571 0 0 51.428571 0 1872.576923 Tm 6.261111 0 Td 47.314815 Tz (electrode, ) Tj 3.013889 0 Td 55.092593 Tz (a ) Tj 0.505556 0 Td 53.472222 Tz (platinum ) Tj 2.761111 0 Td 54.282407 Tz (wire ) Tj 1.458333 0 Td 52.777778 Tz (counter ) Tj 2.352778 0 Td 47.638889 Tz (electrode, ) Tj 3.013889 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 58.333333 Tz (a ) Tj 0.486111 0 Td 62.962963 Tz (Ag/AgCl ) Tj 51.428571 0 0 51.428571 0 1829.18 Tm 6.261111 0 Td 50.411523 Tz (reference ) Tj 3.052778 0 Td 47.638889 Tz (electrode. ) Tj 3.247222 0 Td 63.734568 Tz (Oxygen ) Tj 2.663889 0 Td 50.771605 Tz (evolution ) Tj 3.15 0 Td 47.800926 Tz (reaction ) Tj 2.702778 0 Td 62.962963 Tz (measure ) Tj 52.857143 0 0 52.857143 0 1788.333333 Tm 6.091892 0 Td 56.756757 Tz (ments ) Tj 1.872973 0 Td 58.333333 Tz (were ) Tj 1.57027 0 Td 54.654655 Tz (performed ) Tj 3.178378 0 Td 51.711712 Tz (using ) Tj 1.702703 0 Td 53.603604 Tz (a ) Tj 0.52973 0 Td 46.666667 Tz (calibrated ) Tj 2.989189 0 Td 61.486486 Tz (O, ) Tj 0.983784 0 Td 48.348348 Tz (electrode ) Tj 2.8 0 Td 56.756757 Tz (\(YSI ) Tj 51.428571 0 0 51.428571 0 1746.684211 Tm 6.280556 0 Td 56.018519 Tz (5300A\). ) Tj 2.8 0 Td 53.652263 Tz (Elemental ) Tj 3.266667 0 Td 51.446759 Tz (analyses ) Tj 2.858333 0 Td 58.333333 Tz (were ) Tj 1.769444 0 Td 55.452675 Tz (conducted ) Tj 3.344444 0 Td 59.953704 Tz (by ) Tj 1.088889 0 Td 48.206019 Tz (Atlantic ) Tj 51.428571 0 0 51.428571 0 1705.638961 Tm 6.261111 0 Td 52.572016 Tz (Microlab, ) Tj 3.227778 0 Td 41.481481 Tz (Inc., ) Tj 1.575 0 Td 47.800926 Tz (Atlanta, ) Tj 2.644444 0 Td 56.17284 Tz (Ga. ) Tj 1.380556 0 Td 63.194444 Tz (Mass ) Tj 1.866667 0 Td 52.662037 Tz (spectrometry ) Tj 4.141667 0 Td 62.654321 Tz (was ) Tj 1.477778 0 Td 63.734568 Tz (per ) Tj 51.428571 0 0 51.428571 0 1667.545126 Tm 6.261111 0 Td 58.333333 Tz (formed ) Tj 2.313889 0 Td 53.148148 Tz (using ) Tj 1.808333 0 Td 79.938272 Tz (LCQ ) Tj 1.613889 0 Td 58.693416 Tz (Advantage ) Tj 3.383333 0 Td 46.990741 Tz (liquid ) Tj 1.925 0 Td 56.481481 Tz (chromatography ) Tj 4.997222 0 Td 59.143519 Tz (mass ) Tj 47.142857 0 0 47.142857 0 1626 Tm 6.851515 0 Td 53.846154 Tz (spectrometer. ) Tj 51.428571 0 0 51.428571 0 1580.904459 Tm 7 0 Td 62.654321 Tz (The ) Tj 1.283333 0 Td 57.118056 Tz (examples ) Tj 2.916667 0 Td 48.611111 Tz (as ) Tj 0.758333 0 Td 58.333333 Tz (above ) Tj 1.905556 0 Td 51.851852 Tz (presented ) Tj 2.936111 0 Td 50.771605 Tz (are ) Tj 1.088889 0 Td 51.851852 Tz (not ) Tj 1.069444 0 Td 52.256944 Tz (intended ) Tj 2.683333 0 Td 45.37037 Tz (to ) Tj 0.738889 0 Td 45.37037 Tz (limit ) Tj 51.428571 0 0 51.428571 0 1537.862872 Tm 6.241667 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 55.092593 Tz (scope ) Tj 1.886111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 59.143519 Tz (what ) Tj 1.652778 0 Td 49.691358 Tz (the ) Tj 1.127778 0 Td 50.05144 Tz (inventors ) Tj 2.955556 0 Td 51.311728 Tz (regard ) Tj 2.080556 0 Td 50.231481 Tz (as ) Tj 0.836111 0 Td 46.018519 Tz (their ) Tj 1.594444 0 Td 48.611111 Tz (invention. ) Tj 48.571429 0 0 48.571429 0 1496 Tm 7.432353 0 Td 49.754902 Tz (Further, ) Tj 2.676471 0 Td 43.464052 Tz (all ) Tj 1.111765 0 Td 52.614379 Tz (the ) Tj 1.235294 0 Td 61.764706 Tz (documents ) Tj 3.705882 0 Td 59.477124 Tz (mentioned ) Tj 3.5 0 Td 49.754902 Tz (in ) Tj 0.926471 0 Td 45.465686 Tz (this ) Tj 1.420588 0 Td 52.156863 Tz (disclosure ) Tj 51.428571 0 0 51.428571 0 1456.839557 Tm 6.261111 0 Td 49.691358 Tz (are ) Tj 1.147222 0 Td 51.041667 Tz (incorporated ) Tj 3.888889 0 Td 50.771605 Tz (herein ) Tj 2.061111 0 Td 59.953704 Tz (by ) Tj 1.030556 0 Td 49.331276 Tz (reference ) Tj 2.897222 0 Td 46.990741 Tz (in ) Tj 0.816667 0 Td 45.37037 Tz (their ) Tj 1.555556 0 Td 43.569959 Tz (entirety. ) Tj 38.571429 0 0 38.571429 0 1382 Tm 16.955556 0 Td 101.111111 Tz (REFERENCES ) Tj 51.428571 0 0 51.428571 0 1291 Tm 6.533333 0 Td 45.37037 Tz (1 ) Tj 0.855556 0 Td 50.231481 Tz (a\) ) Tj 0.894444 0 Td 56.712963 Tz (N. ) Tj 1.011111 0 Td 46.990741 Tz (S. ) Tj 0.913889 0 Td 54.012346 Tz (Lewis, ) Tj 2.294444 0 Td 53.472222 Tz (D. ) Tj 0.972222 0 Td 55.092593 Tz (G. ) Tj 1.011111 0 Td 54.166667 Tz (Nocera, ) Tj 2.644444 0 Td 47.962963 Tz (Proc. ) Tj 1.847222 0 Td 45.37037 Tz (Natl. ) Tj 1.672222 0 Td 54.444444 Tz (Acad. ) Tj 2.002778 0 Td 42.12963 Tz (Sci. ) Tj 51.428571 0 0 51.428571 0 1249 Tm 7.058333 0 Td 49.151235 Tz (U.S.A. ) Tj 2.041667 0 Td 53.796296 Tz (2006, ) Tj 1.886111 0 Td 50.231481 Tz (103, ) Tj 1.516667 0 Td 55.632716 Tz (15729-15735; ) Tj 4.238889 0 Td 51.851852 Tz (b\) ) Tj 0.836111 0 Td 50.231481 Tz (V. ) Tj 0.836111 0 Td 49.826389 Tz (Balzani, ) Tj 2.605556 0 Td 56.712963 Tz (A. ) Tj 0.913889 0 Td 49.151235 Tz (Credi, ) Tj 51.428571 0 0 51.428571 0 1208 Tm 7 0 Td 68.055556 Tz (M. ) Tj 0.991667 0 Td 48.206019 Tz (Venturi, ) Tj 2.566667 0 Td 68.055556 Tz (Chem ) Tj 1.847222 0 Td 56.17284 Tz (Sus ) Tj 1.225 0 Td 69.675926 Tz (Chem ) Tj 1.866667 0 Td 54.444444 Tz (2008, ) Tj 1.925 0 Td 37.268519 Tz (1, ) Tj 0.641667 0 Td 52.932099 Tz (26-58; ) Tj 2.1 0 Td 48.611111 Tz (c\) ) Tj 0.777778 0 Td 37.268519 Tz (J. ) Tj 0.7 0 Td 49.074074 Tz (Barber, ) Tj 51.428571 0 0 51.428571 0 1166 Tm 7 0 Td 55.497685 Tz (Biochem. ) Tj 2.936111 0 Td 50.231481 Tz (Soc. ) Tj 1.516667 0 Td 48.070988 Tz (Trans. ) Tj 2.002778 0 Td 55.092593 Tz (2006, ) Tj 1.866667 0 Td 50.771605 Tz (34, ) Tj 1.166667 0 Td 54.282407 Tz (619-631; ) Tj 2.877778 0 Td 48.611111 Tz (d\) ) Tj 0.816667 0 Td 58.333333 Tz (O. ) Tj 0.952778 0 Td 51.851852 Tz (Kruse, ) Tj 2.1 0 Td 38.888889 Tz (J. ) Tj 51.428571 0 0 51.428571 0 1128.093897 Tm 7.019444 0 Td 52.824074 Tz (Rupprecht, ) Tj 3.752778 0 Td 37.268519 Tz (J. ) Tj 1.088889 0 Td 51.851852 Tz (H. ) Tj 1.244444 0 Td 59.053498 Tz (Mussgnug, ) Tj 3.752778 0 Td 58.333333 Tz (G. ) Tj 1.302778 0 Td 53.472222 Tz (C. ) Tj 1.263889 0 Td 56.532922 Tz (Dismukes, ) Tj 3.675 0 Td 50.231481 Tz (B. ) Tj 48.571429 0 0 48.571429 0 1085 Tm 7.432353 0 Td 61.764706 Tz (Hankamer, ) Tj 3.582353 0 Td 59.705882 Tz (Photochem. ) Tj 3.870588 0 Td 52.5 Tz (Photobiol. ) Tj 3.397059 0 Td 45.465686 Tz (Sci. ) Tj 1.338235 0 Td 57.647059 Tz (2005, ) Tj 1.935294 0 Td 59.019608 Tz (4,957-970. ) Tj 51.428571 0 0 51.428571 0 1041.920162 Tm 6.494444 0 Td 78.858025 Tz (2a\) ) Tj 1.672222 0 Td 35.648148 Tz (P. ) Tj 0.719444 0 Td 46.990741 Tz (V. ) Tj 0.875 0 Td 50.555556 Tz (Bernhardt, ) Tj 3.305556 0 Td 46.990741 Tz (L. ) Tj 0.797222 0 Td 56.712963 Tz (A. ) Tj 0.933333 0 Td 49.691358 Tz (Jones, ) Tj 2.080556 0 Td 45.910494 Tz (Inorg. ) Tj 2.002778 0 Td 58.981481 Tz (Chem. ) Tj 2.119444 0 Td 52.5 Tz (1999, ) Tj 1.808333 0 Td 49.691358 Tz (38, ) Tj 51.428571 0 0 51.428571 0 1002.085517 Tm 7.019444 0 Td 55.092593 Tz (5086-5090; ) Tj 3.558333 0 Td 51.851852 Tz (b\) ) Tj 0.836111 0 Td 59.953704 Tz (X. ) Tj 1.030556 0 Td 56.17284 Tz (Hu, ) Tj 1.283333 0 Td 53.472222 Tz (B. ) Tj 0.894444 0 Td 48.611111 Tz (S. ) Tj 0.855556 0 Td 55.681818 Tz (Brunschwig, ) Tj 3.888889 0 Td 40.509259 Tz (J. ) Tj 0.738889 0 Td 55.092593 Tz (C. ) Tj 0.933333 0 Td 45.37037 Tz (Peters, ) Tj 2.138889 0 Td 40.509259 Tz (J. ) Tj 51.428571 0 0 51.428571 0 958 Tm 6.961111 0 Td 62.654321 Tz (Am. ) Tj 1.438889 0 Td 60.277778 Tz (Chem. ) Tj 2.1 0 Td 48.611111 Tz (Soc. ) Tj 1.477778 0 Td 54.444444 Tz (2007, ) Tj 1.944444 0 Td 50.231481 Tz (129, ) Tj 1.458333 0 Td 55.740741 Tz (8988-8998; ) Tj 3.597222 0 Td 46.990741 Tz (c\) ) Tj 0.777778 0 Td 55.092593 Tz (C. ) Tj 0.972222 0 Td 44.155093 Tz (Baffert, ) Tj 2.391667 0 Td 48.611111 Tz (V. ) Tj 51.428571 0 0 51.428571 0 917.878672 Tm 7 0 Td 49.074074 Tz (Artero, ) Tj 2.255556 0 Td 66.435185 Tz (M. ) Tj 0.972222 0 Td 52.5 Tz (Fontecave, ) Tj 3.363889 0 Td 46.450617 Tz (Inorg. ) Tj 1.925 0 Td 58.981481 Tz (Chem. ) Tj 1.983333 0 Td 54.444444 Tz (2007, ) Tj 1.808333 0 Td 49.691358 Tz (46, ) Tj 1.147222 0 Td 54.12037 Tz (1817-1824: ) Tj 51.428571 0 0 51.428571 0 876.972145 Tm 7 0 Td 50.231481 Tz (d\) ) Tj 0.777778 0 Td 37.268519 Tz (J. ) Tj 0.719444 0 Td 35.648148 Tz (P. ) Tj 0.7 0 Td 45.37037 Tz (Bigi. ) Tj 1.555556 0 Td 46.990741 Tz (T. ) Tj 0.855556 0 Td 46.990741 Tz (E. ) Tj 0.797222 0 Td 56.712963 Tz (Hanna, ) Tj 2.236111 0 Td 63.194444 Tz (W. ) Tj 1.011111 0 Td 55.092593 Tz (H. ) Tj 0.913889 0 Td 59.259259 Tz (Harman, ) Tj 2.663889 0 Td 55.092593 Tz (A. ) Tj 0.875 0 Td 57.79321 Tz (Chang, ) Tj 2.294444 0 Td 54.282407 Tz (C.J. ) Tj 51.428571 0 0 51.428571 0 834.132176 Tm 7 0 Td 57.253086 Tz (Chang, ) Tj 2.294444 0 Td 59.62963 Tz (Chem. ) Tj 2.080556 0 Td 65.277778 Tz (Commun. ) Tj 3.013889 0 Td 53.796296 Tz (2010, ) Tj 1.847222 0 Td 49.691358 Tz (46, ) Tj 1.108333 0 Td 54.282407 Tz (958-960; ) Tj 2.838889 0 Td 46.990741 Tz (e\) ) Tj 0.738889 0 Td 46.990741 Tz (Y. ) Tj 0.836111 0 Td 53.472222 Tz (Sun, ) Tj 1.497222 0 Td 37.268519 Tz (J. ) Tj 51.428571 0 0 51.428571 0 796.029112 Tm 7.019444 0 Td 37.268519 Tz (P. ) Tj 0.738889 0 Td 45.37037 Tz (Bigi. ) Tj 1.633333 0 Td 55.092593 Tz (N. ) Tj 0.875 0 Td 56.712963 Tz (A. ) Tj 0.952778 0 Td 45.37037 Tz (Piro, ) Tj 1.594444 0 Td 66.435185 Tz (M. ) Tj 1.069444 0 Td 48.611111 Tz (L. ) Tj 0.797222 0 Td 54.444444 Tz (Tang, ) Tj 1.866667 0 Td 37.268519 Tz (J. ) Tj 0.719444 0 Td 50.231481 Tz (R. ) Tj 0.894444 0 Td 55.740741 Tz (Long, ) Tj 1.905556 0 Td 51.851852 Tz (C. ) Tj 0.894444 0 Td 35.648148 Tz (J. ) Tj 0.680556 0 Td 57.253086 Tz (Chang, ) Tj 51.428571 0 0 51.428571 0 751.287356 Tm 6.961111 0 Td 40.509259 Tz (J. ) Tj 0.661111 0 Td 61.574074 Tz (Am. ) Tj 1.361111 0 Td 58.981481 Tz (Chem. ) Tj 1.983333 0 Td 48.611111 Tz (Soc. ) Tj 1.380556 0 Td 53.796296 Tz (2011, ) Tj 1.827778 0 Td 56.018519 Tz (133,9212-9215; ) Tj 4.861111 0 Td 42.12963 Tz (f\) ) Tj 0.661111 0 Td 59.143519 Tz (P-A. ) Tj 1.555556 0 Td 51.041667 Tz (Jacques, ) Tj 50 0 0 50 0 711 Tm 7.2 0 Td 50 Tz (V. ) Tj 0.78 0 Td 50.952381 Tz (Artero, ) Tj 2.32 0 Td 40 Tz (J. ) Tj 0.74 0 Td 50.952381 Tz (Pcaut, ) Tj 2.34 0 Td 68.333333 Tz (M. ) Tj 1.12 0 Td 53.333333 Tz (Fontecave, ) Tj 3.44 0 Td 50 Tz (Proc. ) Tj 1.8 0 Td 46 Tz (Natl. ) Tj 1.62 0 Td 56 Tz (Acad. ) Tj 1.92 0 Td 44.166667 Tz (Sci. ) Tj 51.428571 0 0 51.428571 0 671.26738 Tm 7.058333 0 Td 49.151235 Tz (U.S.A. ) Tj 2.041667 0 Td 53.796296 Tz (2009, ) Tj 1.944444 0 Td 49.421296 Tz (106, ) Tj 1.419444 0 Td 58.333333 Tz (20627-20632;g\) ) Tj 5.133333 0 Td 37.268519 Tz (J. ) Tj 0.719444 0 Td 46.990741 Tz (L. ) Tj 0.836111 0 Td 59.548611 Tz (Dempsey, ) Tj 3.130556 0 Td 51.851852 Tz (B. ) Tj 0.836111 0 Td 48.611111 Tz (S. ) Tj 51.428571 0 0 51.428571 0 628.953168 Tm 7.019444 0 Td 55.387205 Tz (Brunschwig, ) Tj 3.869444 0 Td 40.509259 Tz (J. ) Tj 0.777778 0 Td 48.611111 Tz (R. ) Tj 0.836111 0 Td 51.446759 Tz (Winkler, ) Tj 2.761111 0 Td 53.472222 Tz (H. ) Tj 0.972222 0 Td 48.611111 Tz (B. ) Tj 0.836111 0 Td 51.851852 Tz (Gray, ) Tj 1.788889 0 Td 51.041667 Tz (Acc. ) Tj 1.536111 0 Td 60.277778 Tz (Chem. ) Tj 2.158333 0 Td 46.180556 Tz (Res. ) Tj 51.428571 0 0 51.428571 0 584 Tm 7 0 Td 53.796296 Tz (2009, ) Tj 1.847222 0 Td 49.691358 Tz (42, ) Tj 1.225 0 Td 54.444444 Tz (1995-2004; ) Tj 3.519444 0 Td 51.851852 Tz (h\) ) Tj 0.836111 0 Td 64.814815 Tz (W. ) Tj 1.05 0 Td 53.472222 Tz (R. ) Tj 0.894444 0 Td 63.014403 Tz (McNamara, ) Tj 3.655556 0 Td 51.851852 Tz (Z. ) Tj 0.913889 0 Td 55.902778 Tz (Han, ) Tj 1.594444 0 Td 38.888889 Tz (P. ) Tj 0.719444 0 Td 37.268519 Tz (J. ) Tj 51.428571 0 0 51.428571 0 544.915789 Tm 7 0 Td 49.826389 Tz (Alperin, ) Tj 2.566667 0 Td 63.194444 Tz (W. ) Tj 0.952778 0 Td 63.194444 Tz (W. ) Tj 0.991667 0 Td 50.084175 Tz (Brennessel, ) Tj 3.5 0 Td 38.888889 Tz (P. ) Tj 0.7 0 Td 46.990741 Tz (L. ) Tj 0.797222 0 Td 51.446759 Tz (Holland, ) Tj 2.702778 0 Td 48.611111 Tz (R. ) Tj 0.836111 0 Td 49.907407 Tz (Eisenberg, ) Tj 3.130556 0 Td 40.509259 Tz (J. ) Tj 51.428571 0 0 51.428571 0 501 Tm 6.961111 0 Td 62.654321 Tz (Am. ) Tj 1.4 0 Td 58.981481 Tz (Chem. ) Tj 2.022222 0 Td 48.611111 Tz (Soc. ) Tj 1.4 0 Td 53.796296 Tz (2011, ) Tj 1.866667 0 Td 48.611111 Tz (133, ) Tj 1.438889 0 Td 55.632716 Tz (15368-15371; ) Tj 4.2 0 Td 35.648148 Tz (i\) ) Tj 0.622222 0 Td 48.611111 Tz (V. ) Tj 0.738889 0 Td 49.074074 Tz (Artero, ) Tj 2.255556 0 Td 66.435185 Tz (M. ) Tj 51.428571 0 0 51.428571 0 460.073418 Tm 7 0 Td 52.391975 Tz (Chavarot-Kerlidou, ) Tj 5.813889 0 Td 68.055556 Tz (M. ) Tj 1.030556 0 Td 51.851852 Tz (Fontecave, ) Tj 3.266667 0 Td 57.253086 Tz (Angew. ) Tj 2.313889 0 Td 54.552469 Tz (Chem., ) Tj 2.216667 0 Td 36.458333 Tz (Int. ) Tj 1.147222 0 Td 48.611111 Tz (Ed. ) Tj 51.428571 0 0 51.428571 0 422.037086 Tm 7 0 Td 52.5 Tz (2011, ) Tj 1.808333 0 Td 49.691358 Tz (50, ) Tj 1.088889 0 Td 55.632716 Tz (72387266;j\) ) Tj 4.238889 0 Td 50.231481 Tz (R. ) Tj 0.836111 0 Td 66.435185 Tz (M. ) Tj 1.030556 0 Td 44.155093 Tz (Kellett, ) Tj 2.294444 0 Td 50.231481 Tz (T. ) Tj 0.797222 0 Td 56.712963 Tz (G. ) Tj 0.913889 0 Td 48.070988 Tz (Spiro, ) Tj 1.983333 0 Td 46.450617 Tz (Inorg. ) Tj 51.428571 0 0 51.428571 0 376 Tm 7.019444 0 Td 59.62963 Tz (Chem. ) Tj 2.255556 0 Td 51.203704 Tz (1985, ) Tj 1.886111 0 Td 49.691358 Tz (24, ) Tj 1.244444 0 Td 55.740741 Tz (2373-2377; ) Tj 3.655556 0 Td 53.472222 Tz (k\) ) Tj 0.952778 0 Td 56.712963 Tz (G. ) Tj 1.030556 0 Td 68.055556 Tz (M. ) Tj 1.166667 0 Td 51.49177 Tz (Jacobsen, ) Tj 3.130556 0 Td 38.888889 Tz (J. ) Tj 0.758333 0 Td 50.231481 Tz (Y. ) Tj 51.428571 0 0 51.428571 0 337.713656 Tm 7 0 Td 55.740741 Tz (Yang, ) Tj 2.080556 0 Td 48.611111 Tz (B. ) Tj 0.952778 0 Td 58.738426 Tz (Twamley, ) Tj 3.15 0 Td 55.092593 Tz (A. ) Tj 1.05 0 Td 56.712963 Tz (D. ) Tj 1.05 0 Td 52.777778 Tz (Wilson, ) Tj 2.644444 0 Td 48.611111 Tz (R. ) Tj 0.972222 0 Td 66.435185 Tz (M. ) Tj 1.205556 0 Td 50.636574 Tz (Bullock, ) Tj 2.8 0 Td 66.435185 Tz (M. ) Tj 51.428571 0 0 51.428571 0 294.125683 Tm 7.019444 0 Td 59.953704 Tz (Rakowski ) Tj 3.208333 0 Td 56.018519 Tz (DuBois, ) Tj 2.702778 0 Td 55.092593 Tz (D. ) Tj 0.972222 0 Td 48.611111 Tz (L. ) Tj 0.933333 0 Td 56.018519 Tz (DuBois, ) Tj 2.722222 0 Td 55.632716 Tz (Energy ) Tj 2.372222 0 Td 49.421296 Tz (Environ. ) Tj 2.702778 0 Td 42.939815 Tz (Sci. ) Tj 51.428571 0 0 51.428571 0 252.035714 Tm 7 0 Td 53.796296 Tz (2008, ) Tj 2.002778 0 Td 38.888889 Tz (1, ) Tj 0.836111 0 Td 52.662037 Tz (167-174: ) Tj 2.936111 0 Td 45.37037 Tz (1\) ) Tj 0.836111 0 Td 50.231481 Tz (E. ) Tj 0.913889 0 Td 46.990741 Tz (S. ) Tj 0.913889 0 Td 53.472222 Tz (Wiedner, ) Tj 2.858333 0 Td 40.509259 Tz (J. ) Tj 0.758333 0 Td 50.231481 Tz (Y. ) Tj 0.875 0 Td 56.388889 Tz (Yang, ) Tj 2.022222 0 Td 61.574074 Tz (W. ) Tj 1.088889 0 Td 55.092593 Tz (G. ) Tj 51.428571 0 0 51.428571 0 211.815681 Tm 7.019444 0 Td 53.472222 Tz (Dougherty, ) Tj 3.441667 0 Td 64.814815 Tz (W. ) Tj 1.05 0 Td 45.37037 Tz (S. ) Tj 0.816667 0 Td 50 Tz (Kassel, ) Tj 2.391667 0 Td 48.611111 Tz (R. ) Tj 0.875 0 Td 64.814815 Tz (M. ) Tj 1.108333 0 Td 49.826389 Tz (Bullock, ) Tj 2.663889 0 Td 66.435185 Tz (M. ) Tj 1.108333 0 Td 48.611111 Tz (R. ) Tj 0.855556 0 Td 56.481481 Tz (DuBois, ) Tj 51.428571 0 0 51.428571 0 170.553411 Tm 7 0 Td 58.333333 Tz (D. ) Tj 0.913889 0 Td 50.231481 Tz (L. ) Tj 0.855556 0 Td 56.018519 Tz (DuBois, ) Tj 2.605556 0 Td 53.580247 Tz (Organometallics ) Tj 5.036111 0 Td 53.796296 Tz (2010, ) Tj 1.827778 0 Td 50.771605 Tz (29, ) Tj 1.147222 0 Td 55.092593 Tz (5390-5401; ) Tj 3.538889 0 Td 66.435185 Tz (m\) ) Tj 30 0 0 30 0 2755 Tm 41.666667 0 Td 72.222222 Tz (5 ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 30 0 0 30 0 1091 Tm 41.4 0 Td 80.555556 Tz (45 ) Tj 30 0 0 30 0 883 Tm 41.433333 0 Td 80.555556 Tz (50 ) Tj 30 0 0 30 0 675 Tm 41.433333 0 Td 77.777778 Tz (55 ) Tj 30 0 0 30 0 467 Tm 41.466667 0 Td 77.777778 Tz (60 ) Tj 30 0 0 30 0 259 Tm 41.466667 0 Td 75 Tz (65 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 77.252252 Tz (34 ) Tj 48.571429 0 0 48.571429 0 2915 Tm 27.444118 0 Td 56.617647 Tz (C. ) Tj 1.008824 0 Td 53.431373 Tz (Creutz, ) Tj 2.532353 0 Td 61.764706 Tz (N. ) Tj 1.05 0 Td 50.898693 Tz (Sutin, ) Tj 2.161765 0 Td 57.189542 Tz (Coord. ) Tj 2.408824 0 Td 64.509804 Tz (Chem. ) Tj 2.326471 0 Td 48.039216 Tz (Rev. ) Tj 1.605882 0 Td 54.901961 Tz (1985, ) Tj 1.997059 0 Td 51.470588 Tz (64, ) Tj 1.194118 0 Td 80.065359 Tz (321 ) Tj 51.428571 0 0 51.428571 0 2871.99449 Tm 25.919444 0 Td 52.662037 Tz (341, ) Tj 1.594444 0 Td 48.611111 Tz (n\) ) Tj 0.836111 0 Td 56.712963 Tz (N. ) Tj 0.952778 0 Td 46.990741 Tz (Sutin, ) Tj 1.944444 0 Td 55.092593 Tz (C. ) Tj 0.933333 0 Td 50.462963 Tz (Creutz, ) Tj 2.411111 0 Td 46.990741 Tz (E. ) Tj 0.875 0 Td 43.981481 Tz (Fujita, ) Tj 2.119444 0 Td 63.194444 Tz (Comments ) Tj 3.344444 0 Td 46.450617 Tz (Inorg. ) Tj 48.571429 0 0 48.571429 0 2828 Tm 27.464706 0 Td 63.823529 Tz (Chem. ) Tj 2.285294 0 Td 54.901961 Tz (1997, ) Tj 1.997059 0 Td 50.326797 Tz (19, ) Tj 1.173529 0 Td 54.330065 Tz (67-92. ) Tj 51.428571 0 0 51.428571 0 2784.529328 Tm 25.375 0 Td 68.055556 Tz (3 ) Tj 0.933333 0 Td 46.990741 Tz (a\) ) Tj 0.855556 0 Td 35.648148 Tz (J. ) Tj 0.777778 0 Td 37.268519 Tz (P. ) Tj 0.719444 0 Td 48.148148 Tz (Collin, ) Tj 2.255556 0 Td 56.712963 Tz (A. ) Tj 0.991667 0 Td 43.75 Tz (Jouaiti, ) Tj 2.391667 0 Td 35.648148 Tz (J. ) Tj 0.777778 0 Td 35.648148 Tz (P. ) Tj 0.738889 0 Td 54.6875 Tz (Sauvage, ) Tj 2.955556 0 Td 46.450617 Tz (Inorg. ) Tj 2.041667 0 Td 59.62963 Tz (Chem. ) Tj 51.428571 0 0 51.428571 0 2739 Tm 25.977778 0 Td 51.851852 Tz (1988, ) Tj 1.944444 0 Td 49.691358 Tz (27, ) Tj 1.341667 0 Td 54.444444 Tz (1986-1990; ) Tj 3.636111 0 Td 50.231481 Tz (b\) ) Tj 0.972222 0 Td 66.435185 Tz (M. ) Tj 1.225 0 Td 59.143519 Tz (Rakowski ) Tj 3.266667 0 Td 53.240741 Tz (Dubois, ) Tj 2.625 0 Td 55.092593 Tz (D. ) Tj 1.069444 0 Td 48.611111 Tz (L. ) Tj 51.428571 0 0 51.428571 0 2695 Tm 25.919444 0 Td 53.703704 Tz (Dubois, ) Tj 2.508333 0 Td 51.041667 Tz (Acc. ) Tj 1.555556 0 Td 60.277778 Tz (Chem. ) Tj 2.138889 0 Td 47.800926 Tz (Res. ) Tj 1.438889 0 Td 53.796296 Tz (2009, ) Tj 1.866667 0 Td 50.771605 Tz (42, ) Tj 1.244444 0 Td 54.444444 Tz (1974-1982; ) Tj 3.5 0 Td 48.611111 Tz (c\) ) Tj 0.777778 0 Td 58.333333 Tz (A. ) Tj 0.991667 0 Td 59.953704 Tz (Le ) Tj 48.571429 0 0 48.571429 0 2653 Tm 27.444118 0 Td 53.529412 Tz (Goff, ) Tj 1.852941 0 Td 53.186275 Tz (V. ) Tj 0.864706 0 Td 52.45098 Tz (Artero, ) Tj 2.470588 0 Td 56.617647 Tz (B. ) Tj 0.947059 0 Td 55.931373 Tz (Jousselme, ) Tj 3.644118 0 Td 41.176471 Tz (P. ) Tj 0.823529 0 Td 58.333333 Tz (D. ) Tj 0.926471 0 Td 54.215686 Tz (Tran, ) Tj 1.894118 0 Td 61.764706 Tz (N. ) Tj 0.988235 0 Td 48.897059 Tz (Guillet, ) Tj 2.655882 0 Td 53.186275 Tz (R. ) Tj 52.857143 0 0 52.857143 0 2609.238579 Tm 25.218919 0 Td 54.954955 Tz (Mtaye, ) Tj 2.440541 0 Td 55.18018 Tz (A. ) Tj 0.87027 0 Td 41.516517 Tz (Fihri, ) Tj 1.664865 0 Td 48.873874 Tz (S. ) Tj 0.756757 0 Td 46.903153 Tz (Palacin, ) Tj 2.421622 0 Td 66.216216 Tz (M. ) Tj 0.983784 0 Td 50.765766 Tz (Fontecave, ) Tj 3.216216 0 Td 52.252252 Tz (Science ) Tj 2.345946 0 Td 52.342342 Tz (2009, ) Tj 51.428571 0 0 51.428571 0 2565.346314 Tm 25.919444 0 Td 52.662037 Tz (326, ) Tj 1.575 0 Td 54.12037 Tz (1384-1387; ) Tj 3.5 0 Td 48.611111 Tz (d\) ) Tj 0.816667 0 Td 56.712963 Tz (U. ) Tj 0.913889 0 Td 37.268519 Tz (J. ) Tj 0.7 0 Td 49.016204 Tz (Kilgore, ) Tj 2.586111 0 Td 37.268519 Tz (J. ) Tj 0.661111 0 Td 56.712963 Tz (A. ) Tj 0.875 0 Td 50.231481 Tz (S. ) Tj 0.875 0 Td 49.421296 Tz (Roberts, ) Tj 2.625 0 Td 55.092593 Tz (D. ) Tj 0.952778 0 Td 53.472222 Tz (H. ) Tj 51.428571 0 0 51.428571 0 2521.110799 Tm 25.919444 0 Td 50.555556 Tz (Pool, ) Tj 1.730556 0 Td 58.333333 Tz (A. ) Tj 0.972222 0 Td 66.435185 Tz (M. ) Tj 1.011111 0 Td 53.472222 Tz (Appel, ) Tj 2.197222 0 Td 66.435185 Tz (M. ) Tj 1.069444 0 Td 40.509259 Tz (P. ) Tj 0.738889 0 Td 50.231481 Tz (Stewart, ) Tj 2.683333 0 Td 66.435185 Tz (M. ) Tj 1.088889 0 Td 51.851852 Tz (R. ) Tj 0.894444 0 Td 56.018519 Tz (DuBois, ) Tj 2.625 0 Td 64.814815 Tz (W. ) Tj 1.030556 0 Td 56.712963 Tz (G. ) Tj 51.428571 0 0 51.428571 0 2478.769437 Tm 25.938889 0 Td 53.472222 Tz (Dougherty, ) Tj 3.422222 0 Td 64.814815 Tz (W. ) Tj 0.952778 0 Td 46.990741 Tz (S. ) Tj 0.777778 0 Td 50 Tz (Kassel, ) Tj 2.333333 0 Td 48.611111 Tz (R. ) Tj 0.797222 0 Td 66.435185 Tz (M. ) Tj 1.069444 0 Td 50.231481 Tz (Bullock, ) Tj 2.625 0 Td 55.092593 Tz (D. ) Tj 0.894444 0 Td 46.990741 Tz (L. ) Tj 0.797222 0 Td 56.018519 Tz (DuBois, ) Tj 2.508333 0 Td 40.509259 Tz (J. ) Tj 51.428571 0 0 51.428571 0 2433 Tm 25.880556 0 Td 63.734568 Tz (Am. ) Tj 1.4 0 Td 58.981481 Tz (Chem. ) Tj 2.002778 0 Td 48.611111 Tz (Soc. ) Tj 1.380556 0 Td 53.796296 Tz (2011, ) Tj 1.827778 0 Td 50.231481 Tz (133, ) Tj 1.380556 0 Td 55.740741 Tz (5861-5872; ) Tj 3.5 0 Td 46.990741 Tz (e\) ) Tj 0.758333 0 Td 66.435185 Tz (M. ) Tj 0.972222 0 Td 48.611111 Tz (L. ) Tj 0.816667 0 Td 57.685185 Tz (Helm, ) Tj 1.905556 0 Td 68.055556 Tz (M. ) Tj 48.571429 0 0 48.571429 0 2391 Tm 27.444118 0 Td 42.892157 Tz (P. ) Tj 0.782353 0 Td 52.757353 Tz (Stewart, ) Tj 2.8 0 Td 56.617647 Tz (R. ) Tj 0.926471 0 Td 72.058824 Tz (M. ) Tj 1.132353 0 Td 54.044118 Tz (Bullock, ) Tj 2.841176 0 Td 72.058824 Tz (M. ) Tj 1.111765 0 Td 56.617647 Tz (R. ) Tj 0.947059 0 Td 59.803922 Tz (DuBois, ) Tj 2.779412 0 Td 58.333333 Tz (D. ) Tj 0.988235 0 Td 53.186275 Tz (L. ) Tj 0.885294 0 Td 59.803922 Tz (DuBois, ) Tj 47.142857 0 0 47.142857 0 2348 Tm 28.254545 0 Td 58.585859 Tz (Science ) Tj 2.715152 0 Td 58.686869 Tz (2011, ) Tj 2.015152 0 Td 57.449495 Tz (333, ) Tj 1.654545 0 Td 58.775253 Tz (863-866. ) Tj 51.428571 0 0 51.428571 0 2302 Tm 25.413889 0 Td 75.617284 Tz (4a\) ) Tj 1.497222 0 Td 56.712963 Tz (G. ) Tj 0.816667 0 Td 56.712963 Tz (A. ) Tj 0.855556 0 Td 55.092593 Tz (N. ) Tj 0.855556 0 Td 48.148148 Tz (Felton, ) Tj 2.158333 0 Td 55.092593 Tz (A. ) Tj 0.855556 0 Td 55.092593 Tz (K. ) Tj 0.816667 0 Td 53.292181 Tz (Vannucci, ) Tj 3.013889 0 Td 38.888889 Tz (J. ) Tj 0.602778 0 Td 57.037037 Tz (Chen, ) Tj 1.905556 0 Td 48.611111 Tz (L. ) Tj 0.738889 0 Td 45.37037 Tz 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55.632716 Tz (12521-12530; ) Tj 4.180556 0 Td 53.472222 Tz (b\) ) Tj 0.797222 0 Td 66.435185 Tz (M. ) Tj 0.952778 0 Td 53.472222 Tz (Y. ) Tj 0.855556 0 Td 53.742284 Tz (Darensbourg, ) Tj 4.102778 0 Td 46.990741 Tz (E. ) Tj 0.738889 0 Td 37.268519 Tz (J. ) Tj 0.680556 0 Td 53.796296 Tz (Lyon, ) Tj 1.827778 0 Td 58.333333 Tz (X. ) Tj 0.875 0 Td 55.092593 Tz (Zhao, ) Tj 51.428571 0 0 51.428571 0 2128.954362 Tm 25.919444 0 Td 34.027778 Tz (I. ) Tj 0.641667 0 Td 38.888889 Tz (P. ) Tj 0.7 0 Td 53.619529 Tz (Georgakaki, ) Tj 3.752778 0 Td 49.259259 Tz (Proc. ) Tj 1.75 0 Td 45.37037 Tz (Natl. ) Tj 1.594444 0 Td 54.444444 Tz (Acad. ) Tj 1.866667 0 Td 42.939815 Tz (Sci. ) Tj 1.322222 0 Td 49.151235 Tz (U.S.A. ) Tj 2.002778 0 Td 54.444444 Tz (2003, ) Tj 1.925 0 Td 48.611111 Tz (100, ) Tj 51.428571 0 0 51.428571 0 2084 Tm 25.919444 0 Td 55.416667 Tz (3683-3688; ) Tj 3.538889 0 Td 46.990741 Tz (c\) ) Tj 0.719444 0 Td 55.092593 Tz (C. ) Tj 0.816667 0 Td 49.907407 Tz (Tard, ) Tj 1.672222 0 Td 59.953704 Tz (X. ) Tj 0.913889 0 Td 47.800926 Tz (Liu, ) Tj 1.341667 0 Td 48.611111 Tz (S. ) Tj 0.758333 0 Td 56.712963 Tz (K. ) Tj 0.913889 0 Td 50.636574 Tz (Ibrahim, ) Tj 2.644444 0 Td 66.435185 Tz (M. ) Tj 0.991667 0 Td 50.231481 Tz (Bruschi, ) Tj 51.428571 0 0 51.428571 0 2042.218798 Tm 25.938889 0 Td 48.611111 Tz (L. ) Tj 1.011111 0 Td 55.092593 Tz (D. ) Tj 1.069444 0 Td 49.151235 Tz (Gioia, ) Tj 2.197222 0 Td 43.75 Tz (S. ) Tj 0.913889 0 Td 55.092593 Tz (C. ) Tj 1.088889 0 Td 51.388889 Tz (Davies, ) Tj 2.547222 0 Td 58.333333 Tz (X. ) Tj 1.069444 0 Td 55.740741 Tz (Yang, ) Tj 2.080556 0 Td 46.018519 Tz (L.-S. ) Tj 1.827778 0 Td 60.925926 Tz (Wang, ) Tj 2.216667 0 Td 56.712963 Tz (G. ) Tj 51.428571 0 0 51.428571 0 1999 Tm 25.938889 0 Td 53.703704 Tz (Sawers, ) Tj 2.508333 0 Td 56.712963 Tz (C. ) Tj 0.933333 0 Td 38.888889 Tz (J. ) Tj 0.738889 0 Td 45.37037 Tz (Pickett, ) Tj 2.508333 0 Td 54.552469 Tz (Nature ) Tj 2.216667 0 Td 54.444444 Tz (2005, ) Tj 1.905556 0 Td 51.851852 Tz (433, ) Tj 1.536111 0 Td 54.282407 Tz (610-613; ) Tj 2.877778 0 Td 51.851852 Tz (d\) ) Tj 0.913889 0 Td 46.990741 Tz (L. ) Tj 55.714286 0 0 55.714286 0 1959 Tm 23.94359 0 Td 50.106838 Tz (Sun, ) Tj 1.435897 0 Td 47.863248 Tz (B. ) Tj 0.789744 0 Td 52.849003 Tz (Akermark, ) Tj 3.051282 0 Td 46.367521 Tz (S. ) Tj 0.753846 0 Td 42.628205 Tz (Ott, ) Tj 1.238462 0 Td 49.358974 Tz (Coord. ) Tj 2.064103 0 Td 55.042735 Tz (Chem. ) Tj 1.938462 0 Td 42.628205 Tz (Rev. ) Tj 1.274359 0 Td 49.65812 Tz (2005, ) Tj 1.705128 0 Td 48.611111 Tz (249, ) Tj 51.428571 0 0 51.428571 0 1915 Tm 25.997222 0 Td 54.12037 Tz (1653-1663; ) Tj 3.85 0 Td 46.990741 Tz (e\) ) Tj 1.108333 0 Td 46.990741 Tz (S. ) Tj 1.166667 0 Td 59.82906 Tz (Kaur-Ghumaan, ) Tj 5.269444 0 Td 46.990741 Tz (L. ) Tj 1.166667 0 Td 53.292181 Tz (Schwartz, ) Tj 3.480556 0 Td 50.231481 Tz (R. ) Tj 51.428571 0 0 51.428571 0 1875.174825 Tm 25.938889 0 Td 58.796296 Tz (Lomoth, ) Tj 2.741667 0 Td 64.814815 Tz (M. ) Tj 1.088889 0 Td 45.910494 Tz (Stein, ) Tj 1.925 0 Td 45.37037 Tz (S. ) Tj 0.816667 0 Td 46.180556 Tz (Ott, ) Tj 1.361111 0 Td 56.712963 Tz (Angew. ) Tj 2.391667 0 Td 55.092593 Tz (Chem., ) Tj 2.333333 0 Td 35.648148 Tz (Int. ) Tj 1.244444 0 Td 48.611111 Tz (Ed. ) Tj 1.205556 0 Td 53.148148 Tz (2010, ) Tj 51.428571 0 0 51.428571 0 1836.054201 Tm 25.919444 0 Td 50.771605 Tz (49, ) Tj 1.186111 0 Td 55.092593 Tz (8033-8036: ) Tj 3.655556 0 Td 37.268519 Tz (f\) ) Tj 0.738889 0 Td 53.472222 Tz (R. ) Tj 0.933333 0 Td 53.472222 Tz (Mejia-Rodriguez, ) Tj 5.444444 0 Td 56.712963 Tz (D. ) Tj 0.933333 0 Td 59.41358 Tz (Chong, ) Tj 2.411111 0 Td 37.268519 Tz (J. ) Tj 0.777778 0 Td 53.472222 Tz (H. ) Tj 51.428571 0 0 51.428571 0 1796.621024 Tm 25.938889 0 Td 51.041667 Tz (Reibenspies, ) Tj 3.986111 0 Td 66.435185 Tz (M. ) Tj 1.147222 0 Td 37.268519 Tz (P. ) Tj 0.777778 0 Td 49.016204 Tz (Soriaga, ) Tj 2.683333 0 Td 66.435185 Tz (M. ) Tj 1.088889 0 Td 48.611111 Tz (Y. ) Tj 0.933333 0 Td 53.472222 Tz (Darensbourg, ) Tj 4.141667 0 Td 38.888889 Tz (J. ) Tj 0.816667 0 Td 60.493827 Tz (Am. ) Tj 51.428571 0 0 51.428571 0 1753.108108 Tm 25.938889 0 Td 60.277778 Tz (Chem. ) Tj 2.002778 0 Td 49.421296 Tz (Soc. ) Tj 1.4 0 Td 53.796296 Tz (2004, ) Tj 1.847222 0 Td 49.421296 Tz (126, ) Tj 1.419444 0 Td 56.712963 Tz (12004-12014;g\) ) Tj 4.938889 0 Td 38.888889 Tz (F. ) Tj 0.641667 0 Td 55.452675 Tz (Gloaguen, ) Tj 3.15 0 Td 37.268519 Tz (J. ) Tj 0.661111 0 Td 53.472222 Tz (D. ) Tj 48.571429 0 0 48.571429 0 1710 Tm 27.464706 0 Td 59.477124 Tz (Lawrence, ) Tj 3.397059 0 Td 49.754902 Tz (T. ) Tj 0.823529 0 Td 53.186275 Tz (B. ) Tj 0.885294 0 Td 55.931373 Tz (Rauchfuss, ) Tj 3.520588 0 Td 42.892157 Tz (J. ) Tj 0.7 0 Td 66.339869 Tz (Am. ) Tj 1.482353 0 Td 63.137255 Tz (Chem. ) Tj 2.141176 0 Td 51.470588 Tz (Soc. ) Tj 1.461765 0 Td 58.333333 Tz (2001, ) Tj 2.017647 0 Td 52.328431 Tz (123, ) Tj 51.428571 0 0 51.428571 0 1669.012146 Tm 25.938889 0 Td 55.092593 Tz (9476-9477; ) Tj 3.577778 0 Td 51.851852 Tz (h\) ) Tj 0.913889 0 Td 37.268519 Tz (F. ) Tj 0.738889 0 Td 59.62963 Tz (Wang, ) Tj 2.1 0 Td 56.388889 Tz (W.-G. ) Tj 1.983333 0 Td 60.277778 Tz (Wang, ) Tj 2.061111 0 Td 47.962963 Tz (X.-J. ) Tj 1.711111 0 Td 60.925926 Tz (Wang, ) Tj 2.138889 0 Td 49.259259 Tz (H.-Y. ) Tj 52.857143 0 0 52.857143 0 1626.305595 Tm 25.218919 0 Td 60.540541 Tz (Wang, ) Tj 2.137838 0 Td 52.342342 Tz (C.-H. ) Tj 1.910811 0 Td 54.864865 Tz (Tung, ) Tj 2.005405 0 Td 46.666667 Tz (L.-Z. ) Tj 1.759459 0 Td 64.114114 Tz (Wu, ) Tj 1.494595 0 Td 55.18018 Tz (Angew. ) Tj 2.421622 0 Td 53.603604 Tz (Chem., ) Tj 2.364865 0 Td 34.684685 Tz (Int. ) Tj 1.286486 0 Td 47.297297 Tz (Ed. ) Tj 51.428571 0 0 51.428571 0 1582 Tm 25.919444 0 Td 53.796296 Tz (2011, ) Tj 1.847222 0 Td 49.691358 Tz (50, ) Tj 1.127778 0 Td 55.416667 Tz (3193-3197; ) Tj 3.577778 0 Td 37.268519 Tz (i\) ) Tj 0.661111 0 Td 40.509259 Tz (P. ) Tj 0.738889 0 Td 51.262626 Tz (Poddutoori, ) Tj 3.655556 0 Td 55.092593 Tz (D. ) Tj 0.875 0 Td 46.990741 Tz (T. ) Tj 0.816667 0 Td 42.12963 Tz (Co., ) Tj 1.225 0 Td 56.712963 Tz (A. ) Tj 0.894444 0 Td 40.509259 Tz (P. ) Tj 0.738889 0 Td 46.990741 Tz (S. ) Tj 51.428571 0 0 51.428571 0 1541.385042 Tm 25.938889 0 Td 56.018519 Tz (Samuel, ) Tj 2.625 0 Td 53.472222 Tz (C. ) Tj 0.933333 0 Td 55.092593 Tz (H. ) Tj 0.972222 0 Td 60.763889 Tz (Kim, ) Tj 1.730556 0 Td 64.814815 Tz (M. ) Tj 1.069444 0 Td 45.37037 Tz (T. ) Tj 0.836111 0 Td 50.636574 Tz (Vagnini, ) Tj 2.702778 0 Td 66.435185 Tz (M. ) Tj 1.127778 0 Td 48.611111 Tz (R. ) Tj 0.913889 0 Td 52.662037 Tz (Wasielewski, ) Tj 51.428571 0 0 51.428571 0 1501.139785 Tm 25.958333 0 Td 56.17284 Tz (Energy ) Tj 2.275 0 Td 49.826389 Tz (Environ. ) Tj 2.625 0 Td 42.12963 Tz (Sci. ) Tj 1.283333 0 Td 51.851852 Tz (2011, ) Tj 1.769444 0 Td 45.37037 Tz (4, ) Tj 0.738889 0 Td 55.092593 Tz (2441-2450; ) Tj 3.752778 0 Td 35.648148 Tz (\) ) Tj 0.408333 0 Td 63.194444 Tz (W. ) Tj 0.952778 0 Td 68.055556 Tz (M. ) Tj 1.030556 0 Td 51.311728 Tz (Singh, ) Tj 51.428571 0 0 51.428571 0 1458.303071 Tm 25.938889 0 Td 55.092593 Tz (D. ) Tj 0.894444 0 Td 56.481481 Tz (Pegram, ) Tj 2.586111 0 Td 53.472222 Tz (H. ) Tj 0.855556 0 Td 57.037037 Tz (Duan, ) Tj 1.944444 0 Td 55.092593 Tz (D. ) Tj 0.894444 0 Td 44.907407 Tz (Kalita, ) Tj 2.1 0 Td 38.888889 Tz (P. ) Tj 0.661111 0 Td 57.407407 Tz (Simone, ) Tj 2.586111 0 Td 58.333333 Tz (G. ) Tj 0.894444 0 Td 50.231481 Tz (L. ) Tj 0.836111 0 Td 58.333333 Tz (Emmert, ) Tj 51.428571 0 0 51.428571 0 1416.186014 Tm 25.9 0 Td 59.953704 Tz (X. ) Tj 0.991667 0 Td 54.444444 Tz (Zhao, ) Tj 1.886111 0 Td 57.253086 Tz (Angew. ) Tj 2.411111 0 Td 54.552469 Tz (Chem., ) Tj 2.313889 0 Td 37.268519 Tz (Int. ) Tj 1.225 0 Td 49.691358 Tz (Ed. ) Tj 1.166667 0 Td 55.092593 Tz (2012, ) Tj 1.925 0 Td 47.530864 Tz (51, ) Tj 1.205556 0 Td 53.796296 Tz (1653-1656. ) Tj 51.428571 0 0 51.428571 0 1375.171303 Tm 25.433333 0 Td 58.333333 Tz (5 ) Tj 0.875 0 Td 48.611111 Tz (a\) ) Tj 0.816667 0 Td 56.712963 Tz (A. ) Tj 1.011111 0 Td 64.814815 Tz (M. ) Tj 1.05 0 Td 54.012346 Tz (Appel, ) Tj 2.275 0 Td 53.472222 Tz (D. ) Tj 0.972222 0 Td 48.611111 Tz (L. ) Tj 0.913889 0 Td 56.481481 Tz (DuBois, ) Tj 2.644444 0 Td 68.055556 Tz (M. ) Tj 1.166667 0 Td 48.611111 Tz (R. ) Tj 0.933333 0 Td 56.018519 Tz (DuBois, ) Tj 2.605556 0 Td 40.509259 Tz (J. ) Tj 0.797222 0 Td 61.574074 Tz (Am. ) Tj 51.428571 0 0 51.428571 0 1332 Tm 25.938889 0 Td 60.277778 Tz (Chem. ) Tj 2.022222 0 Td 48.611111 Tz (Soc. ) Tj 1.4 0 Td 54.444444 Tz (2005, ) Tj 1.866667 0 Td 48.611111 Tz (127, ) Tj 1.419444 0 Td 55.632716 Tz (12717-12726; ) Tj 4.180556 0 Td 50.231481 Tz (b\) ) Tj 0.816667 0 Td 53.472222 Tz (H. ) Tj 0.836111 0 Td 32.407407 Tz (I. ) Tj 0.583333 0 Td 54.208754 Tz (Karunadasa, ) Tj 51.428571 0 0 51.428571 0 1293.14147 Tm 25.919444 0 Td 53.472222 Tz (C. ) Tj 0.894444 0 Td 37.268519 Tz (J. ) Tj 0.719444 0 Td 57.79321 Tz (Chang, ) Tj 2.313889 0 Td 38.888889 Tz (J. ) Tj 0.758333 0 Td 50.231481 Tz (R. ) Tj 0.913889 0 Td 55.740741 Tz (Long, ) Tj 1.944444 0 Td 55.092593 Tz 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51.428571 0 0 51.428571 0 1169.038674 Tm 25.938889 0 Td 58.333333 Tz (Du, ) Tj 1.263889 0 Td 56.712963 Tz (G. ) Tj 0.952778 0 Td 54.282407 Tz (Luo, ) Tj 1.575 0 Td 48.611111 Tz (B. ) Tj 0.855556 0 Td 49.016204 Tz (Lindley, ) Tj 2.586111 0 Td 48.611111 Tz (R. ) Tj 0.894444 0 Td 49.907407 Tz (Eisenberg, ) Tj 3.188889 0 Td 40.509259 Tz (J. ) Tj 0.738889 0 Td 60.493827 Tz (Am. ) Tj 1.4 0 Td 58.981481 Tz (Chem. ) Tj 2.022222 0 Td 49.421296 Tz (Soc. ) Tj 51.428571 0 0 51.428571 0 1127.029024 Tm 25.919444 0 Td 54.444444 Tz (2009, ) Tj 1.886111 0 Td 49.421296 Tz (131, ) Tj 1.361111 0 Td 55.740741 Tz (9192-9194; ) Tj 3.538889 0 Td 48.611111 Tz (c\) ) Tj 0.738889 0 Td 38.888889 Tz (P. ) Tj 0.7 0 Td 54.552469 Tz (Zhang, ) Tj 2.197222 0 Td 68.055556 Tz (M. ) Tj 0.991667 0 Td 60.925926 Tz (Wang, ) Tj 2.022222 0 Td 37.268519 Tz (J. ) Tj 0.641667 0 Td 59.62963 Tz (Dong, ) Tj 1.963889 0 Td 56.712963 Tz (X. ) Tj 51.428571 0 0 51.428571 0 1084.916435 Tm 25.919444 0 Td 46.450617 Tz (Li, ) Tj 1.069444 0 Td 40.509259 Tz (F. ) Tj 0.719444 0 Td 60.925926 Tz (Wang, ) Tj 2.041667 0 Td 50.231481 Tz (L. ) Tj 0.816667 0 Td 65.895062 Tz (Wu, ) Tj 1.438889 0 Td 46.990741 Tz (L. ) Tj 0.758333 0 Td 55.092593 Tz (Sun, ) Tj 1.497222 0 Td 42.12963 Tz (J. ) Tj 0.777778 0 Td 50.555556 Tz (Phys. ) Tj 1.788889 0 Td 60.277778 Tz (Chem. ) Tj 2.1 0 Td 84.259259 Tz (C ) Tj 0.622222 0 Td 55.092593 Tz (2010, ) Tj 1.944444 0 Td 47.800926 Tz (114, ) Tj 51.428571 0 0 51.428571 0 1041 Tm 25.977778 0 Td 55.632716 Tz (15868-15874; ) Tj 4.413889 0 Td 51.851852 Tz (d\) ) Tj 0.991667 0 Td 56.712963 Tz (A. ) Tj 1.088889 0 Td 43.75 Tz (Fihri, ) Tj 1.963889 0 Td 48.611111 Tz (V. ) Tj 0.952778 0 Td 49.074074 Tz (Artero, ) Tj 2.469444 0 Td 68.055556 Tz (M. ) Tj 1.244444 0 Td 51.851852 Tz (Razavet, ) Tj 2.897222 0 Td 53.472222 Tz (C. ) Tj 51.428571 0 0 51.428571 0 1001.150611 Tm 25.938889 0 Td 45.37037 Tz (Baffert, ) Tj 2.430556 0 Td 63.194444 Tz (W. ) Tj 1.05 0 Td 46.450617 Tz (Leibl, ) Tj 1.925 0 Td 66.435185 Tz (M. ) Tj 1.088889 0 Td 52.175926 Tz (Fontecave, ) Tj 3.363889 0 Td 57.253086 Tz (Angew. ) Tj 2.391667 0 Td 55.092593 Tz (Chem., ) Tj 2.313889 0 Td 36.458333 Tz (Int. ) Tj 1.225 0 Td 48.611111 Tz (Ed. ) Tj 51.428571 0 0 51.428571 0 958 Tm 25.919444 0 Td 54.444444 Tz (2008, ) Tj 1.808333 0 Td 50.771605 Tz (47, ) Tj 1.088889 0 Td 54.282407 Tz (564-567; ) Tj 2.780556 0 Td 46.990741 Tz (e\) ) Tj 0.777778 0 Td 55.092593 Tz (D. ) Tj 0.836111 0 Td 46.180556 Tz (Streich, ) Tj 2.372222 0 Td 51.851852 Tz (Y. ) Tj 0.777778 0 Td 45.833333 Tz (Astuti, ) Tj 2.1 0 Td 68.055556 Tz (M. ) Tj 1.011111 0 Td 49.421296 Tz (Orlandi, ) Tj 2.605556 0 Td 46.990741 Tz (L. ) Tj 48.571429 0 0 48.571429 0 919 Tm 27.464706 0 Td 56.427015 Tz (Schwartz, ) Tj 3.397059 0 Td 51.470588 Tz (R. ) Tj 0.967647 0 Td 61.27451 Tz (Lomoth, ) Tj 2.882353 0 Td 51.470588 Tz (L. ) Tj 0.967647 0 Td 63.76634 Tz (Hammarstrm, ) Tj 4.9 0 Td 48.039216 Tz (S. ) Tj 0.885294 0 Td 48.897059 Tz (Ott, ) Tj 1.482353 0 Td 61.764706 Tz (Chem.- ) Tj 51.428571 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0.988235 0 Td 72.058824 Tz (M. ) Tj 1.255882 0 Td 64.852941 Tz (McCormick, ) Tj 4.282353 0 Td 56.617647 Tz (B. ) Tj 1.091176 0 Td 58.333333 Tz (D. ) Tj 1.111765 0 Td 48.039216 Tz (Calitree, ) Tj 2.923529 0 Td 61.764706 Tz (A. ) Tj 1.152941 0 Td 55.759804 Tz (Orchard, ) Tj 3.026471 0 Td 63.480392 Tz (N. ) Tj 1.194118 0 Td 56.617647 Tz (D. ) Tj 51.428571 0 0 51.428571 0 754.088889 Tm 25.938889 0 Td 50.771605 Tz (Kraut, ) Tj 2.158333 0 Td 40.509259 Tz (F. ) Tj 0.797222 0 Td 48.611111 Tz (V. ) Tj 0.972222 0 Td 46.759259 Tz (Bright, ) Tj 2.313889 0 Td 64.814815 Tz (M. ) Tj 1.166667 0 Td 50.231481 Tz (R. ) Tj 0.952778 0 Td 48.070988 Tz (Detty, ) Tj 2.1 0 Td 48.611111 Tz (R. ) Tj 0.972222 0 Td 50.231481 Tz (Eisenberg, ) Tj 3.305556 0 Td 38.888889 Tz (J. ) Tj 0.836111 0 Td 60.493827 Tz (Am. ) Tj 51.428571 0 0 51.428571 0 709 Tm 25.938889 0 Td 60.277778 Tz (Chem. ) Tj 2.177778 0 Td 50.231481 Tz (Soc. ) Tj 1.575 0 Td 54.444444 Tz (2010, ) Tj 2.041667 0 Td 50.231481 Tz (132, ) Tj 1.613889 0 Td 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0 0 40 0 2464 Tm 9 0 Td 102.083333 Tz (We ) Tj 1.55 0 Td 62.5 Tz (claim: ) Tj 51.428571 0 0 51.428571 0 2416.251082 Tm 7.038889 0 Td 38.888889 Tz (1. ) Tj 0.7 0 Td 87.5 Tz (A ) Tj 0.758333 0 Td 52.5 Tz (metal ) Tj 1.808333 0 Td 60.185185 Tz (complex ) Tj 2.761111 0 Td 59.953704 Tz (of ) Tj 0.855556 0 Td 54.62963 Tz (formula ) Tj 2.547222 0 Td 36.458333 Tz (\(I\): ) Tj 40 0 0 40 0 2306 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 2258 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.926471 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 47.696078 Tz (transition ) Tj 3.191176 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 2222.517241 Tm 7 0 Td 84.259259 Tz (G ) Tj 0.972222 0 Td 37.268519 Tz (is ) Tj 0.913889 0 Td 50.462963 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 2181 Tm 7.719444 0 Td 53.337191 Tz (pyridin-2-yl\)methanamine ) Tj 7.933333 0 Td 56.712963 Tz (\(DIQ-Bpy\): ) Tj 51.428571 0 0 51.428571 0 2136.309278 Tm 6.980556 0 Td 50.231481 Tz (Y, ) Tj 0.855556 0 Td 48.611111 Tz (for ) Tj 1.030556 0 Td 55.092593 Tz (each ) Tj 1.555556 0 Td 50.673401 Tz (occurrence, ) Tj 3.558333 0 Td 52.599715 Tz (independently ) Tj 4.336111 0 Td 38.888889 Tz (is ) Tj 0.661111 0 Td 58.333333 Tz (a ) Tj 0.525 0 Td 55.555556 Tz (halogen ) Tj 2.527778 0 Td 56.388889 Tz (group ) Tj 51.428571 0 0 51.428571 0 2093.672131 Tm 7.719444 0 Td 53.472222 Tz (or ) Tj 0.855556 0 Td 51.851852 Tz (a ) Tj 0.583333 0 Td 53.796296 Tz (water ) Tj 1.847222 0 Td 51.851852 Tz (moiety; ) Tj 51.428571 0 0 51.428571 0 2050.468705 Tm 6.980556 0 Td 59.953704 Tz (X, ) Tj 0.952778 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 51.262626 Tz (occurrence, ) Tj 3.616667 0 Td 52.849003 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 49.691358 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 2009.418006 Tm 7 0 Td 90.740741 Tz (m ) Tj 0.816667 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 51.851852 Tz (the ) Tj 1.205556 0 Td 61.574074 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 1967.463576 Tm 7 0 Td 58.333333 Tz (n ) Tj 0.622222 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 50.771605 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 52.391975 Tz (anions ) Tj 2.138889 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 55.497685 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 1926 Tm 7.432353 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 41.176471 Tz (is ) Tj 0.761765 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 54.901961 Tz (or ) Tj 0.885294 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50 Tz (neutral ) Tj 2.408824 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 1883.981457 Tm 7 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 37.268519 Tz (is ) Tj 0.661111 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 61.033951 Tz (number ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 47.222222 Tz (neutral ) Tj 2.255556 0 Td 53.652263 Tz (molecules ) Tj 3.130556 0 Td 54.012346 Tz (per ) Tj 1.166667 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex. ) Tj 51.428571 0 0 51.428571 0 1842.421488 Tm 7 0 Td 42.12963 Tz (2. ) Tj 0.758333 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 53.148148 Tz (metal ) Tj 1.866667 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.875 0 Td 53.148148 Tz (claim ) Tj 1.925 0 Td 38.888889 Tz (1, ) Tj 0.777778 0 Td 55.092593 Tz (wherein ) Tj 2.586111 0 Td 48.611111 Tz (said ) Tj 1.438889 0 Td 53.148148 Tz (metal ) Tj 1.847222 0 Td 40.509259 Tz (is ) Tj 40 0 0 40 0 1807 Tm 8.05 0 Td 59.52381 Tz (cobalt. ) Tj 51.428571 0 0 51.428571 0 1758.401617 Tm 7 0 Td 42.12963 Tz (3. ) Tj 0.738889 0 Td 63.734568 Tz (The ) Tj 1.4 0 Td 52.5 Tz (metal ) Tj 1.808333 0 Td 60.185185 Tz (complex ) Tj 2.761111 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (claim ) Tj 1.866667 0 Td 43.75 Tz (2, ) Tj 0.777778 0 Td 55.092593 Tz (wherein ) Tj 2.547222 0 Td 84.259259 Tz (Y ) Tj 0.7 0 Td 40.509259 Tz (is ) Tj 0.719444 0 Td 47.170782 Tz (chloride. ) Tj 51.428571 0 0 51.428571 0 1717.452514 Tm 7 0 Td 42.12963 Tz (4. ) Tj 0.738889 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 49.151235 Tz (cobalt ) Tj 2.002778 0 Td 60.185185 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 52.5 Tz (claim ) Tj 1.847222 0 Td 43.75 Tz (3, ) Tj 0.797222 0 Td 54.62963 Tz (wherein ) Tj 2.547222 0 Td 51.851852 Tz (a ) Tj 0.544444 0 Td 38.888889 Tz (is ) Tj 0.738889 0 Td 40.509259 Tz (0; ) Tj 0.758333 0 Td 59.41358 Tz (and ) Tj 1.283333 0 Td 87.5 Tz (X ) Tj 40 0 0 40 0 1682 Tm 8.05 0 Td 50 Tz (is ) Tj 0.975 0 Td 60.416667 Tz (CIT. ) Tj 52.857143 0 0 52.857143 0 1634.106122 Tm 6.810811 0 Td 40.990991 Tz (5. ) Tj 0.737838 0 Td 85.135135 Tz (A ) Tj 0.681081 0 Td 52.342342 Tz (metal ) Tj 1.816216 0 Td 58.108108 Tz (complex ) Tj 2.648649 0 Td 59.90991 Tz (of ) Tj 0.87027 0 Td 53.153153 Tz (formula ) Tj 2.478378 0 Td 36.261261 Tz (\(III\): ) Tj 41.428571 0 0 41.428571 0 1576 Tm 10.113793 0 Td 74.242424 Tz (M\(G\)Y\(X\)\(L\) ) Tj 51.428571 0 0 51.428571 0 1516.915966 Tm 7 0 Td 51.851852 Tz (or ) Tj 0.836111 0 Td 51.851852 Tz (a ) Tj 0.563889 0 Td 39.537037 Tz (salt, ) Tj 1.438889 0 Td 49.074074 Tz (solvate ) Tj 2.294444 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 52.777778 Tz (hydrate ) Tj 2.469444 0 Td 46.180556 Tz (thereof; ) Tj 40 0 0 40 0 1482 Tm 8.025 0 Td 73.214286 Tz (wherein ) Tj 48.571429 0 0 48.571429 0 1434 Tm 7.411765 0 Td 113.235294 Tz (M ) Tj 0.926471 0 Td 42.892157 Tz (is ) Tj 0.761765 0 Td 61.764706 Tz (a ) Tj 0.638235 0 Td 47.696078 Tz (transition ) Tj 3.191176 0 Td 51.470588 Tz (metal; ) Tj 51.428571 0 0 51.428571 0 1398.509804 Tm 7 0 Td 84.259259 Tz (G ) Tj 0.913889 0 Td 38.888889 Tz (is ) Tj 0.913889 0 Td 51.716821 Tz (6'-\(\(bis\(pyridin-2-ylmethyl\)amino\)methyl\)-N,N-di ) Tj 51.428571 0 0 51.428571 0 1356.637363 Tm 7.719444 0 Td 50.846105 Tz (methyl-2,2'-bipyridin-6-amine ) Tj 9.780556 0 Td 59.82906 Tz (\(DPA-ABpy'\), ) Tj 5.619444 0 Td 53.472222 Tz (or ) Tj 51.428571 0 0 51.428571 0 1315 Tm 7.719444 0 Td 49.453704 Tz (N,N-bis\(\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 1274 Tm 7.719444 0 Td 53.337191 Tz (pyridin-2-yl\)methanamine ) Tj 7.933333 0 Td 56.712963 Tz (\(DIQ-Bpy\): ) Tj 51.428571 0 0 51.428571 0 1227.330818 Tm 6.980556 0 Td 50.231481 Tz (Y, ) Tj 0.777778 0 Td 49.691358 Tz (for ) Tj 0.991667 0 Td 55.902778 Tz (each ) Tj 1.516667 0 Td 50.968013 Tz (occurrence, ) Tj 3.558333 0 Td 52.350427 Tz (independently ) Tj 4.277778 0 Td 38.888889 Tz (is ) Tj 0.622222 0 Td 48.148148 Tz (absent, ) Tj 2.216667 0 Td 55.092593 Tz (a ) Tj 0.466667 0 Td 56.018519 Tz (halogen ) Tj 51.428571 0 0 51.428571 0 1187.780781 Tm 7.719444 0 Td 56.388889 Tz (group ) Tj 1.963889 0 Td 50.231481 Tz (or ) Tj 0.797222 0 Td 58.333333 Tz (a ) Tj 0.583333 0 Td 55.092593 Tz (water ) Tj 1.886111 0 Td 51.851852 Tz (moiety; ) Tj 40 0 0 40 0 2359 Tm 29.8 0 Td 37.5 Tz (\(I\) ) Tj 40 0 0 40 0 1577 Tm 29.325 0 Td 38.333333 Tz (\(III\) ) Tj 30 0 0 30 0 2547 Tm 41.5 0 Td 75 Tz (10 ) Tj 30 0 0 30 0 2339 Tm 41.5 0 Td 72.222222 Tz (15 ) Tj 30 0 0 30 0 1923 Tm 41.433333 0 Td 77.777778 Tz (25 ) Tj 30 0 0 30 0 1716 Tm 41.433333 0 Td 80.555556 Tz (30 ) Tj 30 0 0 30 0 1507 Tm 41.433333 0 Td 77.777778 Tz (35 ) Tj 30 0 0 30 0 1299 Tm 41.4 0 Td 83.333333 Tz (40 ) Tj 52.857143 0 0 52.857143 0 2968 Tm 32.540541 0 Td 77.252252 Tz (36 ) Tj 51.428571 0 0 51.428571 0 2915.45706 Tm 25.9 0 Td 59.953704 Tz (X, ) Tj 0.972222 0 Td 48.611111 Tz (for ) Tj 1.069444 0 Td 55.902778 Tz (each ) Tj 1.594444 0 Td 50.968013 Tz (occurrence, ) Tj 3.616667 0 Td 52.599715 Tz (independently ) Tj 4.394444 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 58.333333 Tz (an ) Tj 0.933333 0 Td 50.231481 Tz (anion; ) Tj 51.428571 0 0 51.428571 0 2872.425806 Tm 25.919444 0 Td 90.740741 Tz (m ) Tj 0.836111 0 Td 37.268519 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.205556 0 Td 61.033951 Tz (number ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.855556 0 Td 48.611111 Tz (cations ) Tj 2.275 0 Td 55.092593 Tz (per ) Tj 1.244444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex; ) Tj 51.428571 0 0 51.428571 0 2828.476821 Tm 25.919444 0 Td 58.333333 Tz (n ) Tj 0.641667 0 Td 37.268519 Tz (is ) Tj 0.7 0 Td 49.691358 Tz (the ) Tj 1.147222 0 Td 62.114198 Tz (number ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 52.932099 Tz (anions ) Tj 2.158333 0 Td 52.932099 Tz (per ) Tj 1.186111 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.902778 Tz (complex; ) Tj 48.571429 0 0 48.571429 0 2784 Tm 27.464706 0 Td 72.058824 Tz (L ) Tj 0.679412 0 Td 42.892157 Tz (is ) Tj 0.782353 0 Td 54.901961 Tz (absent ) Tj 2.244118 0 Td 53.186275 Tz (or ) Tj 0.864706 0 Td 58.333333 Tz (a ) Tj 0.617647 0 Td 50.490196 Tz (neutral ) Tj 2.429412 0 Td 54.901961 Tz (molecule; ) Tj 3.252941 0 Td 62.908497 Tz (and ) Tj 51.428571 0 0 51.428571 0 2740.965654 Tm 25.919444 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 38.888889 Tz (is ) Tj 0.680556 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 61.574074 Tz (number ) Tj 2.430556 0 Td 56.712963 Tz (of ) Tj 0.816667 0 Td 47.685185 Tz (neutral ) Tj 2.275 0 Td 53.652263 Tz (molecules ) Tj 3.130556 0 Td 52.932099 Tz (per ) Tj 1.166667 0 Td 53.148148 Tz (metal ) Tj 1.827778 0 Td 55.497685 Tz (complex. ) Tj 51.428571 0 0 51.428571 0 2696.429363 Tm 25.938889 0 Td 42.12963 Tz (6. ) Tj 0.738889 0 Td 64.814815 Tz (The ) Tj 1.419444 0 Td 51.851852 Tz (metal ) Tj 1.827778 0 Td 59.722222 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 53.796296 Tz (claim ) Tj 1.866667 0 Td 45.37037 Tz (5, ) Tj 0.797222 0 Td 55.555556 Tz (wherein ) Tj 2.586111 0 Td 106.944444 Tz (M ) Tj 0.875 0 Td 42.12963 Tz (is ) Tj 0.738889 0 Td 55.092593 Tz (Co, ) Tj 1.322222 0 Td 52.932099 Tz (Ru, ) Tj 48.571429 0 0 48.571429 0 2653 Tm 26.682353 0 Td 51.470588 Tz (Ni, ) Tj 1.235294 0 Td 54.901961 Tz (or ) Tj 0.905882 0 Td 50.326797 Tz (Fe. ) Tj 51.428571 0 0 51.428571 0 2609.501433 Tm 25.919444 0 Td 43.75 Tz (7. ) Tj 0.855556 0 Td 63.734568 Tz (The ) Tj 1.477778 0 Td 53.148148 Tz (metal ) Tj 1.886111 0 Td 60.648148 Tz (complex ) Tj 2.838889 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 53.796296 Tz (claim ) Tj 1.963889 0 Td 43.75 Tz (6, ) Tj 0.855556 0 Td 55.092593 Tz (wherein ) Tj 2.625 0 Td 87.5 Tz (G ) Tj 0.894444 0 Td 37.268519 Tz (is ) Tj 0.797222 0 Td 89.660494 Tz (DPA ) Tj 50 0 0 50 0 2571 Tm 25.92 0 Td 63.333333 Tz (ABpy. ) Tj 51.428571 0 0 51.428571 0 2521.401617 Tm 25.919444 0 Td 43.75 Tz (8. ) Tj 0.738889 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 51.851852 Tz (metal ) Tj 1.788889 0 Td 60.185185 Tz (complex ) Tj 2.741667 0 Td 59.953704 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (claim ) Tj 1.866667 0 Td 42.12963 Tz (6, ) Tj 0.719444 0 Td 55.555556 Tz (wherein ) Tj 2.547222 0 Td 87.5 Tz (Y ) Tj 0.738889 0 Td 37.268519 Tz (is ) Tj 0.661111 0 Td 51.851852 Tz (absent ) Tj 2.080556 0 Td 55.092593 Tz (or ) Tj 51.428571 0 0 51.428571 0 2481.115385 Tm 25.2 0 Td 55.092593 Tz (a ) Tj 0.583333 0 Td 54.444444 Tz (water ) Tj 1.886111 0 Td 49.537037 Tz (moiety. ) Tj 51.428571 0 0 51.428571 0 2434.481481 Tm 25.919444 0 Td 43.75 Tz (9. ) Tj 0.875 0 Td 63.734568 Tz (The ) Tj 1.516667 0 Td 52.5 Tz (metal ) Tj 1.905556 0 Td 60.185185 Tz (complex ) Tj 2.858333 0 Td 56.712963 Tz (of ) Tj 0.933333 0 Td 53.148148 Tz (claim ) Tj 1.983333 0 Td 43.75 Tz (6, ) Tj 0.875 0 Td 55.092593 Tz (wherein ) Tj 2.683333 0 Td 48.611111 Tz (said ) Tj 1.516667 0 Td 53.148148 Tz (metal ) Tj 51.428571 0 0 51.428571 0 2394.896962 Tm 25.2 0 Td 59.722222 Tz (complex ) Tj 3.052778 0 Td 37.268519 Tz (is ) Tj 1.205556 0 Td 69.513889 Tz (NiCDPA-ABpy\)\(OH\)\(BF\) ) Tj 9.119444 0 Td 53.472222 Tz (or ) Tj 1.302778 0 Td 77.237654 Tz (Co\(DPA ) Tj 52.857143 0 0 52.857143 0 2348.816092 Tm 24.5 0 Td 69.054054 Tz (ABpy\)\(PF\), ) Tj 4.389189 0 Td 52.027027 Tz (or ) Tj 0.813514 0 Td 56.756757 Tz (a ) Tj 0.567568 0 Td 38.468468 Tz (salt, ) Tj 1.418919 0 Td 47.747748 Tz (solvate ) Tj 2.213514 0 Td 52.027027 Tz (or ) Tj 0.832432 0 Td 50.900901 Tz (hydrate ) Tj 2.383784 0 Td 44.538288 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 2306.549237 Tm 25.938889 0 Td 48.611111 Tz (10. ) Tj 1.127778 0 Td 84.259259 Tz (A ) Tj 0.7 0 Td 46.585648 Tz (catalyst ) Tj 2.488889 0 Td 54.12037 Tz (comprising ) Tj 3.480556 0 Td 58.333333 Tz (a ) Tj 0.622222 0 Td 51.851852 Tz (metal ) Tj 1.808333 0 Td 59.259259 Tz (complex ) Tj 2.761111 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (claim ) Tj 1.886111 0 Td 40.509259 Tz (1. ) Tj 51.428571 0 0 51.428571 0 2263.656458 Tm 25.938889 0 Td 46.450617 Tz (11. ) Tj 1.108333 0 Td 84.259259 Tz (A ) Tj 0.719444 0 Td 52.314815 Tz (process ) Tj 2.508333 0 Td 47.530864 Tz (for ) Tj 1.088889 0 Td 55.092593 Tz (producing ) Tj 3.208333 0 Td 57.523148 Tz (hydrogen ) Tj 3.052778 0 Td 58.333333 Tz (from ) Tj 1.672222 0 Td 56.712963 Tz (an ) Tj 0.952778 0 Td 56.944444 Tz (aqueous ) Tj 51.428571 0 0 51.428571 0 2219.51465 Tm 25.219444 0 Td 48.206019 Tz (Solution ) Tj 2.547222 0 Td 54.768519 Tz (comprising ) Tj 3.480556 0 Td 58.333333 Tz (a ) Tj 0.602778 0 Td 46.180556 Tz (step ) Tj 1.380556 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 55.632716 Tz (adding ) Tj 2.236111 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 46.180556 Tz (catalyst ) Tj 2.430556 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (claim ) Tj 1.866667 0 Td 56.712963 Tz (10 ) Tj 51.428571 0 0 51.428571 0 2173.863905 Tm 25.180556 0 Td 46.990741 Tz (to ) Tj 0.855556 0 Td 47.800926 Tz (said ) Tj 1.380556 0 Td 56.018519 Tz (aqueous ) Tj 2.625 0 Td 46.450617 Tz (solution. ) Tj 51.428571 0 0 51.428571 0 2130.571995 Tm 25.938889 0 Td 48.611111 Tz (12. ) Tj 1.088889 0 Td 64.814815 Tz (The ) Tj 1.341667 0 Td 51.388889 Tz (process ) Tj 2.411111 0 Td 56.712963 Tz (of ) Tj 0.797222 0 Td 52.5 Tz (claim ) Tj 1.847222 0 Td 46.450617 Tz (11, ) Tj 1.05 0 Td 47.685185 Tz (further ) Tj 2.197222 0 Td 54.444444 Tz (comprising ) Tj 3.480556 0 Td 55.092593 Tz (a ) Tj 0.544444 0 Td 47.800926 Tz (step ) Tj 1.380556 0 Td 56.712963 Tz (of ) Tj 51.428571 0 0 51.428571 0 2089.653465 Tm 25.2 0 Td 50.636574 Tz (carrying ) Tj 2.663889 0 Td 50.771605 Tz (out ) Tj 1.127778 0 Td 45.910494 Tz (electrolysis ) Tj 3.538889 0 Td 51.851852 Tz (or ) Tj 0.797222 0 Td 49.907407 Tz (photolysis ) Tj 3.247222 0 Td 58.333333 Tz (on ) Tj 0.913889 0 Td 50.771605 Tz (the ) Tj 1.127778 0 Td 56.481481 Tz (aqueous ) Tj 2.586111 0 Td 60.763889 Tz (solu ) Tj 51.428571 0 0 51.428571 0 2045.8125 Tm 25.180556 0 Td 46.990741 Tz (tion ) Tj 1.419444 0 Td 50.87963 Tz (containing ) Tj 3.266667 0 Td 50.771605 Tz (the ) Tj 1.166667 0 Td 43.930041 Tz (catalyst. ) Tj 51.428571 0 0 51.428571 0 1998.47619 Tm 25.938889 0 Td 48.611111 Tz (13. ) Tj 1.108333 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 51.851852 Tz (process ) Tj 2.411111 0 Td 58.333333 Tz (of ) Tj 0.836111 0 Td 53.148148 Tz (claim ) Tj 1.847222 0 Td 49.691358 Tz (12, ) Tj 1.147222 0 Td 55.092593 Tz (wherein ) Tj 2.547222 0 Td 49.421296 Tz (said ) Tj 1.4 0 Td 56.481481 Tz (aqueous ) Tj 2.625 0 Td 59.953704 Tz (solu ) Tj 51.428571 0 0 51.428571 0 1955.990099 Tm 25.180556 0 Td 46.990741 Tz (tion ) Tj 1.419444 0 Td 54.372428 Tz (comprises ) Tj 3.169444 0 Td 50.231481 Tz (ascorbic ) Tj 2.644444 0 Td 46.018519 Tz (acid. ) Tj 51.428571 0 0 51.428571 0 1911.427807 Tm 25.958333 0 Td 48.611111 Tz (14. ) Tj 1.108333 0 Td 63.734568 Tz (The ) Tj 1.361111 0 Td 51.851852 Tz (process ) Tj 2.45 0 Td 56.712963 Tz (of ) Tj 0.836111 0 Td 53.796296 Tz (claim ) Tj 1.905556 0 Td 45.37037 Tz (11, ) Tj 1.088889 0 Td 55.092593 Tz (wherein ) Tj 2.566667 0 Td 49.421296 Tz (said ) Tj 1.419444 0 Td 46.585648 Tz (catalyst ) Tj 2.469444 0 Td 83.179012 Tz (com ) Tj 52.857143 0 0 52.857143 0 1872.674074 Tm 24.5 0 Td 46.246246 Tz (prises ) Tj 2.27027 0 Td 65.765766 Tz (NiCDPA-ABpy\)\(OH\)\(BF\), ) Tj 8.702703 0 Td 52.027027 Tz (or ) Tj 1.059459 0 Td 60.880111 Tz ([Co\(DPA-ABpy\) ) Tj 51.428571 0 0 51.428571 0 1824 Tm 25.219444 0 Td 66.759259 Tz (\(PF\). ) Tj 51.428571 0 0 51.428571 0 1783.388518 Tm 25.958333 0 Td 48.611111 Tz (15. ) Tj 1.05 0 Td 64.814815 Tz (The ) Tj 1.4 0 Td 51.851852 Tz (metal ) Tj 1.788889 0 Td 60.185185 Tz (complex ) Tj 2.741667 0 Td 58.333333 Tz (of ) Tj 0.816667 0 Td 53.148148 Tz (claim ) Tj 1.866667 0 Td 42.12963 Tz (1, ) Tj 0.719444 0 Td 55.555556 Tz (wherein ) Tj 2.547222 0 Td 87.5 Tz (G ) Tj 0.758333 0 Td 40.509259 Tz (is ) Tj 0.719444 0 Td 54.62963 Tz (N,N-bis ) Tj 51.428571 0 0 51.428571 0 1749 Tm 25.219444 0 Td 48.37963 Tz (\(\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\) ) Tj 51.428571 0 0 51.428571 0 1702.690667 Tm 25.2 0 Td 59.511785 Tz (methanamine ) Tj 4.180556 0 Td 56.064815 Tz (\(DIQ-Bpy\). ) Tj 51.428571 0 0 51.428571 0 1665.555006 Tm 25.958333 0 Td 48.611111 Tz (16. ) Tj 1.847222 0 Td 50.529101 Tz (N,N-bis\(isoquinolin-1-yl\)methyl\)\(6-\(pyridin-2-yl\) ) Tj 52.857143 0 0 52.857143 0 1623 Tm 24.518919 0 Td 50.828829 Tz (pyridin-2-yl\)methanamine. ) Tj 51.428571 0 0 51.428571 0 1579.49505 Tm 25.958333 0 Td 48.611111 Tz (17. ) Tj 1.05 0 Td 87.5 Tz (A ) Tj 0.738889 0 Td 51.851852 Tz (metal ) Tj 1.769444 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 55.416667 Tz (comprising ) Tj 3.519444 0 Td 52.441077 Tz (N,N-bis\(isoquinolin-1- ) Tj 51.428571 0 0 51.428571 0 1539.348416 Tm 25.180556 0 Td 50.605413 Tz (yl\)methyl\)\(6-\(pyridin-2-yl\)pyridin-2-yl\)methanamine, ) Tj 15.944444 0 Td 59.41358 Tz (and ) Tj 1.225 0 Td 55.092593 Tz (a ) Tj 51.428571 0 0 51.428571 0 1491.260809 Tm 25.180556 0 Td 46.342593 Tz (transition ) Tj 3.033333 0 Td 49.151235 Tz (metal; ) Tj 2.061111 0 Td 50.231481 Tz (or ) Tj 0.816667 0 Td 55.092593 Tz (a ) Tj 0.563889 0 Td 39.537037 Tz (salt, ) Tj 1.458333 0 Td 46.180556 Tz (Solvate, ) Tj 2.469444 0 Td 53.472222 Tz (or ) Tj 0.836111 0 Td 52.314815 Tz (hydrate ) Tj 2.430556 0 Td 46.180556 Tz (thereof. ) Tj 51.428571 0 0 51.428571 0 1450.323155 Tm 25.958333 0 Td 48.611111 Tz (18. ) Tj 1.011111 0 Td 63.734568 Tz (The ) Tj 1.322222 0 Td 53.148148 Tz (metal ) Tj 1.75 0 Td 60.185185 Tz (complex ) Tj 2.663889 0 Td 59.953704 Tz (of ) Tj 0.797222 0 Td 53.148148 Tz (claim ) Tj 1.808333 0 Td 48.611111 Tz (17, ) Tj 1.05 0 Td 55.092593 Tz (wherein ) Tj 2.508333 0 Td 49.691358 Tz (the ) Tj 1.069444 0 Td 45.694444 Tz (transition ) Tj 48.571429 0 0 48.571429 0 1409 Tm 26.723529 0 Td 55.588235 Tz (metal ) Tj 1.935294 0 Td 41.176471 Tz (is ) Tj 0.741176 0 Td 61.764706 Tz (Co, ) Tj 1.4 0 Td 58.333333 Tz (Ru, ) Tj 1.317647 0 Td 52.614379 Tz (Ni, ) Tj 1.235294 0 Td 54.901961 Tz (or ) Tj 0.926471 0 Td 49.183007 Tz (Fe. ) Tj 51.428571 0 0 51.428571 0 1368.683938 Tm 25.958333 0 Td 48.611111 Tz (19. ) Tj 1.030556 0 Td 64.814815 Tz (The ) Tj 1.380556 0 Td 52.5 Tz (metal ) Tj 1.769444 0 Td 59.722222 Tz (complex ) Tj 2.702778 0 Td 58.333333 Tz (of ) Tj 0.797222 0 Td 53.148148 Tz (claim ) Tj 1.847222 0 Td 47.530864 Tz (17, ) Tj 1.05 0 Td 55.555556 Tz (wherein ) Tj 2.566667 0 Td 48.611111 Tz (the ) Tj 1.030556 0 Td 60.185185 Tz (complex ) Tj 51.428571 0 0 51.428571 0 1327.157895 Tm 25.2 0 Td 47.685185 Tz (further ) Tj 2.236111 0 Td 54.012346 Tz (comprises ) Tj 3.15 0 Td 58.333333 Tz (an ) Tj 0.952778 0 Td 49.151235 Tz (anion. ) Tj 51.428571 0 0 51.428571 0 1284.900976 Tm 25.919444 0 Td 49.691358 Tz (20. ) Tj 1.205556 0 Td 63.734568 Tz (The ) Tj 1.438889 0 Td 60.185185 Tz (complex ) Tj 2.838889 0 Td 59.953704 Tz (of ) Tj 0.933333 0 Td 52.5 Tz (claim ) Tj 1.944444 0 Td 48.611111 Tz (17, ) Tj 1.225 0 Td 55.092593 Tz (wherein ) Tj 2.663889 0 Td 48.611111 Tz (the ) Tj 1.166667 0 Td 60.185185 Tz (complex ) Tj 2.838889 0 Td 40.509259 Tz (is ) Tj 51.428571 0 0 51.428571 0 1247.011173 Tm 25.433333 0 Td 58.117284 Tz (Ru\(DIQ-Bpy\)\(Cl\) ) Tj 5.502778 0 Td 57.685185 Tz (\(PF\). ) Tj 24.285714 0 0 24.285714 0 1195 Tm 67.117647 0 Td 68.627451 Tz (k ) Tj 2.305882 0 Td 68.627451 Tz (k ) Tj 2.347059 0 Td 68.627451 Tz (k ) Tj 2.305882 0 Td 68.627451 Tz (k ) Tj 2.305882 0 Td 68.627451 Tz (k ) Tj ET Q endstream endobj xref 4 1 0001847119 00000 n 9 1 0001847389 00000 n 14 1 0001847661 00000 n 19 1 0001847934 00000 n 24 1 0001848207 00000 n 29 1 0001848480 00000 n 34 1 0001848753 00000 n 39 1 0001849026 00000 n 44 1 0001849299 00000 n 49 1 0001849572 00000 n 54 1 0001849846 00000 n 59 1 0001850120 00000 n 64 1 0001850394 00000 n 69 1 0001850668 00000 n 74 1 0001850942 00000 n 79 1 0001851216 00000 n 84 1 0001851490 00000 n 89 1 0001851764 00000 n 94 1 0001852038 00000 n 99 1 0001852312 00000 n 104 1 0001852588 00000 n 109 1 0001852865 00000 n 114 1 0001853142 00000 n 119 1 0001853419 00000 n 124 1 0001853696 00000 n 129 1 0001853973 00000 n 134 1 0001854250 00000 n 139 1 0001854527 00000 n 144 1 0001854804 00000 n 149 1 0001855081 00000 n 154 1 0001855358 00000 n 159 1 0001855635 00000 n 169 1 0001855912 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